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1. 发明申请

US20100029967A1 Diphosphine ligands 审中-公开
标题翻译：二膦配体
公开(公告)号：US20100029967A1
公开(公告)日：2010-02-04
申请号：US12308941
申请日：2007-06-29
申请人： Benoit Pugin , Xiangdong Feng , Felix Spindler
发明人： Benoit Pugin , Xiangdong Feng , Felix Spindler
IPC分类号： C07F15/00
CPC分类号： C07F17/00 , B01J31/2295 , B01J31/2409 , B01J31/2428 , B01J2231/643 , B01J2231/645 , B01J2531/16 , B01J2531/17 , B01J2531/18 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/825 , B01J2531/827 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07B53/00 , C07F17/02
摘要： Compounds of the formulae I and Ia in the form of mixtures of diastereomers or pure diastereomers, (I), (Ia), where R1 is a hydrogen atom or C1-C4-alkyl and R′1 is C1-C4-alkyl; X1 and X2 are each, independently of one another, a sec-phosphino group; T is C6-C20-arylene or C4-C18-heteroarylene having heteroatoms selected from the group consisting of O, S, —N═ and N(C1-C4-alkyl); v is 0 or an integer from 1 to 4; X1 is bound in the ortho position relative to the T-C* bond; Q is vinyl, methyl, ethyl, —CH2—OR, —CH2—N(C1-C4-alkyl)2 or a C- or S-bonded chiral group which directs metals of metallation reagents into the ortho position; R is hydrogen, a silyl radical or an aliphatic, cycloaliphatic, aromatic or aromatic-aliphatic hydrocarbon radical which has from 1 to 18 carbon atoms and is unsubstituted or substituted by C1-C4-alkyl, C1-C4-alkoxy, F or CF3; are ligands for metal complexes as homogeneous catalyst in asymmetric syntheses.
摘要翻译：式（I），（Ia），其中R 1是氢原子或C 1 -C 4 - 烷基和R 11是C 1 -C 4 - 烷基的非对映异构体或纯非对映体混合物形式的式I和Ia化合物; X1和X2各自独立地为仲膦基; T是具有选自O，S，-N-和N（C 1 -C 4 - 烷基）的杂原子的C 6 -C 20亚芳基或C 4 -C 18亚杂芳基; v为0或1至4的整数; X1相对于T-C *键的邻位结合; Q是乙烯基，甲基，乙基，-CH 2 -OR，-CH 2 -N（C 1 -C 4烷基）2或C-或S-键合的手性基团，其将金属化试剂的金属引导到邻位; R是氢，具有1至18个碳原子且未被取代或被C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，F或CF 3取代的甲硅烷基或脂族，脂环族，芳族或芳族 - 脂族烃基; 是不对称合成中金属络合物作为均相催化剂的配体。

2. 发明申请

US20090156851A1 Ferrocene-Diphosphine Ligands 审中-公开
标题翻译：二茂铁 - 二膦配体
公开(公告)号：US20090156851A1
公开(公告)日：2009-06-18
申请号：US11990208
申请日：2006-08-10
申请人： Walter Weissensteiner , Yaping Wang , Felix Spindler , Benoit Pugin , Xiangdong Feng
发明人： Walter Weissensteiner , Yaping Wang , Felix Spindler , Benoit Pugin , Xiangdong Feng
IPC分类号： C07F9/02 , C07F15/02
CPC分类号： C07F17/02
摘要： Compounds of the formula (I) in the form of racemates, mixtures of stereoisomers or optically pure stereoisomers, formula (I), where X1 and X2 are each, independently of one another, a secondary phosphino group; R1 is a halogen atom or a—substituent bound via a C atom, N atom, S atom, Si atom, a P(O) group or a P(S) group to the cyclopentadienyl ring; R2 is C1-C4-alkyl or phenyl; m is from 1 to 3 and n is 0 or from 1 to 5, are ligands for complexes of transition metals as enantioselective and homogeneous catalysts. As a result of the substitution, the conversion, the stereoselectivity and/or the configuration of the adduct formed can be influenced and optimization of catalysts can be made possible in this way.
摘要翻译：式（I）化合物为外消旋体形式，立体异构体混合物或光学纯立体异构体式（I），其中X1和X2各自独立地为次膦基; R1是通过C原子，N原子，S原子，Si原子，P（O）基团或P（S）键连接到环戊二烯基环上的卤素原子或取代基; R2是C1-C4烷基或苯基; m为1至3，n为0或1至5为过渡金属络合物作为对映选择性和均相催化剂的配体。作为取代的结果，可以影响形成的加合物的转化率，立体选择性和/或构型，并且可以以这种方式使催化剂的优化成为可能。

3. 发明申请

US20090171114A1 Chiral Ligands Used in Transition Metal Catysts for Asymmetric Addition Reactions Especially Hydrogenation 有权
标题翻译：用于非对称加成反应的过渡金属催化剂中的手性配体特别是氢化
公开(公告)号：US20090171114A1
公开(公告)日：2009-07-02
申请号：US12227574
申请日：2007-05-23
申请人： Andreas Pfaltz , Yann Ribourdouille , Xiangdong Feng , Balamurugan Ramalingam , Benoit Pugin , Felix Spindler
发明人： Andreas Pfaltz , Yann Ribourdouille , Xiangdong Feng , Balamurugan Ramalingam , Benoit Pugin , Felix Spindler
IPC分类号： C07C69/34 , C07F15/02 , C07F9/53 , B01J31/18
CPC分类号： C07F9/5022 , B01J31/1875 , B01J31/2495 , B01J2231/643 , B01J2231/645 , B01J2531/821 , B01J2531/822 , B01J2531/827 , C07B2200/07 , C07C51/36 , C07C67/303 , C07C213/02 , C07C231/12 , C07F15/008 , C07F17/02 , C07C57/30 , C07C69/675 , C07C69/732 , C07C69/34 , C07C217/08 , C07C233/47
摘要： Ligands of the formula (I) secondary phosphine-Q-P(═O)HR1 (I) in the form of mixtures of diastereomers or pure diastereomers, in which secondary phosphine is a secondary phosphine group with hydrocarbon radicals or heterohydrocarbon radicals as substituents; Q is a bivalent bisaryl or bisheteroaryl radical with an axial chiral centre to which the two phosphorus atoms are bonded in the ortho positions to the bisaryl or bisheteroaryl bridge bond, or Q is a bivalent ferrocenyl radical with a planar chiral centre or without a planar chiral centre, to which the phosphorus atom of the secondary phosphine is bonded directly or via a C1-C4-carbon chain to a cyclopentadienyl ring, the —P*(═O)HR1 group is bonded either on the same cyclopentadienyl ring in ortho position to the bonded secondary phosphine or on the other cyclopentadienyl ring; P* is a chiral phosphorus atom, and R1 is a hydrocarbon radical, a heterohydrocarbon radical or a ferrocenyl radical, where R1 is a ferrocenyl radical with a planar chiral centre when Q is a ferrocenyl radical without a planar chiral centre. Metal complexes of these ligands are homogeneous catalysts for asymmetric addition reactions, particularly hydrogenations.
摘要翻译：式（I）以非对映异构体或纯非对映异构体混合物形式的仲膦-Q-P（-O）HR1（I）的配体，其中次膦是具有烃基或杂烃基作为取代基的仲膦基; Q是具有轴向手性中心的二价双芳基或双杂芳基，其中两个磷原子与双芳基或双杂芳基桥键的邻位键合，或Q是具有平面手性中心或不具有平面手性的二价二茂铁基中心，仲膦的磷原子直接或通过C1-C4-碳键连接到环戊二烯基环上，-P *（ - O）HR 1基团在邻位相邻的环戊二烯基环上键合到键合的次膦或在另一个环戊二烯基环上; P *是手性磷原子，R1是烃基，杂烃基或二茂铁基，其中当Q是没有平面手性中心的二茂铁基时，R 1是具有平面手性中心的二茂铁基。这些配体的金属络合物是用于不对称加成反应的均相催化剂，特别是氢化。

4. 发明申请

US20090082581A1 Ferrocenyl ligands, production and use thereof 审中-公开
标题翻译：二茂铁基配体，其生产和使用
公开(公告)号：US20090082581A1
公开(公告)日：2009-03-26
申请号：US11919762
申请日：2006-05-02
申请人： Benoit Pugin , Xiangdong Feng
发明人： Benoit Pugin , Xiangdong Feng
IPC分类号： C07F17/02
CPC分类号： C07F17/02
摘要： The invention relates to the compounds of formula (I) in the form of enantiomer-pure diastereomers or a mixture of diastereomers, wherein R′1 represents C1-C4 alkyl, C6-C10 aryl, C7-C10 alkyl or C7-C12 alkaralkyl and n is 0 or an integer of from 1 to 5; R1 represents a hydrogen atom, halogen, a hydrocarbon group with 1 to 20 C atoms that is either unsubstituted or substituted with —SC1-C4 alkyl, —OC1-C4 alkyl, —OC6-C10 aryl or —Si(C1C4 alkyl)3, or a silyl group with 3 C1-C12 hydrocarbon groups; Y represents vinyl, methyl, ethyl, —CH2—OR, —CH2—N(C1-C4 alkyl)2, a C-bound chiral group that directs metals of metallation reagents to the ortho position X1, or Y is a group —CHR2—OR′2; R2 represents C1-C8 alkyl, C5-C8 cycloalkyl, C6-C10 aryl, C7-C12 aralkyl or C7-C12 alkaralkyl; R′2 represents hydrogen or C1-C18 acyl; X1 and X2 independently represent a P-bound P(III) substituent, —SH or an S-bound group of mercaptan; and R represents hydrogen, a silyl group or an aliphatic, cycloaliphatic, aromatic or aromatic-aliphatic hydrocarbon group with 1 to 18 C atoms which is unsubstituted or substituted with C1-C4 alkyl, C1-C4 alkoxy, F or CF3. The inventive compounds are ligands for metal complexes of transition metals such as Ru, Rh or Ir which are catalysts for especially the enantioselective hydration of prochiral unsaturated compounds. Use of these compounds allows to achieve high catalyst activities and an excellent stereoselectivity.
摘要翻译：本发明涉及对映异构体纯的非对映异构体形式的式（I）化合物或非对映异构体的混合物，其中R'1代表C1-C4烷基，C6-C10芳基，C7-C10烷基或C7-C12烷基烷基， n为0或1〜5的整数， R 1表示氢原子，卤素，未取代或被-SC 1 -C 4烷基，-OC 1 -C 4烷基，-OC 6 -C 10芳基或-Si（C 1 -C 4烷基）3取代的具有1至20个碳原子的烃基，或具有3个C 1 -C 12烃基的甲硅烷基; Y表示乙烯基，甲基，乙基，-CH 2 -OR，-CH 2 -N（C 1 -C 4烷基）2，将金属化试剂的金属引导至邻位X1的C-键手性基团，或Y为基团-CHR2 -OR'2; R2代表C1-C8烷基，C5-C8环烷基，C6-C10芳基，C7-C12芳烷基或C7-C12烷基烷基; R'2表示氢或C 1 -C 18酰基; X 1和X 2独立地表示P键的P（III）取代基-SH或S结合的硫醇基团; 并且R表示氢，具有未取代的或被C 1 -C 4烷基，C 1 -C 4烷氧基，F或CF 3取代的具有1至18个C原子的脂族，脂环族，芳族或芳族 - 脂族烃基的甲硅烷基或脂族，脂环族，芳族或芳族 - 脂族烃基。本发明化合物是过渡金属如Ru，Rh或Ir的金属络合物的配体，其是用于特别是前手性不饱和化合物的对映选择性水合的催化剂。使用这些化合物可以实现高催化剂活性和优异的立体选择性。

5. 发明授权

US08008529B2 Chiral ligands used in transition metal catalysts for asymmetric addition reactions especially hydrogenation 有权
标题翻译：用于非对称加成反应的过渡金属催化剂中的手性配体，特别是氢化
公开(公告)号：US08008529B2
公开(公告)日：2011-08-30
申请号：US12227574
申请日：2007-05-23
申请人： Andreas Pfaltz , Yann Ribourdouille , Xiangdong Feng , Balamurugan Ramalingam , Benoît Pugin , Felix Spindler
发明人： Andreas Pfaltz , Yann Ribourdouille , Xiangdong Feng , Balamurugan Ramalingam , Benoît Pugin , Felix Spindler
IPC分类号： C07F15/02 , C07F9/53 , C07C69/34 , B01J31/18
CPC分类号： C07F9/5022 , B01J31/1875 , B01J31/2495 , B01J2231/643 , B01J2231/645 , B01J2531/821 , B01J2531/822 , B01J2531/827 , C07B2200/07 , C07C51/36 , C07C67/303 , C07C213/02 , C07C231/12 , C07F15/008 , C07F17/02 , C07C57/30 , C07C69/675 , C07C69/732 , C07C69/34 , C07C217/08 , C07C233/47
摘要： Ligands of the formula (I) secondary phosphine-Q-P(═O)HR1 (I) in the form of mixtures of diastereomers or pure diastereomers, in which secondary phosphine is a secondary phosphine group with hydrocarbon radicals or heterohydrocarbon radicals as substituents; Q is a bivalent bisaryl or bisheteroaryl radical with an axial chiral centre to which the two phosphorus atoms are bonded in the ortho positions to the bisaryl or bisheteroaryl bridge bond, or Q is a bivalent ferrocenyl radical with a planar chiral centre or without a planar chiral centre, to which the phosphorus atom of the secondary phosphine is bonded directly or via a C1-C4-carbon chain to a cyclopentadienyl ring, the —P*(═O)HR1 group is bonded either on the same cyclopentadienyl ring in ortho position to the bonded secondary phosphine or on the other cyclopentadienyl ring; P* is a chiral phosphorus atom, and R1 is a hydrocarbon radical, a heterohydrocarbon radical or a ferrocenyl radical, where R1 is a ferrocenyl radical with a planar chiral centre when Q is a ferrocenyl radical without a planar chiral centre. Metal complexes of these ligands are homogeneous catalysts for asymmetric addition reactions, particularly hydrogenations.
摘要翻译：式（I）以非对映异构体或纯非对映异构体混合物形式的仲膦-Q-P（= O）HR1（I）的配体，其中次膦是具有烃基或杂烃基作为取代基的次膦基; Q是具有轴向手性中心的二价双芳基或双杂芳基，其中两个磷原子与双芳基或双杂芳基桥键的邻位键合，或Q是具有平面手性中心或不具有平面手性的二价二茂铁基中心，仲膦的磷原子直接或通过C1-C4-碳键连接到环戊二烯基环上，-P *（= O）HR 1基团在邻位上的相同的环戊二烯基环上键合到键合的次膦或在另一个环戊二烯基环上; P *是手性磷原子，R1是烃基，杂烃基或二茂铁基，其中当Q是没有平面手性中心的二茂铁基时，R 1是具有平面手性中心的二茂铁基。这些配体的金属络合物是用于不对称加成反应的均相催化剂，特别是氢化。

6. 发明授权

US08147610B2 Cementitious formulations and products 有权
标题翻译：水泥配方及产品
公开(公告)号：US08147610B2
公开(公告)日：2012-04-03
申请号：US12244753
申请日：2008-10-02
申请人： Xiangdong Feng , Meiling Gong , Chinmay Avinash Gowardhan , Chongjun Jiang , Michael John Julius , Amitabha Kumar , Shannon Marie Labernik , Xiangyuan Liu , Liyan Ma , Basil Taha Naji , Kalynne Hitzeman Paradis , David John Sharman
发明人： Xiangdong Feng , Meiling Gong , Chinmay Avinash Gowardhan , Chongjun Jiang , Michael John Julius , Amitabha Kumar , Shannon Marie Labernik , Xiangyuan Liu , Liyan Ma , Basil Taha Naji , Kalynne Hitzeman Paradis , David John Sharman
IPC分类号： C04B14/00 , C04B16/00 , C04B24/00 , C04B28/10 , C04B7/00 , C04B7/34 , C04B28/00 , C04B32/00 , C04B18/06 , C04B2/00
CPC分类号： C04B28/02 , C04B14/06 , C04B14/10 , C04B20/0076 , C04B22/124 , C04B40/024 , C04B2103/50 , C04B22/10 , C04B22/06 , C04B12/04
摘要： Cementitious formulations and their products with enhanced reactivity are provided. Formulations in certain embodiments may include at least one calcium source, a reactant and a filler in a hydrated environment, wherein the reactant, in one form, is crystalline silica that has been modified for reactivity. Enhancement of a reactant may include one or more modifications to its content, grind and/or the cement to silica ratio, as well as addition of one or more additives in the formulation, additives in the form of at least one alumina source, defoamer, catalyst and/or a clay.
摘要翻译：提供了具有增强反应性的水泥配方及其产品。在某些实施方案中的制剂可以包括在水合环境中的至少一种钙源，反应物和填料，其中一种形式的反应物是已被修饰用于反应性的结晶二氧化硅。反应物的增强可以包括对其含量，研磨和/或水泥 - 二氧化硅比例的一种或多种修饰，以及在制剂中添加一种或多种添加剂，至少一种氧化铝源，消泡剂，催化剂和/或粘土。

7. 发明授权

US07687401B2 Substantially spherical composite ceria/titania particles 失效
标题翻译：基本球形复合二氧化铈/二氧化钛颗粒
公开(公告)号：US07687401B2
公开(公告)日：2010-03-30
申请号：US11380980
申请日：2006-05-01
申请人： Xiangdong Feng , Yie-Shein Her , Anthony C. Sutorik , M. Sharon Paras
发明人： Xiangdong Feng , Yie-Shein Her , Anthony C. Sutorik , M. Sharon Paras
IPC分类号： H01L21/302
CPC分类号： C09G1/02 , B82Y30/00 , C01G23/00 , C01G23/003 , C01P2002/76 , C01P2004/03 , C01P2004/04 , C01P2004/32 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C04B35/6264 , C04B35/6267 , C04B35/62695 , C04B35/62821 , C04B35/6325 , C04B2235/3229 , C04B2235/3232 , C04B2235/441 , C04B2235/449 , C04B2235/528 , C04B2235/5445 , C04B2235/5454 , C09K3/1436 , C09K3/1463 , H01L21/31053
摘要： The present invention provides substantially spherical composite ceria/titania particles, a method of forming the same, and chemical mechanical polishing compositions comprising such particles. The substantially spherical particles include a substantially crystalline core portion including one or more crystallites having a cubic lattice structure including Ce(1-x)Ti(x)O2, where x is
摘要翻译：本发明提供了基本上球形的复合二氧化铈/二氧化钛颗粒，其形成方法和包含这种颗粒的化学机械抛光组合物。基本上为球形的颗粒包括基本上结晶的芯部分，其包括一个或多个具有立方晶格结构的晶体，其包括Ce（1-x）Ti（x）O 2，其中x <0.25，以及覆盖至少一部分基本上为晶体的核心部分，基本上无定形的包层包括Ti（1-y）Ce（y）O 2，其中y为＆lt; n 1; 0.50。形成颗粒的方法包括在燃烧支持气体中燃烧包括羧酸铈盐和钛（IV）螯合物的有机溶剂，并收集包含两个或更多个基本上为球形的颗粒的附聚物。聚集体可用作化学机械抛光组合物中的研磨材料，以在制造集成电路器件期间去除膜层。

8. 发明申请

US20070254484A1 SUBSTANTIALLY SPHERICAL COMPOSITE CERIA/TITANIA PARTICLES 失效
标题翻译：特种球形复合陶瓷/钛酸钡颗粒
公开(公告)号：US20070254484A1
公开(公告)日：2007-11-01
申请号：US11380980
申请日：2006-05-01
申请人： Xiangdong Feng , Yie-Shein Her , Anthony Sutorik , M. Paras
发明人： Xiangdong Feng , Yie-Shein Her , Anthony Sutorik , M. Paras
IPC分类号： H01L21/461
CPC分类号： C09G1/02 , B82Y30/00 , C01G23/00 , C01G23/003 , C01P2002/76 , C01P2004/03 , C01P2004/04 , C01P2004/32 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C04B35/6264 , C04B35/6267 , C04B35/62695 , C04B35/62821 , C04B35/6325 , C04B2235/3229 , C04B2235/3232 , C04B2235/441 , C04B2235/449 , C04B2235/528 , C04B2235/5445 , C04B2235/5454 , C09K3/1436 , C09K3/1463 , H01L21/31053
摘要： The present invention provides substantially spherical composite ceria/titania particles, a method of forming the same, and chemical mechanical polishing compositions comprising such particles. The substantially spherical particles include a substantially crystalline core portion including one or more crystallites having a cubic lattice structure including Ce(1-x)Ti(x)O2, where x is
摘要翻译：本发明提供了基本上球形的复合二氧化铈/二氧化钛颗粒，其形成方法和包含这种颗粒的化学机械抛光组合物。基本上球形的颗粒包括基本上结晶的芯部分，其包括一个或多个具有包括Ce（1-x）Ti（x）O 2 其中x为<0.25，以及覆盖基本上结晶的芯部分的至少一部分的基本无定形的包层，所述基本上无定形的包层包括Ti（1-y）（y）O 2，其中y是<= 0.50。形成颗粒的方法包括在燃烧支持气体中燃烧包括羧酸铈盐和钛（IV）螯合物的有机溶剂，并收集包含两个或更多个基本上为球形的颗粒的附聚物。聚集体可用作化学机械抛光组合物中的研磨材料，以在制造集成电路器件期间去除膜层。

9. 发明申请

US20060112649A1 Hydrothermal synthesis of cerium-titanium oxide for use in CMP 有权
标题翻译：用于CMP的铈钛氧化物的水热合成
公开(公告)号：US20060112649A1
公开(公告)日：2006-06-01
申请号：US11283530
申请日：2005-11-18
申请人： Xiangdong Feng , Yie-Shein Her , Yi Yang
发明人： Xiangdong Feng , Yie-Shein Her , Yi Yang
IPC分类号： C09K3/14
CPC分类号： C03C19/00 , C09G1/02 , C09K3/1436 , C09K3/1463 , H01L21/31053 , H01L21/3212
摘要： The present invention provides a method of synthesizing abrasive particles and methods of using the same in chemical mechanical polishing slurry applications. The nanosized abrasive particles according to the invention are produced by hydrothermal synthesis using an insoluble source of cerium. The crystallites of the particles include cerium ions and titanium ions.
摘要翻译：本发明提供了一种合成磨粒的方法及其在化学机械抛光浆中的应用。根据本发明的纳米尺寸的磨料颗粒是通过使用不溶的铈源的水热合成制备的。颗粒的微晶包括铈离子和钛离子。

10. 发明申请

US20060032836A1 METHODS OF CONTROLLING THE PROPERTIES OF ABRASIVE PARTICLES FOR USE IN CHEMICAL-MECHANICAL POLISHING SLURRIES 审中-公开
标题翻译：控制用于化学机械抛光液的磨粒的性质的方法
公开(公告)号：US20060032836A1
公开(公告)日：2006-02-16
申请号：US11162337
申请日：2005-09-07
申请人： Xiangdong Feng , Yie-Shein Her
发明人： Xiangdong Feng , Yie-Shein Her
IPC分类号： C03C15/00 , B44C1/22
CPC分类号： C03C19/00 , B82Y30/00 , C01F17/0043 , C01G23/04 , C01G23/053 , C01P2002/60 , C01P2002/76 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/90 , C09C1/3653 , C09G1/02 , C09K3/1409 , C09K3/1436 , C09K3/1463 , H01L21/31053 , H01L21/3212
摘要： The present invention provides methods of controlling the properties of abrasive particles produced via hydrothermal synthesis for use in chemical-mechanical polishing slurries. In accordance with the methods of the invention, variables such as cerium salt concentration, dopant solution concentration, hydrothermal medium pH, hydrothermal temperature and processing duration are controlled to produce particles having the desired properties and shapes. The abrasive particles formed in accordance with the method of the invention can be used to produce CMP slurries that provide substantial improvements in the polishing of STI structures and a reduction in defects.
摘要翻译：本发明提供控制用于化学机械抛光浆料的水热合成制备的磨料颗粒的性质的方法。根据本发明的方法，控制诸如铈盐浓度，掺杂剂溶液浓度，水热介质pH，水热温度和加工时间等变量以产生具有所需性质和形状的颗粒。根据本发明的方法形成的磨料颗粒可用于生产CMP浆料，其提供STI结构的抛光和减少缺陷的实质性改进。

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