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1. 发明专利

JP2011138782A Forming method of proton conductive polymer membrane 审中-公开
标题翻译：原子导电聚合物膜的形成方法
公开(公告)号：JP2011138782A
公开(公告)日：2011-07-14
申请号：JP2011009959
申请日：2011-01-20
申请人： Basf Fuel Cell Gmbh , ビーエーエスエフフューエルセルゲゼルシャフトミットベシュレンクテルハフツング
发明人： KIEFER JOACHIM , UENSAL OEMER , CALUNDANN GORDON , CRIVELLO JAMES
IPC分类号： C08F2/44 , H01B13/00 , C08F228/02 , C08F230/02 , C08F291/00 , C08J5/22 , C08J7/18 , H01B1/06 , H01M8/02 , H01M8/04 , H01M8/10
CPC分类号： H01M8/1023 , C08J5/2231 , C08J2325/08 , H01M8/04197 , H01M8/1011 , H01M8/1025 , H01M8/1039 , H01M8/1044 , H01M8/106 , H01M8/1072 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a proton conductive electrolyte membrane with an intrinsic conductivity at 160°C of 0.001 S/cm or higher. SOLUTION: This forming method of the proton conductive electrolyte membrane of an intrinsic conductivity at 160°C of 0.001S/cm comprises a step (A) of dipping a polymer film in liquid containing a vinyl-content sulfonic acid and a vinyl-content phosphonic acid and impregnating the liquid in the film to be swollen, and a step (B) of polymerizing the vinyl-content sulfonic acid and the vinyl-content phosphonic acid existing in the film. However, the film for swelling is formed of polyazole, the liquid for swelling contains the vinyl-content phosphonic acid by 20 mass% or larger, a mass ratio of the vinyl-content phosphonic acid to the vinyl-content sulfonic acid in the liquid for swelling is 1:1 or larger, and the film after swelling contains the vinyl-content sulfonic acid by 10 mass%. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供在160℃下的固有电导率为0.001S / cm或更高的质子传导电解质膜。解决方案：160℃下固有电导率为0.001S / cm的质子传导电解质膜的形成方法包括将聚合物膜浸渍在含有乙烯基含量磺酸和乙烯基的液体的液体中的步骤（A） - 含有膦酸并浸渍在待溶胀的膜中的液体;以及聚合存在于膜中的乙烯基含量磺酸和乙烯基含量膦酸的步骤（B）。然而，用于溶胀的膜由聚唑形成，溶胀液含有乙烯基含量膦酸20质量％以上，乙烯基含量膦酸与乙烯基含量磺酸在液体中的质量比溶胀为1：1以上，溶胀后的膜含有10质量％的乙烯基含量的磺酸。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2011006690A Proton conductive polymer membrane 有权
标题翻译：原子导电聚合物膜
公开(公告)号：JP2011006690A
公开(公告)日：2011-01-13
申请号：JP2010177244
申请日：2010-08-06
申请人： Basf Fuel Cell Gmbh , ベーアーエスエフフューエルセルゲーエムベーハー
发明人： CALUNDANN GORDON , SANSONE MICHAEL J , UENSAL OEMER , KIEFER JOACHIM
IPC分类号： C08J5/22 , C08G73/08 , H01M8/02 , H01M8/10
CPC分类号： Y02E60/521
摘要： PROBLEM TO BE SOLVED: To provide a new polyazole-based proton conductive polymer membrane.SOLUTION: The polyazole-based proton conductive polymer membrane has superior chemical and thermal properties and, therefore, is useful, in particular, as a polymer electrolyte membrane (PEM) for producing a membrane-electrode unit for a PEM fuel cell.
摘要翻译：要解决的问题：提供一种新型的基于聚唑的质子传导性聚合物膜。解决方案：聚唑类质子传导性聚合物膜具有优异的化学和热性能，因此特别适用于聚合物电解质膜（PEM ），用于制造用于PEM燃料电池的膜电极单元。

3. 发明专利

JP2009293045A Proton-conducting polymer membrane comprising polymer with sulfonic acid group and use thereof in fuel cells 审中-公开
标题翻译：含有磺酸基的聚合物的导电聚合物膜和在燃料电池中的使用
公开(公告)号：JP2009293045A
公开(公告)日：2009-12-17
申请号：JP2009217782
申请日：2009-09-18
申请人： Basf Fuel Cell Gmbh , バスフ・ヒュエル・セル・ゲーエムベーハー
发明人： KIEFER JOACHIM , UENSAL OEMER , CALUNDANN GORDON
IPC分类号： C08G73/06 , C08J5/22 , B01D67/00 , B01D69/14 , B01D71/62 , B01D71/72 , C08F2/44 , C08F28/02 , C08F283/04 , C08G61/12 , C08G73/08 , C08G73/18 , C08G79/04 , H01B1/06 , H01B13/00 , H01M8/02 , H01M8/10
CPC分类号： B01D67/0006 , B01D69/141 , B01D71/62 , B01D71/72 , B01D2323/34 , B01D2325/24 , B01D2325/26 , C08G61/124 , C08G73/06 , C08G73/0616 , C08G73/0633 , C08G73/18 , C08G79/04 , C08J5/2256 , C08J2379/06 , H01M8/1004 , H01M8/1023 , H01M8/1027 , H01M8/103 , H01M8/1044 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a proton-conducting polymer membrane suitable for polymer electrolyte membranes and the like. SOLUTION: The proton-conducting polymer membrane comprises polymers containing sulfonic acid groups and has the conductivity of at least 0.001 S/cm. The membrane is obtainable by a method comprising the steps of: (A) mixing a vinyl-containing sulfonic acid with one or more aromatic polycarboxylic acids, their esters, their acid halides, and their acid anhydrides, and one or more of aromatic tetra-amino compounds, or mixing the vinyl-containing sulfonic acid with one or more aromatic and/or heteroaromatic diaminocarboxylic acids, their esters, their acid halides, or their acid anhydrides; (B) heating the mixture obtainable according to step (A) under inert gas to temperatures of up to 350°C, to form polyazole polymers; (C) applying a layer to a support, using the mixture according to step (A) and/or (B); and (D) polymerizing the vinyl-containing sulfonic acid present in the sheetlike structure obtainable according to step (C). COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供适用于聚合物电解质膜等的质子传导聚合物膜。解决方案：质子传导性聚合物膜包含含有磺酸基的聚合物，其导电率至少为0.001S / cm。膜可以通过包括以下步骤的方法获得：（A）将含乙烯基的磺酸与一种或多种芳族多元羧酸，它们的酯，它们的酰卤和它们的酸酐混合，以及一种或多种芳族四或将含乙烯基的磺酸与一种或多种芳族和/或杂芳族二氨基羧酸，它们的酯，其酰基卤或其酸酐混合; （B）在惰性气体下将根据步骤（A）获得的混合物加热至高达350℃的温度，以形成聚唑聚合物; （C）使用根据步骤（A）和/或（B）的混合物将层施加到载体上; 和（D）使根据步骤（C）获得的片状结构中存在的含乙烯基磺酸聚合。版权所有（C）2010，JPO＆INPIT

4. 发明专利

JP2011089123A Proton-conducting polymer membrane containing polyazole blend, and application thereof in fuel cell 审中-公开
标题翻译：含有聚酰胺混合物的导电聚合物膜及其在燃料电池中的应用
公开(公告)号：JP2011089123A
公开(公告)日：2011-05-06
申请号：JP2010258846
申请日：2010-11-19
申请人： Basf Fuel Cell Gmbh , ベーアーエスエフフューエルセルゲーエムベーハー
发明人： UENSAL OEMER , KIEFER JOACHIM , CALUNDANN GORDON , SANSONE MICHAEL , BENICEWICZ BRIAN , CHOE EUI WON
IPC分类号： C08J5/22 , B01D71/62 , C08G73/18 , C08L79/04 , C08L101/00 , H01B1/06 , H01B13/00 , H01M4/86 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2275 , B01D71/62 , C08G73/18 , C08J2379/06 , H01M8/1023 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1034 , H01M8/1037 , H01M8/1039 , H01M8/1041 , H01M8/1048 , H01M8/1072 , H01M8/1081 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a new polymer electrolyte membrane which can be used for a variety of purposes owing to its excellent chemical and thermal properties. SOLUTION: The proton-conducting polymer membrane containing polyazole is obtained by a method comprising the following steps: (A) preparation of a mixture comprising polyphosphoric acid, at least one polyazole (polymer A) and/or one or more compounds which are suitable for forming polyazoles under the action of heat according to step (B); (B) heating of the mixture obtainable according to step (A) under inert gas to temperatures of up to 400°C; (C) application of a layer using the mixture from step (A) and/or (B) to a support; and (D) treatment of the membrane formed in step (C) until it is self-supporting (wherein at least one further polymer (polymer B) which is not a polyazole is added to the composition obtainable according to step (A) and/or step (B) and the weight ratio of polyazole to polymer B is in the range from 0.1 to 50). COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种由于其优异的化学和热性能而可用于各种目的的新的聚合物电解质膜。解决方案：含有聚唑的质子传导聚合物膜通过包括以下步骤的方法获得：（A）制备包含多磷酸，至少一种聚唑（聚合物A）和/或一种或多种化合物的混合物，适用于根据步骤（B）在热作用下形成多唑; （B）在惰性气体下将根据步骤（A）获得的混合物加热至高达400℃的温度; （C）使用来自步骤（A）和/或（B）的混合物将层施加到载体上; 和（D）处理在步骤（C）中形成的膜直到其自支撑（其中至少一种不是聚唑的另外的聚合物（聚合物B）加入到根据步骤（A）获得的组合物和/ 或步骤（B），并且聚唑与聚合物B的重量比在0.1至50的范围内）。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2011190445A Asymmetric polymer film, method for manufacturing the same, and use thereof 审中-公开
标题翻译：不对称聚合物膜，其制造方法及其用途
公开(公告)号：JP2011190445A
公开(公告)日：2011-09-29
申请号：JP2011064782
申请日：2011-03-23
申请人： Basf Fuel Cell Gmbh , ベーアーエスエフフューエルセルゲーエムベーハー
发明人： PETERSEN JOACHIM , BAURMEISTER JOCHEN , UENSAL OEMER , JORDT FRAUKE , KIEFER JOACHIM
IPC分类号： C08J5/18 , B01D67/00 , B01D69/00 , B01D69/14 , B01D71/62 , C08G61/12 , C08G73/06 , C08K3/00 , C08L79/04 , H01B1/06 , H01G9/02 , H01M8/02 , H01M8/10 , H05K1/03
CPC分类号： B01D71/62 , B01D67/0088 , B01D69/00 , B01D69/141 , C08G61/124 , C08G73/0633 , C08G73/0677 , C08G73/0694 , H01M8/103 , H01M8/1048 , H01M8/1067 , H01M8/1081 , H05K1/0346 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide such a polymer membrane on the basis of a polyazole which is obtained by a feasible process, as assumes a uniform acid-doping across the whole cross section of the membrane. SOLUTION: The asymmetric polymer film is based on a polyazole with a specific structure, and has a smooth surface and a rough surface, with the roughness of the smooth surface being less than 2 μm and that of the rough surface 3-10 μm, and preferably, is added additionally with a proton-conducting filler. The asymmetric, polyazole-based polymer film, resulting from the asymmetric structure, can undergo the doping rapidly and uniformly with an acid to thereby form a proton-conductive membrane, and, resulting from the excellent chemical, thermal and mechanical characteristics, is especially suitable for manufacturing a polymer electrolyte membrane (PEM) for use in so-called PEM fuel cells. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了在通过可行的方法获得的聚唑的基础上提供这样的聚合物膜，假定在膜的整个横截面上均匀的酸掺杂。解决方案：不对称聚合物膜基于具有特定结构的多唑，具有光滑的表面和粗糙的表面，光滑表面的粗糙度小于2μm，粗糙表面3-10的粗糙度并且优选地另外添加质子传导性填料。由不对称结构产生的不对称的聚唑基聚合物膜可以用酸快速且均匀地进行掺杂，从而形成质子传导膜，并且由于优异的化学，热和机械特性而特别适合用于制造用于所谓的PEM燃料电池的聚合物电解质膜（PEM）。版权所有（C）2011，JPO＆INPIT

6. 发明专利

JP2011080075A Proton-conducting polymer membrane comprising sulfonic acid group-containing polyazole, and use thereof in fuel cell 审中-公开
标题翻译：包含含硫酸基团的聚酰胺的导电聚合物膜及其在燃料电池中的应用
公开(公告)号：JP2011080075A
公开(公告)日：2011-04-21
申请号：JP2010259249
申请日：2010-11-19
申请人： Basf Fuel Cell Gmbh , ベーアーエスエフフューエルセルゲーエムベーハー
发明人： UENSAL OEMER , KIEFER JOACHIM , CALUNDANN GORDON , SANSONE MICHAEL , BENICEWICZ BRIAN , CHOE EUI WON
IPC分类号： C08J5/22 , B01D71/62 , B01D71/82 , C08G73/18 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2256 , B01D71/62 , B01D71/82 , C08G73/18 , H01M8/103 , H01M8/1067 , H01M8/1072 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide novel polymer electrolyte membranes. SOLUTION: Proton-conducting polymer membranes comprise sulfonic acid group-containing polyazoles and can be obtained by a method comprising the following steps of (A)-(D): (A) one or more aromatic and/or heteroaromatic tetra-amino compound/s is/are mixed with one or several aromatic and/or heteroaromatic carboxylic acid/s or the derivatives thereof, which contain at least two acid groups per carboxylic acid monomer, at least a part of the tetra-amino compounds and/or the carboxylic acids comprising at least one sulfonic acid group, or one or more aromatic and/or heteroaromatic diaminocarboxylic acid/s, at least a part of which contain sulfonic acid groups, is/are mixed in polyphosphoric acid so as to form a solution and/or dispersion; (B) the solution and/or dispersion obtained in step (A) is/are heated to temperatures of up to 350°C under inert gas so as to form polyazole polymers having benzimidazole units; (C) a layer is applied to a support using the mixture according to step (A) and/or (B); and (D) the membrane formed in step (C) is treated in the presence of moisture or water and/or water vapor at a temperature within a range of 0-150°C until the membrane is made self-supporting. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供新颖的聚合物电解质膜。导电聚合物膜包含含磺酸基的多唑类，并且可以通过包括以下步骤（A） - （D）的方法获得：（A）一种或多种芳族和/或杂芳族四 - 氨基化合物与一种或几种芳族和/或杂芳族羧酸或其衍生物混合，其每个羧酸单体含有至少两个酸基，至少一部分四氨基化合物和/ 或包含至少一个磺酸基团的羧酸或其至少一部分含有磺酸基团的一种或多种芳族和/或杂芳族二氨基羧酸在多磷酸中混合以形成溶液和/或分散体; （B）将步骤（A）中得到的溶液和/或分散体在惰性气体下加热至高达350℃，形成具有苯并咪唑单元的聚唑聚合物; （C）使用根据步骤（A）和/或（B）的混合物将层施加到载体上; 和（D）步骤（C）中形成的膜在0〜150℃的温度范围内，在水分或水和/或水蒸汽的存在下进行处理，直到膜自支撑为止。版权所有（C）2011，JPO＆INPIT

7. 发明专利

DE50211981D1 未知
公开(公告)号：DE50211981D1
公开(公告)日：2008-05-08
申请号：DE50211981
申请日：2002-08-10
申请人： BASF FUEL CELL GMBH
发明人： KIEFER JOACHIM , UENSAL OEMER
IPC分类号： C08J5/18 , C08J5/22 , B01D67/00 , B01D69/14 , B01D71/62 , B01D71/68 , C08L81/06 , C08L101/02 , H01B1/06 , H01M8/1023 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1044 , H01M8/1048 , H01M8/1072 , H01M8/1081
摘要： The present invention relates to a polymer blend membrane comprising a bridged polymer which is produced by a selected process. The membrane of the invention displays a significantly improved fracture toughness (elongation at break/stress) combined with virtually unchanged other properties. The membranes of the invention are suitable for producing membrane-electrode units for fuel cells.

8. 发明专利

ES2292993T3 MEMBRANA ELECTROLITICA CONDUCTORA DE PROTONES CON PERMEABILIDAD REDUCIDA DE METANOL Y SU APLICACION EN PILAS DE COMBUSTIBLE. 未知
公开(公告)号：ES2292993T3
公开(公告)日：2008-03-16
申请号：ES03743390
申请日：2003-03-04
申请人： BASF FUEL CELL GMBH
发明人： KIEFER JOACHIM , UENSAL OEMER , CALUNDANN GORDON , CRIVELLO JAMES
IPC分类号： C08F2/44 , C08J7/16 , C08F291/00 , C08J5/22 , H01B1/06 , H01M8/02 , H01M8/04 , H01M8/10
摘要： Membrana electrolítica conductora de protones que puede obtenerse mediante un procedimiento que comprende las etapas A) hinchar una lámina polimérica con un líquido que comprende ácido sulfónico que contiene vinilo y B) polimerizar el ácido sulfónico que contiene vinilo presente en el líquido incorporado en la etapa A).

9. 发明专利

CA2619258A1 METHOD FOR CONDITIONING MEMBRANE-ELECTRODE-UNITS FOR FUEL CELLS 未知
公开(公告)号：CA2619258A1
公开(公告)日：2007-03-15
申请号：CA2619258
申请日：2006-09-08
申请人： BASF FUEL CELL GMBH
发明人： KUNDLER ISABEL , KIEFER JOACHIM , UENSAL OEMER , PADBERG CHRISTOPH , SCHMIDT THOMAS , BAURMEISTER JOCHEN , WEBER MATHIAS , HOPPES GLEN , CALUNDANN GORDON
IPC分类号： H01M8/12 , C08J5/22 , C08K3/32 , C08L79/04
摘要： The invention relates to a method for conditioning membrane-electrode-units for fuel cells, wherein the power of the used membrane-electrode-units increases and also wherein the efficiency of the resulting polymer electrolyte membrane-fuels cells can be improved.

10. 发明专利

AT480874T 未知
公开(公告)号：AT480874T
公开(公告)日：2010-09-15
申请号：AT03718780
申请日：2003-04-22
申请人： BASF FUEL CELL GMBH
发明人： UENSAL OEMER , KIEFER JOACHIM
IPC分类号： H01B1/06 , H01M2/00 , H01M8/02 , H01M8/10
摘要： The present invention relates to a proton-conducting multilayer electrolyte membrane with a barrier layer, a process for producing it and a fuel cell containing such a membrane.

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