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1. 发明授权

US06518442B1 Process for the recovery of fluorinated alkandic acids from wastewater 有权
标题翻译：从废水中回收氟化烷基酸的工艺
公开(公告)号：US06518442B1
公开(公告)日：2003-02-11
申请号：US09700639
申请日：2000-11-16
申请人： Bernd Felix , Tilman Zipplies , Stephan Führer , Thomas Kaiser , Armin Budesheim
发明人： Bernd Felix , Tilman Zipplies , Stephan Führer , Thomas Kaiser , Armin Budesheim
IPC分类号： C07C5143
CPC分类号： C02F1/547 , B01J41/05 , C02F1/42 , C02F2101/14 , C07C51/47 , C07C53/21
摘要： The invention relates to a method for removing fluorinated emulsifying agent acids from waste waters, characterized in that the finely dispersed solids in the waste water are stabilized with a nonionic or cationic surfactant or an analogous acting surface active substance, the fluorinated emulsifying agent acids are subsequently bonded on an anion exchange resin and the fluorinated emulsifying agent acids are eluted from the latter.
摘要翻译：本发明涉及一种从废水中除去氟化乳化剂酸的方法，其特征在于废水中的细分散固体用非离子或阳离子表面活性剂或类似的作用表面活性物质来稳定，随后氟化乳化剂酸结合在阴离子交换树脂上，并且氟化乳化剂酸从后者中洗脱出来。

2. 发明授权

US5634963A Degassing apparatus and use thereof 失效
标题翻译：脱气装置及其用途
公开(公告)号：US5634963A
公开(公告)日：1997-06-03
申请号：US546614
申请日：1995-10-23
申请人： Herbert Strasser , Bernd Felix , Ulrich Reiff , Hans-Bodo Richter , Tilman Zipplies
发明人： Herbert Strasser , Bernd Felix , Ulrich Reiff , Hans-Bodo Richter , Tilman Zipplies
IPC分类号： B01D19/00 , B02C23/00 , B29B7/42 , B29B7/84 , B29C47/76
CPC分类号： B29C47/767 , B29C47/0009 , B29K2027/18
摘要： An apparatus suitable in particular for degassing fluoropolymers which have been subjected to thermal degradation contains--in the direction of flow of the product--a product intake, a coolable conveyor section, a comminution apparatus, a heated conveyor section and a product discharge, the entire apparatus being designed to be gastight and advantageously being designed to be resistant to pressure surges and having a gas outlet in the area of the coolable conveyor section and/or in the area of the comminution apparatuses.
摘要翻译：特别适用于对经过热降解的含氟聚合物进行脱气的设备包括 - 产品流动方向 - 产品入口，可冷却输送段，粉碎设备，加热输送段和产品排放物，整个设备被设计为气密的并且有利地设计成抵抗压力冲击并且在可冷却输送机部分的区域中和/或在粉碎设备的区域中具有气体出口。

3. 发明授权

US08222322B2 Method of making fluoropolymer dispersion 有权
标题翻译：制备含氟聚合物分散体的方法
公开(公告)号：US08222322B2
公开(公告)日：2012-07-17
申请号：US12684239
申请日：2010-01-08
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08L1/00
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method of making a fluoropolymer dispersion by first providing a fluoropolymer dispersion comprising fluoropolymer particles and one or more fluorinated surfactants selected from fluorinated carboxylic acids or salts thereof having the general formula: [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear fully fluorinated alkylene group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3; then adding one or more non-fluorinated surfactants selected from anionic and non-ionic surfactants followed by reducing the total amount of the one or more fluorinated surfactants to an amount of not more than 500 ppm, for example not more than 250 ppm based on the total weight of the dispersion while maintaining or increasing the amount of solids in the dispersion.
摘要翻译：首先提供含氟聚合物颗粒和一种或多种选自氟化羧酸或其盐的含氟表面活性剂的含氟聚合物分散体的制备方法，所述含氟聚合物分散体具有以下通式：[Rf-OL-COO-] iXi +（I）其中L表示线性全氟化亚烷基，Rf表示直链部分或完全氟化的脂族基团或被一个氧原子间隔的直链部分或全氟化的脂族基团，X i +表示i为i且i为1,2或3的阳离子; 然后加入一种或多种选自阴离子和非离子表面活性剂的非氟化表面活性剂，然后将一种或多种氟化表面活性剂的总量减少至不超过500ppm，例如不超过250ppm，基于分散体的总重量，同时保持或增加分散体中固体的量。

4. 发明授权

US07754795B2 Coating composition 有权
标题翻译：涂料组成
公开(公告)号：US07754795B2
公开(公告)日：2010-07-13
申请号：US11420431
申请日：2006-05-25
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08K5/00
CPC分类号： C09D127/18 , C08K5/06 , C08K5/09 , C08L27/12 , C08L71/02 , C08L2205/02 , C08L2205/03 , C08L2205/035 , C08L2666/02 , C08L2666/14
摘要： A coating composition having (i) an aqueous dispersion of fluoropolymer particles comprising a non-melt processible polymer of tetrafluoroethylene, (ii) a fluorinated surfactant, (iii) a non-ionic non-fluorinated surfactant and (iv) a non-fluorinated polymer, wherein the fluorinated surfactant is selected from fluorinated carboxylic acids or salts thereof of the general formula (I): [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear partially or fully fluorinated alkylene group or an aliphatic hydrocarbon group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one or more oxygen atoms, Xi+ represents a cation having the valence i and i is 1, 2 or 3.
摘要翻译：一种涂料组合物，其具有（i）含氟聚合物颗粒的水分散体，其包含四氟乙烯的不可熔融加工聚合物，（ii）氟化表面活性剂，（iii）非离子非氟化表面活性剂和（iv）非氟化聚合物其中氟化表面活性剂选自通式（I）的氟化羧酸或其盐：[Rf-OL-COO-] iXi +（I）其中L表示直链部分或完全氟化的亚烷基或脂族烃基 Rf表示直链部分或完全氟化的脂族基团或被一个或多个氧原子间隔的线性部分或全部氟化的脂肪族基团，Xi +表示i为i且i为1,2或3的阳离子。

5. 发明申请

US20100113679A1 METHOD OF MAKING FLUOROPOLYMER DISPERSION 有权
标题翻译：制备氟聚合物分散体的方法
公开(公告)号：US20100113679A1
公开(公告)日：2010-05-06
申请号：US12684239
申请日：2010-01-08
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G.I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Lochhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael C. Dadalas , George G.I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08L27/18
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method of making a fluoropolymer dispersion by first providing a fluoropolymer dispersion comprising fluoropolymer particles and one or more fluorinated surfactants selected from fluorinated carboxylic acids or salts thereof having the general formula: [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear fully fluorinated alkylene group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one oxygen atom, Xi+ represents a cation having the valence i and i is 1, 2 or 3;then adding one or more non-fluorinated surfactants selected from anionic and non-ionic surfactants followed by reducing the total amount of the one or more fluorinated surfactants to an amount of not more than 500 ppm, for example not more than 250 ppm based on the total weight of the dispersion while maintaining or increasing the amount of solids in the dispersion.
摘要翻译：首先提供含氟聚合物颗粒和一种或多种选自氟化羧酸或其盐的含氟表面活性剂的含氟聚合物分散体的制备方法，所述含氟聚合物分散体具有以下通式：[Rf-OL-COO-] iXi +（I）其中L表示线性全氟化亚烷基，Rf表示直链部分或完全氟化的脂族基团或被一个氧原子间隔的直链部分或全氟化的脂族基团，X i +表示i为i且i为1,2或3的阳离子; 然后加入一种或多种选自阴离子和非离子表面活性剂的非氟化表面活性剂，然后将一种或多种氟化表面活性剂的总量减少至不超过500ppm，例如不超过250ppm，基于分散体的总重量，同时保持或增加分散体中固体的量。

6. 发明申请

US20110245520A1 METHOD OF MAKING FLUORINATED ALKOXY CARBOXYLIC ACIDS AND PRECURSORS THEREOF 有权
标题翻译：制备氟化烷氧基羧酸及其前体的方法
公开(公告)号：US20110245520A1
公开(公告)日：2011-10-06
申请号：US13133734
申请日：2009-11-24
申请人： Tilman Zipplies , Klaus Hintzer , Oleg Shyshkov
发明人： Tilman Zipplies , Klaus Hintzer , Oleg Shyshkov
IPC分类号： C07C247/04 , C07C51/08
CPC分类号： C07C255/13 , C07C51/08 , C07C59/135 , C07C67/08 , C07C69/708 , C07C247/04 , C07C253/14
摘要： A method for preparing saturated partially fluorinated alkoxy carboxylic acids or salts thereof by treating a compound: (II), where Rf represents a fluorinated, linear or branched alkyl residue interruptible by one or more oxygen atoms, n is 0 or 1, with a Z-anion in a reaction medium comprising water and an organic solvent, where the Z-anion is selected from CN—, SCN— and OCN— or combinations thereof. A method of making partially fluorinated ethers of the general formula (I) wherein Rf is defined as above, n is 0 or 1, and Z is nitrile (—CN), azide (—N3), thiocyanate (—SCN) or cyanate (—OCN) group, said method comprising treating a fluorinated olefin of the general formula (II) wherein the Z-anion is CN—, OCN—, SCN— or N3−. A compound of the general formula (I) as previously described where Z is selected from SCN, OCN and N3.
摘要翻译：通过处理化合物（II）制备饱和部分氟化的烷氧基羧酸或其盐的方法，其中Rf表示可被一个或多个氧原子中断的氟化的直链或支链烷基，n为0或1，Z为阴离子在包含水和有机溶剂的反应介质中，其中Z-阴离子选自CN-，SCN-和OCN-或其组合。制备通式（I）的部分氟化醚的方法，其中Rf定义如上，n为0或1，Z为腈（-CN），叠氮化物（-N 3），硫氰酸酯（-SCN）或氰酸酯 -OCN）基团，所述方法包括处理通式（II）的氟化烯烃，其中Z-阴离子是CN-，OCN-，SCN-或N 3 - 。其中Z选自SCN，OCN和N 3，如前所述的通式（I）的化合物。

7. 发明授权

US07795332B2 Method of removing fluorinated carboxylic acid from aqueous liquid 有权
标题翻译：从含水液体中除去氟化羧酸的方法
公开(公告)号：US07795332B2
公开(公告)日：2010-09-14
申请号：US11420416
申请日：2006-05-25
申请人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Löchhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
发明人： Klaus Hintzer , Michael Jürgens , Harald Kaspar , Herbert Koenigsmann , Kai Helmut Löchhaas , Andreas R. Maurer , Werner Schwertfeger , Tilman Zipplies , George G. I. Moore , Jay F. Schulz , Richard M. Flynn
IPC分类号： C08L1/00
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method for removing a fluorinated carboxylic acid or salt thereof from an aqueous liquid by contacting the aqueous liquid with adsorbent particles. The fluorinated carboxylic acid or salt thereof is selected from the group consisting of partially fluorinated carboxylic acids or salts thereof and fully fluorinated carboxylic acids or salts thereof.
摘要翻译：通过使含水液体与吸附剂颗粒接触从水性液体中除去氟化羧酸或其盐的方法。氟化羧酸或其盐选自部分氟化的羧酸或其盐和完全氟化的羧酸或其盐。

8. 发明申请

US20070015864A1 METHOD OF MAKING FLUOROPOLYMER DISPERSION 有权
标题翻译：制备氟聚合物分散体的方法
公开(公告)号：US20070015864A1
公开(公告)日：2007-01-18
申请号：US11420386
申请日：2006-05-25
申请人： Klaus Hintzer , Michael Jurgens , Harald Kaspar , Herbert Koenigsmann , Kai Lochhaas , Andreas Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael Dadalas , George Moore , Jay Schulz , Richard Flynn
发明人： Klaus Hintzer , Michael Jurgens , Harald Kaspar , Herbert Koenigsmann , Kai Lochhaas , Andreas Maurer , Werner Schwertfeger , Tilman Zipplies , Ludwig Mayer , Michael Dadalas , George Moore , Jay Schulz , Richard Flynn
IPC分类号： C08L27/12
CPC分类号： C08L27/12 , C08L71/02 , Y02C20/30 , C08L2666/22
摘要： A method of making a fluoropolymer dispersion by first providing a fluoropolymer dispersion comprising fluoropolymer particles and one or more fluorinated surfactants selected from fluorinated carboxylic acids or salts thereof having the general formula: [Rf—O-L-COO−]iXi+ (I) wherein L represents a linear partially or fully fluorinated alkylene group or an aliphatic hydrocarbon group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one or more oxygen atoms, Xi+ represents a cation having the valence i and i is 1, 2 or 3; Then adding one or more non-fluorinated surfactants selected from anionic and non-ionic surfactants followed by reducing the total amount of the one or more fluorinated surfactants to an amount of not more than 500 ppm, for example not more than 250 ppm based on the total weight of the dispersion while maintaining or increasing the amount of solids in the dispersion.
摘要翻译：首先提供含氟聚合物颗粒和一种或多种选自氟化羧酸或其盐的含氟表面活性剂的含氟聚合物分散体的制备氟聚合物分散体的方法，所述氟化聚合物分散体具有以下通式：<？in-line-formula description =“In-Line Formulas” （I）结束=“引导”→[R f> OL O> - ））））））））））））））））））））））））） <？in-line-formula description =“In-line formula”end =“tail”？>其中L表示线性部分或完全氟化的亚烷基或脂族烃基，R f表示线性部分或全氟化的脂族基团或被一个或多个氧原子间隔的线性部分或完全氟化的脂肪族基团，表示i为i且i为1,2或3的阳离子; 然后加入一种或多种选自阴离子和非离子表面活性剂的非氟化表面活性剂，然后将一种或多种氟化表面活性剂的总量减少至不超过500ppm，例如不超过250ppm，基于分散体的总重量，同时保持或增加分散体中固体的量。

9. 发明申请

US20060128872A1 Aqueous Dispersions of Polytetrafluoroethylene Having a Low Amount of Fluorinated Surfactant 有权
标题翻译：具有少量氟化表面活性剂的聚四氟乙烯的水性分散体
公开(公告)号：US20060128872A1
公开(公告)日：2006-06-15
申请号：US11275959
申请日：2006-02-07
申请人： Tilman Zipplies , Klaus Hintzer , Michael Dadalas , Gernot Loehr
发明人： Tilman Zipplies , Klaus Hintzer , Michael Dadalas , Gernot Loehr
IPC分类号： C08G18/62
CPC分类号： C09D127/18 , C08F6/16 , C08F214/26 , C08L27/18 , C08L71/02 , C08L2666/02 , C08L2666/22
摘要： An aqueous non-melt processible polytetrafluoroethylene dispersion having non-melt processible polytetrafluoroethylene particles in an amount of 30 to 70% by weight and an amount of non-ionic surfactant between 2 and 15% by weight based on the weight of polytetrafluoroethylene solids. The dispersion is free of fluorinated surfactant or contains fluorinated surfactant in amounts of not more than 200 ppm based on the amount of polytetrafluoroethylene solids. At least part of the non-melt processible polytetrafluoroethylene particles comprise an effective amount of ionic end groups in the polytetrafluoroethylene polymer chains.
摘要翻译：一种水溶性可熔融加工的聚四氟乙烯分散体，其具有30至70重量％的非熔体加工的聚四氟乙烯颗粒和基于聚四氟乙烯固体重量的2至15重量％的非离子表面活性剂的量。该分散体不含氟化表面活性剂，或含有基于聚四氟乙烯固体量不大于200ppm的含氟表面活性剂。至少部分不可熔融加工的聚四氟乙烯颗粒在聚四氟乙烯聚合物链中包含有效量的离子端基。

10. 发明申请

US20060003168A1 Primer coating of PTFE for metal substrates 有权
标题翻译：用于金属基材的PTFE底漆涂层
公开(公告)号：US20060003168A1
公开(公告)日：2006-01-05
申请号：US11172345
申请日：2005-06-30
申请人： Michael Dadalas , Klaus Hintzer , Gernot Loehr , Tilman Zipplies
发明人： Michael Dadalas , Klaus Hintzer , Gernot Loehr , Tilman Zipplies
IPC分类号： B32B27/00
CPC分类号： C09D179/08 , C08L27/08 , C09D5/002 , C09D177/00 , C09D179/04 , C09D181/06 , Y10T428/3154 , C08L2666/14 , C08L2666/04
摘要： The present invention provides an aqueous coating composition comprising (i) particles of a non-melt processible polymer of tetrafluoroethylene and (ii) a non-fluorinated polymer selected from the group consisting of a polysulfone, a polyamide, a polyimide, a polyamide-imide, a polybismaleimide and mixtures thereof, wherein said particles are core-shell particles whereby the shell comprises a copolymer of tetrafluoroethylene and a partially fluorinated or non-fluorinated comonomer. The aqueous coating composition may be used for providing a primer coating on a substrate such as a metal or glass substrate. Such primer coating may provide good or excellent non-stick coatings combined with good or excellent scratch and wear resistance of the coating. Also, such primer coating may provide for good to excellent PTFE coatings that can resist hot salt water. The aqueous coating composition may also be used to provide other coating layers of a multi-layer coating.
摘要翻译：本发明提供一种水性涂料组合物，其包含（i）四氟乙烯的不可熔融加成聚合物的颗粒和（ii）选自聚砜，聚酰胺，聚酰亚胺，聚酰胺 - 酰亚胺的非氟化聚合物，多双马来酰亚胺及其混合物，其中所述颗粒是核 - 壳颗粒，其中壳包含四氟乙烯和部分氟化或非氟化共聚单体的共聚物。水性涂料组合物可以用于在诸如金属或玻璃基材的基材上提供底漆涂层。这种底漆涂层可以提供良好或优异的不粘涂层，同时具有涂层的良好或优异的耐擦伤性和耐磨性。此外，这种底漆涂层可以提供可耐受热盐水的良好至优异的PTFE涂层。水性涂料组合物也可用于提供多层涂层的其它涂层。

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