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1. 发明申请

WO2007001380B1 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 审中-公开
标题翻译：用于固体氧化物燃料电池和其他高温应用的高强度绝缘接头及其制造方法
公开(公告)号：WO2007001380B1
公开(公告)日：2007-08-23
申请号：PCT/US2005033755
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
发明人： WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
IPC分类号： C03C8/24 , C03C8/14 , C04B37/02 , H01M8/12 , H01M8/24
CPC分类号： C03C27/044 , B32B2315/02 , C03C8/24 , C03C27/042 , C04B35/645 , C04B37/025 , C04B2235/6025 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6583 , C04B2235/661 , C04B2237/10 , C04B2237/30 , C04B2237/32 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/52 , C04B2237/592 , C04B2237/704 , C04B2237/706 , C04B2237/708 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：在两个部件之间形成的密封件将在高温操作环境中保持气密，所述高温操作环境经历频繁的热循环，其特别用作固体氧化物燃料电池中的绝缘接头。第一金属部件附接到增强材料。通过将玻璃加热至适于熔融玻璃形成材料的温度，在位于第一金属部件与第二部件之间的玻璃形成材料以及在第一金属部件与第二部件之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整个密封增加了巨大的强度。可以将陶瓷材料添加到玻璃形成材料中，以帮助在第一金属部件和第二部件之间形成绝缘屏障并且在加热步骤期间调节玻璃的粘度。

2. 发明申请

WO2007001380A3 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 审中-公开
标题翻译：固体氧化物燃料电池的高强度绝缘接头及其他高温应用及其制造方法
公开(公告)号：WO2007001380A3
公开(公告)日：2007-07-26
申请号：PCT/US2005033755
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
发明人： WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
IPC分类号： C03C8/24 , C03C8/14 , C04B37/02 , H01M8/12 , H01M8/24
CPC分类号： C03C27/044 , B32B2315/02 , C03C8/24 , C03C27/042 , C04B35/645 , C04B37/025 , C04B2235/6025 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6583 , C04B2235/661 , C04B2237/10 , C04B2237/30 , C04B2237/32 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/52 , C04B2237/592 , C04B2237/704 , C04B2237/706 , C04B2237/708 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：在两个部件之间形成的密封件，其将在经受频繁热循环的高温操作环境中保持气密，这在固体氧化物燃料电池中作为绝缘接头特别有用。第一金属部件附接到增强材料。定位在第一金属部分和第二部分之间的玻璃形成材料，并且通过将玻璃加热到适于熔化玻璃形成材料的温度，在第一金属部分和第二部分之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整体密封增加了巨大的强度。陶瓷材料可以添加到玻璃形成材料中，以帮助在第一金属部分和第二部分之间形成绝缘屏障，并且在加热步骤期间调节玻璃的粘度。

3. 发明专利

CA2857047A1 INTERMEDIATE TEMPERATURE SODIUM METAL-HALIDE ENERGY STORAGE DEVICES 未知
公开(公告)号：CA2857047A1
公开(公告)日：2013-08-08
申请号：CA2857047
申请日：2013-01-30
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： KIM JIN YONG , LI GUOSHENG , LU XIAOCHUAN , SPRENKLE VINCENT L , LEMMON JOHN P , YANG ZHENGUO , COYLE CHRISTOPHER A
IPC分类号： H01M10/38 , H01B1/06 , H01M2/08
摘要： Sodium metal-halide energy storage devices utilizing a substituting salt in its secondary electrolyte can operate at temperatures lower than conventional ZEBRA batteries while maintaining desirable performance and lifetime characteristics. According to one example, a sodium metal-halide energy storage device operates at a temperature less than or equal to 200 °C and has a liquid secondary electrolyte having MxNa1-yAlCl4-yHy, wherein M is a metal cation of a substituting salt, H is an anion of the substituting salt, y is a mole fraction of substituted Na and CI, and x is a ratio of y over r, where r is the oxidation state of M. The melting temperature of the substituting salt is less than that of NaCl.

4. 发明专利

DE69936228D1 未知
公开(公告)号：DE69936228D1
公开(公告)日：2007-07-12
申请号：DE69936228
申请日：1999-12-23
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： DOMANSKY KAREL , FRYXELL GLEN E , LIU JUN , KOHLER NATHAN J , BASKARAN SURESH , LI XIAOHONG , THEVUTHASAN SUNTHARAMPILLAI , COYLE CHRISTOPHER A , BIRNBAUM JEROME C
IPC分类号： C01B33/12 , C01B37/02 , B01J19/00 , H01L21/316
摘要： The present invention is a mesoporous silica film having a low dielectric constant and method of making having the steps of combining a surfactant in a silica precursor solution, spin-coating a film from this solution mixture, forming a partially hydroxylated mesoporous film, and dehydroxylating the hydroxylated film to obtain the mesoporous film. It is advantageous that the small polyoxyethylene ether surfactants used in spin-coated films as described in the present invention will result in fine pores smaller on average than about 20 nm. The resulting mesoporous film has a dielectric constant less than 3, which is stable in moist air with a specific humidity. The present invention provides a method for superior control of film thickness and thickness uniformity over a coated wafer, and films with low dielectric constant. The present invention is a method of dehydroxylating a silica surface that is hydroxylated having the steps of exposing the silica surface separately to a silicon organic compound and a dehydroxylating gas. Exposure to the silicon organic compound can be in liquid, gas or solution phase, and exposure to a dehydroxylating gas is typically at elevated temperatures. In one embodiment, the improvement of the dehydroxylation procedure is the repetition of the soaking and dehydroxylating gas exposure. In another embodiment, the improvement is the use of an inert gas that is substantially free of hydrogen. In yet another embodiment, the present invention is the combination of the two-step dehydroxylation method with a surfactant templating method of making a mesoporous film.

5. 发明专利

DE69936228T2 未知
公开(公告)号：DE69936228T2
公开(公告)日：2008-02-07
申请号：DE69936228
申请日：1999-12-23
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： DOMANSKY KAREL , FRYXELL GLEN E , LIU JUN , KOHLER NATHAN J , BASKARAN SURESH , LI XIAOHONG , THEVUTHASAN SUNTHARAMPILLAI , COYLE CHRISTOPHER A , BIRNBAUM JEROME C
IPC分类号： C01B33/12 , C01B37/02 , B01J19/00 , H01L21/316
摘要： The present invention is a mesoporous silica film having a low dielectric constant and method of making having the steps of combining a surfactant in a silica precursor solution, spin-coating a film from this solution mixture, forming a partially hydroxylated mesoporous film, and dehydroxylating the hydroxylated film to obtain the mesoporous film. It is advantageous that the small polyoxyethylene ether surfactants used in spin-coated films as described in the present invention will result in fine pores smaller on average than about 20 nm. The resulting mesoporous film has a dielectric constant less than 3, which is stable in moist air with a specific humidity. The present invention provides a method for superior control of film thickness and thickness uniformity over a coated wafer, and films with low dielectric constant. The present invention is a method of dehydroxylating a silica surface that is hydroxylated having the steps of exposing the silica surface separately to a silicon organic compound and a dehydroxylating gas. Exposure to the silicon organic compound can be in liquid, gas or solution phase, and exposure to a dehydroxylating gas is typically at elevated temperatures. In one embodiment, the improvement of the dehydroxylation procedure is the repetition of the soaking and dehydroxylating gas exposure. In another embodiment, the improvement is the use of an inert gas that is substantially free of hydrogen. In yet another embodiment, the present invention is the combination of the two-step dehydroxylation method with a surfactant templating method of making a mesoporous film.

6. 发明专利

AU2379900A Mesoporous silica film from a solution containing a surfactant and methods of making same 未知
公开(公告)号：AU2379900A
公开(公告)日：2000-07-31
申请号：AU2379900
申请日：1999-12-23
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： DOMANSKY KAREL , FRYXELL GLEN E , LIU JUN , KOHLER NATHAN J , BASKARAN SURESH , LI XIAOHONG , THEVUTHASAN SUNTHARAMPILLAI , COYLE CHRISTOPHER A , BIRNBAUM JEROME C
IPC分类号： C01B33/12 , B01J19/00 , C01B37/02 , H01L21/316
摘要： The present invention is a mesoporous silica film having a low dielectric constant and method of making having the steps of combining a surfactant in a silica precursor solution, spin-coating a film from this solution mixture, forming a partially hydroxylated mesoporous film, and dehydroxylating the hydroxylated film to obtain the mesoporous film. It is advantageous that the small polyoxyethylene ether surfactants used in spin-coated films as described in the present invention will result in fine pores smaller on average than about 20 nm. The resulting mesoporous film has a dielectric constant less than 3, which is stable in moist air with a specific humidity. The present invention provides a method for superior control of film thickness and thickness uniformity over a coated wafer, and films with low dielectric constant. The present invention is a method of dehydroxylating a silica surface that is hydroxylated having the steps of exposing the silica surface separately to a silicon organic compound and a dehydroxylating gas. Exposure to the silicon organic compound can be in liquid, gas or solution phase, and exposure to a dehydroxylating gas is typically at elevated temperatures. In one embodiment, the improvement of the dehydroxylation procedure is the repetition of the soaking and dehydroxylating gas exposure. In another embodiment, the improvement is the use of an inert gas that is substantially free of hydrogen. In yet another embodiment, the present invention is the combination of the two-step dehydroxylation method with a surfactant templating method of making a mesoporous film.

7. 发明专利

AU2013215308A1 Intermediate temperature sodium metal-halide energy storage devices 未知
公开(公告)号：AU2013215308A1
公开(公告)日：2014-06-19
申请号：AU2013215308
申请日：2013-01-30
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： KIM JIN YONG , LI GUOSHENG , LU XIAOCHUAN , SPRENKLE VINCENT L , LEMMON JOHN P , YANG ZHENGUO , COYLE CHRISTOPHER A
IPC分类号： H01M10/38 , H01B1/06 , H01M2/08
摘要： Sodium metal-halide energy storage devices utilizing a substituting salt in its secondary electrolyte can operate at temperatures lower than conventional ZEBRA batteries while maintaining desirable performance and lifetime characteristics. According to one example, a sodium metal-halide energy storage device operates at a temperature less than or equal to 200 °C and has a liquid secondary electrolyte having M

8. 发明专利

CA2579781A1 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 未知
公开(公告)号：CA2579781A1
公开(公告)日：2007-01-04
申请号：CA2579781
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： MEINHARDT KERRY D , XIA GUANGUANG , PAXTON DEAN M , SPRENKLE VINCENT L , COYLE CHRISTOPHER A , HARDY JOHN S , CHICK LAWRENCE A , WEIL K SCOTT
IPC分类号： B32B3/06 , B32B15/04 , H01M8/02 , H01M8/10
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.

9. 发明公开

EP2810333A4 INTERMEDIATE TEMPERATURE SODIUM METAL-HALIDE ENERGY STORAGE DEVICES 审中-公开
标题翻译： MITTELTEMPERATUR-NATRIUMMETALLHALOGEN-ENERGIESPEICHERVORRICHTUNGEN
公开(公告)号：EP2810333A4
公开(公告)日：2015-07-29
申请号：EP13743522
申请日：2013-01-30
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： KIM JIN YONG , LI GUOSHENG , LU XIAOCHUAN , SPRENKLE VINCENT L , LEMMON JOHN P , YANG ZHENGUO , COYLE CHRISTOPHER A
IPC分类号： H01M10/39 , C01F7/00 , H01B1/06 , H01M2/08
CPC分类号： H01M10/0563 , C01F7/002 , C01P2006/40 , H01M10/399 , H01M2300/0048 , H01M2300/0057

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