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1. 发明申请

WO2007001380B1 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 审中-公开
标题翻译：用于固体氧化物燃料电池和其他高温应用的高强度绝缘接头及其制造方法
公开(公告)号：WO2007001380B1
公开(公告)日：2007-08-23
申请号：PCT/US2005033755
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
发明人： WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
IPC分类号： C03C8/24 , C03C8/14 , C04B37/02 , H01M8/12 , H01M8/24
CPC分类号： C03C27/044 , B32B2315/02 , C03C8/24 , C03C27/042 , C04B35/645 , C04B37/025 , C04B2235/6025 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6583 , C04B2235/661 , C04B2237/10 , C04B2237/30 , C04B2237/32 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/52 , C04B2237/592 , C04B2237/704 , C04B2237/706 , C04B2237/708 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：在两个部件之间形成的密封件将在高温操作环境中保持气密，所述高温操作环境经历频繁的热循环，其特别用作固体氧化物燃料电池中的绝缘接头。第一金属部件附接到增强材料。通过将玻璃加热至适于熔融玻璃形成材料的温度，在位于第一金属部件与第二部件之间的玻璃形成材料以及在第一金属部件与第二部件之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整个密封增加了巨大的强度。可以将陶瓷材料添加到玻璃形成材料中，以帮助在第一金属部件和第二部件之间形成绝缘屏障并且在加热步骤期间调节玻璃的粘度。

2. 发明申请

WO2006014155A1 SOLID OXIDE FUEL CELL FRAMES AND METHOD OF MANUFACTURE 审中-公开
标题翻译：固体氧化物燃料电池框架及其制造方法
公开(公告)号：WO2006014155A1
公开(公告)日：2006-02-09
申请号：PCT/US2004/021385
申请日：2004-07-02
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL, K., Scott , PAXTON, Dean, Michael , MEINHARDT, Kerry, D.
发明人： WEIL, K., Scott , PAXTON, Dean, Michael , MEINHARDT, Kerry, D.
IPC分类号： H01M8/02
CPC分类号： H01M8/0273 , H01M8/0206 , H01M8/021 , H01M8/0247 , H01M8/0258 , H01M8/0282 , H01M8/2404 , H01M8/2425 , H01M8/2483 , H01M2008/1293 , Y02P70/56
摘要： A cassette for a SOFC stack formed by stamping a separator plate, stamping a frame, attaching a PEN cell to the frame, and attaching the frame to the separator plate. An insulating seal, preferably formed of glass, is provided between the PEN cell and the frame to provide electrical isolation between the frame and the separator plate. Electrical isolation is further provided by forming an insulating seal, preferably formed of glass, between the frame and the separator plate. A plurality of cassettes formed may be formed into a SOFC stack by sealing successive cassettes on top of one and another so that the anode side of each cassette is in electrical communication with the cathode side of each adjacent cassette, and forming an electrically isolated and gas tight seal between the frame of each cassette and the separator plate of each adjacent cassette. Separator plates and the frames are configured so that when a series of separator plates and frames having PEN cells are stacked together, (thereby forming a stack alternating between the two; separator plate/frame/separator plate/frame/ etc...), two separate pathways for gaseous flow are formed.
摘要翻译：用于通过冲压分离板，冲压框架，将PEN单元连接到框架上并将框架附接到分隔板而形成的SOFC堆叠的盒。优选由玻璃形成的绝缘密封件设置在PEN电池和框架之间，以在框架和隔板之间提供电气隔离。通过在框架和分隔板之间形成绝缘密封件，进一步提供优选由玻璃形成的隔离。形成的多个盒可以通过将一个或多个顶部上的连续盒密封而形成为SOFC堆叠，使得每个盒的阳极侧与每个相邻盒的阴极侧电连通，并且形成电隔离和气体每个盒的框架和每个相邻盒的隔板之间的密封。分隔板和框架被构造成使得当具有PEN单元的一系列分隔板和框架堆叠在一起时（从而在两者之间形成一个交替的堆叠;隔离板/框架/隔板/框架等）时，形成用于气流的两个单独路径。

3. 发明申请

WO2010039434A2 CASSETTES FOR SOLID-OXIDE FUEL CELL STACKS AND METHODS OF MAKING THE SAME 审中-公开
标题翻译：用于固体氧化物燃料电池堆的盒及其制造方法
公开(公告)号：WO2010039434A2
公开(公告)日：2010-04-08
申请号：PCT/US2009057137
申请日：2009-09-16
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL K SCOTT , MEINHARDT KERRY D , SPRENKLE VINCENT L
发明人： WEIL K SCOTT , MEINHARDT KERRY D , SPRENKLE VINCENT L
IPC分类号： H01M8/02 , H01M8/12 , H01M8/24
CPC分类号： H01M8/0273 , H01M8/0247 , H01M8/0256 , H01M8/028 , H01M8/1231 , H01M8/2475 , Y10T29/4911
摘要： Solid-oxide fuel cell (SOFC) stack assembly designs are consistently investigated to develop an assembly that provides optimal performance, and durability, within desired cost parameters. A new design includes a repeat unit having a SOFC cassette and being characterized by a three-component construct. The three components include an oxidation-resistant, metal window frame hermetically joined to an electrolyte layer of a multi-layer, anode-supported ceramic cell and a pre-casselte including a separator plate having a plurality of vias that provide electrical contact between an anode-side collector within the pre-cassette and a cathode-side current collector of an adjacent cell. The third component is a cathode-side seal, which includes a standoff that supports a cathode channel spacing between each of the cassettes in a stack. Cassettes arc formed by joining the pre-cassette and the window frame.
摘要翻译：固体氧化物燃料电池（SOFC）堆叠组件设计一直在进行研究，以开发能够在所需成本参数范围内提供最佳性能和耐用性的组件。新设计包括具有SOFC盒的重复单元，其特征在于三组分结构。这三个部件包括与多层阳极支撑陶瓷电池的电解质层气密连接的抗氧化金属窗框，以及包括隔板的预铸铁壳，所述隔板具有多个通孔，所述通孔提供阳极预盒子内的侧面集电器和相邻电池的阴极侧集电器。第三部件是阴极侧密封件，其包括支撑堆叠中的每个盒之间的阴极通道间隔的支架。盒式磁带是通过连接预录像带和窗口框架形成的。

4. 发明申请

WO2007001380A2 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 审中-公开
标题翻译：用于固体氧化物燃料电池和其他高温应用的高强度绝缘接头及其制造方法
公开(公告)号：WO2007001380A2
公开(公告)日：2007-01-04
申请号：PCT/US2005/033755
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL, K., Scott , CHICK, Lawrence, A. , COYLE, Christopher, A. , HARDY, John, S. , XIA, Guanguang , MEINHARDT, Kerry, D. , SPRENKLE, Vincent, L. , PAXTON, Dean, M.
发明人： WEIL, K., Scott , CHICK, Lawrence, A. , COYLE, Christopher, A. , HARDY, John, S. , XIA, Guanguang , MEINHARDT, Kerry, D. , SPRENKLE, Vincent, L. , PAXTON, Dean, M.
CPC分类号： C03C27/044 , B32B2315/02 , C03C8/24 , C03C27/042 , C04B35/645 , C04B37/025 , C04B2235/6025 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6583 , C04B2235/661 , C04B2237/10 , C04B2237/30 , C04B2237/32 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/52 , C04B2237/592 , C04B2237/704 , C04B2237/706 , C04B2237/708 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：在经历频繁热循环的高温操作环境中将保持气密的两个部件之间形成的密封件，其特别用作固体氧化物燃料电池中的绝缘接头。第一金属部件附接到增强材料。通过将玻璃加热至适于熔融玻璃形成材料的温度，在位于第一金属部件与第二部件之间的玻璃形成材料以及在第一金属部件与第二部件之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整个密封增加了巨大的强度。可以将陶瓷材料添加到玻璃形成材料中，以帮助在第一金属部件和第二部件之间形成绝缘屏障并且在加热步骤期间调节玻璃的粘度。

5. 发明申请

WO2010039434A3 CASSETTES FOR SOLID-OXIDE FUEL CELL STACKS AND METHODS OF MAKING THE SAME 审中-公开
公开(公告)号：WO2010039434A3
公开(公告)日：2010-04-08
申请号：PCT/US2009/057137
申请日：2009-09-16
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL, K., Scott , MEINHARDT, Kerry, D. , SPRENKLE, Vincent, L.
发明人： WEIL, K., Scott , MEINHARDT, Kerry, D. , SPRENKLE, Vincent, L.
IPC分类号： H01M8/02 , H01M8/12 , H01M8/24
摘要： Solid-oxide fuel cell (SOFC) stack assembly designs are consistently investigated to develop an assembly that provides optimal performance, and durability, within desired cost parameters. A new design includes a repeat unit having a SOFC cassette and being characterized by a three-component construct. The three components include an oxidation-resistant, metal window frame hermetically joined to an electrolyte layer of a multi-layer, anode-supported ceramic cell and a pre-casselte including a separator plate having a plurality of vias that provide electrical contact between an anode-side collector within the pre-cassette and a cathode-side current collector of an adjacent cell. The third component is a cathode-side seal, which includes a standoff that supports a cathode channel spacing between each of the cassettes in a stack. Cassettes arc formed by joining the pre-cassette and the window frame.

6. 发明申请

WO2007001380A3 HIGH STRENGTH INSULATING JOINTS FOR SOLID OXIDE FUEL CELLS AND OTHER HIGH TEMPERATURE APPLICATIONS AND METHOD OF MAKING 审中-公开
标题翻译：固体氧化物燃料电池的高强度绝缘接头及其他高温应用及其制造方法
公开(公告)号：WO2007001380A3
公开(公告)日：2007-07-26
申请号：PCT/US2005033755
申请日：2005-09-19
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
发明人： WEIL K SCOTT , CHICK LAWRENCE A , COYLE CHRISTOPHER A , HARDY JOHN S , XIA GUANGUANG , MEINHARDT KERRY D , SPRENKLE VINCENT L , PAXTON DEAN M
IPC分类号： C03C8/24 , C03C8/14 , C04B37/02 , H01M8/12 , H01M8/24
CPC分类号： C03C27/044 , B32B2315/02 , C03C8/24 , C03C27/042 , C04B35/645 , C04B37/025 , C04B2235/6025 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6583 , C04B2235/661 , C04B2237/10 , C04B2237/30 , C04B2237/32 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/52 , C04B2237/592 , C04B2237/704 , C04B2237/706 , C04B2237/708 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between two parts that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：在两个部件之间形成的密封件，其将在经受频繁热循环的高温操作环境中保持气密，这在固体氧化物燃料电池中作为绝缘接头特别有用。第一金属部件附接到增强材料。定位在第一金属部分和第二部分之间的玻璃形成材料，并且通过将玻璃加热到适于熔化玻璃形成材料的温度，在第一金属部分和第二部分之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整体密封增加了巨大的强度。陶瓷材料可以添加到玻璃形成材料中，以帮助在第一金属部分和第二部分之间形成绝缘屏障，并且在加热步骤期间调节玻璃的粘度。

7. 发明申请

WO2003059843A1 METHOD OF JOINING CERAMIC AND METAL PARTS 审中-公开
标题翻译：陶瓷和金属部件接合方法
公开(公告)号：WO2003059843A1
公开(公告)日：2003-07-24
申请号：PCT/US2003/000763
申请日：2003-01-09
申请人： BATTELLE MEMORIAL INSTITUTE , WEIL, K., Scott , HARDY, John, S. , KIM, Jin, Yong
发明人： WEIL, K., Scott , HARDY, John, S. , KIM, Jin, Yong
IPC分类号： C04B37/02
CPC分类号： H01M8/0286 , B23K1/0008 , B23K1/008 , B23K35/004 , B23K35/3006 , B23K35/322 , B32B2311/30 , B32B2315/02 , C04B35/2633 , C04B35/2641 , C04B35/50 , C04B37/006 , C04B37/023 , C04B37/026 , C04B2235/3213 , C04B2235/3215 , C04B2235/3227 , C04B2235/3229 , C04B2235/3239 , C04B2235/3251 , C04B2235/3275 , C04B2235/3281 , C04B2235/407 , C04B2235/408 , C04B2235/65 , C04B2235/80 , C04B2237/125 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/365 , C04B2237/406 , C04B2237/54 , H01M8/0271 , H01M8/0282 , H01M8/0297 , H01M2008/1293 , Y02P70/56
摘要： A method of joining metal and ceramic parts, wherein an alumina forming metal part and a ceramic part are provided. A braze material in placed between the alumina forming metal part and the ceramic part, and the combination is then heated in an oxidizing atmosphere, preferably in air at a temperature of between 500 °C and 1300 °C. The alumina forming metal parts are selected from the group consisting of high temperature stainless steels, such as Durafoil (alpha-4), Fecralloy, Alumina-coated 430 stainless steel and Crofer-22APU, and high temperature superalloys such as Haynes 214, Nicrofer 6025, and Ducraloy. The braze material is selected as a metal oxide-noble metal mixture, preferably AG-CuO, Ag-V 2 O 5 , and Pt-Nb 2 O 5 , and more preferably between 30.65 to 100 mole% Ag in CuO.
摘要翻译：一种连接金属和陶瓷部件的方法，其中提供了氧化铝形成金属部件和陶瓷部件。在氧化铝形成金属部件和陶瓷部件之间放置钎焊材料，然后将该组合物在氧化气氛中，优选在空气中在500℃至1300℃的温度下加热。氧化铝形成金属部件选自高温不锈钢，例如Durafoil（α-4），Fecralloy，涂有氧化铝的430不锈钢和Crofer-22APU，以及高温超合金，例如Haynes 214，Nicrofer 6025 和Ducraloy。选择钎焊材料作为金属氧化物 - 贵金属混合物，优选AG-CuO，Ag-V 2 O 5和Pt-Nb 2 O 5，更优选CuO中的30.65-100摩尔％的Ag。

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