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1. 发明申请

WO2017108586A1 A METHOD FOR WITHDRAWING AGGLOMERATES FROM A FLUIDISED BED REACTOR 审中-公开
标题翻译：一种从流化床反应器中除去聚集体的方法
公开(公告)号：WO2017108586A1
公开(公告)日：2017-06-29
申请号：PCT/EP2016/081280
申请日：2016-12-15
申请人： BOREALIS AG
发明人： AL-HAJ ALI, Mohammad , KANELLOPOULOS, Vasileios , KRALLIS, Apostolos , NYFORS, Klaus , AGUAYO ARELLANO, Pablo Ivan , WEICKERT, Gunter , PRINSEN, Eric-Jan
IPC分类号： B01J4/00
CPC分类号： B01J8/0035 , B01J2208/00761 , B01J2208/00769
摘要： The present invention relates to a process and apparatus for withdrawing polymer agglomerates from a fluidised bed polymerisation reactor, the polymerisation reactor comprising a bottom zone having a generally conical shape and no fluidisation grid. The agglomerates are withdrawn by using an agglomerate trap below the bottom zone. A value of a process variable indicative of the content of agglomerates in the agglomerate trap is measured and the opening time of the valves transferring polymer to and from the agglomerate trap is adjusted based on the measured value.
摘要翻译：本发明涉及一种用于从流化床聚合反应器中回收聚合物附聚物的方法和设备，该聚合反应器包括具有大致圆锥形状的底部区域和不具有流化网格。通过在底部区域下方使用团聚物收集器来收集团聚物。测量指示凝聚物收集器中凝聚物含量的过程变量的值，并且基于测量值来调节将聚合物转移到凝聚物收集器和从聚集物收集器转移聚合物的阀的打开时间。

2. 发明申请

WO2016198631A1 METHOD AND APPARATUS FOR POLYMERISING OLEFINS IN GAS PHASE 审中-公开
标题翻译：在气相中聚合烯烃的方法和装置
公开(公告)号：WO2016198631A1
公开(公告)日：2016-12-15
申请号：PCT/EP2016/063342
申请日：2016-06-10
申请人： BOREALIS AG
发明人： KANELLOPOULOS, Vasileios , NYFORS, Klaus , AGUAYO ARELLANO, Pablo Ivan , WEICKERT, Gunter , PRINSEN, Eric-Jan
IPC分类号： C08F2/01 , B01J8/08 , B01J8/18 , B01J8/24 , C08F2/34
CPC分类号： C08F10/02 , B01J8/005 , B01J8/0055 , B01J8/006 , B01J8/1818 , B01J8/1827 , B01J8/1836 , B01J8/1863 , B01J8/1872 , B01J2208/00176 , B01J2208/00893 , B01J2208/00991 , C08F2/01 , C08F2/34 , C08F2500/07
摘要： The present invention deals with an olefin polymerisation process. At least one olefin is polymerised in gas phase in a fluidised bed in the presence of an olefin polymerisation catalyst in a polymerisation reactor having a vertical body; a generally conical downwards tapering bottom zone; a generally cylindrical middle zone above and connected to said bottom zone; and a generally conical upwards tapering top zone above and connected to said middle zone. Fluidisation gas is introduced to the bottom zone of the reactor from where it passes upwards through the reactor, and withdrawn from the top zone of the reactor. The gas is then compressed, cooled and returned into the bottom zone of the reactor. A fluidised bed is thus formed within the reactor where the growing polymer particles are suspended in the upwards rising gas stream wherein the superficial velocity of the fluidisation gas is less than the transport velocity of the particles. There is no fluidisation grid in the reactor. The fluidisation gas is passed from an inlet chamber into the bottom zone and the gas flows from the upper part of the inlet chamber to the lower part thereof and the gas flows from the lower part of the inlet chamber to the bottom zone.
摘要翻译：本发明涉及烯烃聚合方法。在具有垂直体的聚合反应器中，在烯烃聚合催化剂存在下，在流化床中将至少一种烯烃在气相中聚合; 大致圆锥形的向下锥形底部区域; 在所述底部区域上方并与之连接的大致圆柱形的中间区域以及在所述中间区域上方并连接到所述中间区域的大致圆锥形的向上锥形顶部区域。将流化气体引入反应器的底部区域，从其向上通过反应器，并从反应器的顶部区域排出。然后将气体压缩，冷却并返回到反应器的底部区域。因此，在反应器内形成流化床，其中生长的聚合物颗粒悬浮在向上升的气流中，其中流化气体的表观速度小于颗粒的输送速度。反应器中没有流化网。流化气体从入口室进入底部区域，并且气体从入口室的上部流动到其下部，并且气体从入口室的下部流动到底部区域。

3. 发明申请

WO2020244834A1 PROCESS AND REACTOR ASSEMBLY FOR THE ENHANCEMENT OF HYDRODYNAMICS IN A GAS-SOLIDS FLUIDIZED BED REACTOR 审中-公开
公开(公告)号：WO2020244834A1
公开(公告)日：2020-12-10
申请号：PCT/EP2020/059811
申请日：2020-04-06
申请人： BOREALIS AG
发明人： WEICKERT, Gunter , KANELLOPOULOS, Vasileios , PRINSEN, Eric-Jan , AGUAYO ARELLANO, Pablo Ivan , VAHTERI, Markku , SALMINEN, Juha , RUSKEENIEMI, Jari-Jussi , TUPE, Ravindra , ELOVAINIO, Erno , NYFORS, Klaus
IPC分类号： B01J19/18 , B01J8/24 , B01J8/38 , B01J8/44
摘要： A process for polymerizing olefin monomer(s) in a gas-solids olefin polymerization reactor comprising a top zone; a middle zone, which comprises a top end in direct contact with said top zone and which is located below said top zone, the middle zone having a generally cylindrical shape; and a bottom zone, which is in direct contact with a bottom end of the middle zone and which is located below the middle zone; comprising the following steps: introducing a fluidization gas stream into the bottom zone; polymerizing olefin monomer(s) in the presence of a polymerization catalyst in a dense phase formed by particles of a polymer of the olefin monomer(s) suspended in an upwards flowing stream of the fluidization gas in the middle zone; introducing a jet gas stream through one or more jet gas feeding ports in a jet gas feeding area of the middle zone at the dense phase in the middle zone of the gas-solids olefin polymerization reactor; wherein the kinetic energy (E JG ) input in the reactor by the jet stream is between 1.5 and 50 times higher than the kinetic energy (E FG ) input in the reactor by the fluidization gas stream (FG).

4. 发明申请

WO2018233999A1 PROCESS AND APPARATUS FOR REMOVING POLYMER MATERIAL FROM A GAS-SOLIDS OLEFIN POLYMERIZATION REACTOR 审中-公开
公开(公告)号：WO2018233999A1
公开(公告)日：2018-12-27
申请号：PCT/EP2018/064207
申请日：2018-05-30
申请人： BOREALIS AG
发明人： NYFORS, Klaus , ELOVAINIO, Erno , KANELLOPOULOS, Vasileios , WEICKERT, Gunter , PRINSEN, Eric-Jan
IPC分类号： C08F2/01 , B01J8/18 , B01J8/00 , C08F2/34 , C08F10/00
摘要： The present invention relates to a process for removing polymer material from a gas-solids olefin polymerization reactor wherein the gas-solids olefin polymerization reactor is connected to the top part of an outlet vessel via a feed pipe wherein the powder surface of discharged polymer material and the barrier gas injection point are situated in the outlet vessel as such to fulfill the following criteria: R' = X/Y ≤ 2.0; and R'' = X/D ≥ 1.0; wherein X = Distance between the powder surface and the barrier gas injection point; Y = Distance between the barrier gas injection point and the vessel outlet; and D = Equivalent outlet vessel diameter, an apparatus for continuously removing polymer material comprising a gas-solids olefin polymerization reactor, an outlet vessel and a feed pipe connecting the gas-solids olefin polymerization reactor with the top part of the outlet vessel and the use of said apparatus for polymerizing alpha- olefin homo- or copolymers having alpha-olefin monomer units of from 2 to 12 carbon atoms and for increasing the barrier gas efficiency of the gas-solids olefin reactor to at least 75 %.

5. 发明申请

WO2012056042A2 FEEDING SOLID MATERIAL INTO A HIGH DENSITY FLUIDIZED BED REACTOR 审中-公开
标题翻译：将固体物质输送到高密度流化床反应器中
公开(公告)号：WO2012056042A2
公开(公告)日：2012-05-03
申请号：PCT/EP2011/069128
申请日：2011-10-31
申请人： BOREALIS AG , WEICKERT, Gunter , BERGSTRA, Michiel , ERIKSSON, Erik
发明人： WEICKERT, Gunter , BERGSTRA, Michiel , ERIKSSON, Erik
IPC分类号： B01J8/00 , B01J8/10 , B01J8/38 , C08F10/00 , C08F2/34
CPC分类号： B01J8/0045 , B01J8/12 , B01J8/1827 , B01J8/26 , B01J8/386 , B01J8/388 , B01J2208/00752 , B01J2208/00761 , B01J2208/00876 , B01J2219/00038 , C08F10/00 , C08F110/02 , C08F2500/18 , C08F2/01
摘要： The reactor system (40) comprises a first reactor unit (47) with an outlet (50) for an product stream comprising a solid phase product in particulate form, and a fluidized bed reactor unit (41) provided with a particle inlet (64) coupled to the outlet of the first reactor unit (47) through a transportation pipe (60), which comprises mechanical displacement means (62) embodied as a screw and driven to rotate at a predefined rotation speed, and a densification zone (65) defined between said mechanical displacement means (62) and said particle inlet (64), in which densification zone (65), in operation, a density of the product stream is increased, said densification zone (65) defining a flow direction into said fluidized bed reactor unit (41). An unobstructed space (A) is defined in said fluidized bed reactor unit (41), the space extending from said particle inlet (64) over a distance of at least 0.4⋅D in said flow direction where D is the internal diameter of said fluidized bed reactor unit (41) at the level of said particle inlet (64).
摘要翻译：反应器系统（40）包括具有用于产物流的出口（50）的第一反应器单元（47），其包含颗粒形式的固相产物和设置有颗粒入口（64）的流化床反应器单元（41）通过运输管道（60）耦合到第一反应器单元（47）的出口，输送管道（60）包括实施为螺杆并被驱动以预定转速旋转的机械位移装置（62）和限定的致密化区在所述机械移动装置（62）和所述颗粒入口（64）之间，其中致密区（65）在操作中产品流的密度增加，所述致密化区（65）限定了流入所述流化床反应器单元（41）。在所述流化床反应器单元（41）中限定了无阻塞空间（A），所述流化床反应器单元（41）中的空间从所述颗粒入口（64）在所述流动方向上延伸至少0.4D的距离，其中D是所述流化床在所述颗粒入口（64）的水平面上的床反应器单元（41）。

6. 发明公开

EP3418310A1 PROCESS AND APPARATUS FOR REMOVING POLYMER MATERIAL FROM A GAS-SOLIDS OLEFIN POLYMERIZATION REACTOR 有权
公开(公告)号：EP3418310A1
公开(公告)日：2018-12-26
申请号：EP17177643.8
申请日：2017-06-23
申请人： Borealis AG
发明人： NYFORS, Klaus , ELOVAINIO, Erno , KANELLOPOULOS, Vasileios , WEICKERT, Gunter , PRINSEN, Eric-Jan
IPC分类号： C08F2/01 , B01J8/18 , B01J8/00 , C08F2/34 , C08F10/00
摘要： The present invention relates to a process for removing polymer material from a gas-solids olefin polymerization reactor wherein the gas-solids olefin polymerization reactor is connected to the top part of an outlet vessel via a feed pipe wherein the powder surface of discharged polymer material and the barrier gas injection point are situated in the outlet vessel as such to fulfill the following criteria: Rʹ = X / Y ≤ 2.0 ; and Rʹʹ = X / D ≥ 1.0 ; wherein X = Distance between the powder surface and the barrier gas injection point; Y = Distance between the barrier gas injection point and the vessel outlet; and D = Equivalent outlet vessel diameter, an apparatus for continuously removing polymer material comprising a gas-solids olefin polymerization reactor, an outlet vessel and a feed pipe connecting the gas-solids olefin polymerization reactor with the top part of the outlet vessel and the use of said apparatus for polymerizing alpha-olefin homo- or copolymers having alpha-olefin monomer units of from 2 to 12 carbon atoms and for increasing the barrier gas efficiency of the gas-solids olefin reactor to at least 75 %.

7. 发明授权

EP2632582B1 FEEDING SOLID MATERIAL INTO A HIGH DENSITY FLUIDIZED BED REACTOR 有权
标题翻译：将固体物料送入高密度流化床反应器
公开(公告)号：EP2632582B1
公开(公告)日：2018-03-21
申请号：EP11776209.6
申请日：2011-10-31
申请人： Borealis AG
发明人： WEICKERT, Gunter , BERGSTRA, Michiel , ERIKSSON, Erik
IPC分类号： B01J8/00 , B01J8/10 , B01J8/38 , C08F10/00 , C08F2/34
CPC分类号： B01J8/0045 , B01J8/12 , B01J8/1827 , B01J8/26 , B01J8/386 , B01J8/388 , B01J2208/00752 , B01J2208/00761 , B01J2208/00876 , B01J2219/00038 , C08F10/00 , C08F110/02 , C08F2500/18 , C08F2/01
摘要： The reactor system (40) comprises a first reactor unit (47) with an outlet (50) for an product stream comprising a solid phase product in particulate form, and a fluidized bed reactor unit (41) provided with a particle inlet (64) coupled to the outlet of the first reactor unit (47) through a transportation pipe (60), which comprises mechanical displacement means (62) embodied as a screw and driven to rotate at a predefined rotation speed, and a densification zone (65) defined between said mechanical displacement means (62) and said particle inlet (64), in which densification zone (65), in operation, a density of the product stream is increased, said densification zone (65) defining a flow direction into said fluidized bed reactor unit (41). An unobstructed space (A) is defined in said fluidized bed reactor unit (41), the space extending from said particle inlet (64) over a distance of at least 0.4·D in said flow direction where D is the internal diameter of said fluidized bed reactor unit (41) at the level of said particle inlet (64).

8. 发明公开

EP2632582A2 FEEDING SOLID MATERIAL INTO A HIGH DENSITY FLUIDIZED BED REACTOR 有权
标题翻译： ZUFUHR VON FESTSTOFFEN IN EINEN HOCHDICHTEN FLIESSBETTREAKTOR
公开(公告)号：EP2632582A2
公开(公告)日：2013-09-04
申请号：EP11776209.6
申请日：2011-10-31
申请人： Borealis AG
发明人： WEICKERT, Gunter , BERGSTRA, Michiel , ERIKSSON, Erik
IPC分类号： B01J8/00 , B01J8/10 , B01J8/38 , C08F10/00 , C08F2/34
CPC分类号： B01J8/0045 , B01J8/12 , B01J8/1827 , B01J8/26 , B01J8/386 , B01J8/388 , B01J2208/00752 , B01J2208/00761 , B01J2208/00876 , B01J2219/00038 , C08F10/00 , C08F110/02 , C08F2500/18 , C08F2/01
摘要： The reactor system (40) comprises a first reactor unit (47) with an outlet (50) for an product stream comprising a solid phase product in particulate form, and a fluidized bed reactor unit (41) provided with a particle inlet (64) coupled to the outlet of the first reactor unit (47) through a transportation pipe (60), which comprises mechanical displacement means (62) embodied as a screw and driven to rotate at a predefined rotation speed, and a densification zone (65) defined between said mechanical displacement means (62) and said particle inlet (64), in which densification zone (65), in operation, a density of the product stream is increased, said densification zone (65) defining a flow direction into said fluidized bed reactor unit (41). An unobstructed space (A) is defined in said fluidized bed reactor unit (41), the space extending from said particle inlet (64) over a distance of at least 0.4·D in said flow direction where D is the internal diameter of said fluidized bed reactor unit (41) at the level of said particle inlet (64).
摘要翻译：反应器系统（40）包括具有用于产物流的出口（50）的第一反应器单元（47），其包含颗粒形式的固相产物和设置有颗粒入口（64）的流化床反应器单元（41）通过输送管道（60）耦合到第一反应器单元（47）的出口，输送管道（60）包括被实施为螺杆并被驱动以预定转速旋转的机械位移装置（62）和定义的致密化区在所述机械移动装置（62）和所述颗粒入口（64）之间，其中致密区（65）在操作中产品流的密度增加，所述致密化区（65）限定到所述流化床反应器单元（41）。在所述流化床反应器单元（41）中限定了无阻塞空间（A），所述流化床反应器单元（41）中的空间从所述颗粒入口（64）延伸到所述流动方向上至少0.4D的距离，其中D是所述流化床在所述颗粒入口（64）的水平面上的床反应器单元（41）。

10. 发明授权

EP3418310B1 PROCESS AND APPARATUS FOR REMOVING POLYMER MATERIAL FROM A GAS-SOLIDS OLEFIN POLYMERIZATION REACTOR 有权
公开(公告)号：EP3418310B1
公开(公告)日：2020-04-08
申请号：EP17177643.8
申请日：2017-06-23
申请人： Borealis AG
发明人： NYFORS, Klaus , ELOVAINIO, Erno , KANELLOPOULOS, Vasileios , WEICKERT, Gunter , PRINSEN, Eric-Jan
IPC分类号： C08F2/01 , B01J8/18 , B01J8/00 , C08F2/34 , C08F10/00

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