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1. 发明申请

WO2008054804A3 HYDROXYMETHYL FURFURAL OXIDATION METHODS 审中-公开
标题翻译：羟丙基氧化氧化方法
公开(公告)号：WO2008054804A3
公开(公告)日：2008-09-18
申请号：PCT/US2007023063
申请日：2007-10-31
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA MICHAEL A , HALLEN RICHARD T , HU JIANLI , WHITE JAMES F , GARY MICHEL J
发明人： LILGA MICHAEL A , HALLEN RICHARD T , HU JIANLI , WHITE JAMES F , GARY MICHEL J
IPC分类号： C07D307/44 , B01J23/00 , C07D307/48
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O 2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50°C to about 200°C A method of producing an oxidation catalyst where ZrO 2 is provided and is calcined. The ZrO 2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O 2 .
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中提供包含HMF的起始材料进入反应器。将空气和O 2 2中的至少一个提供到反应器中。使起始材料与载体材料上的Pt催化剂接触，在载体材料上进行接触，反应器温度为约50℃至约200℃，制备氧化催化剂的方法，其中ZrO 2 并被煅烧。将ZrO 2 2与乙酰丙酮铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2 2的流下被钝化。

2. 发明申请

WO2007146836B1 HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL 审中-公开
标题翻译：羟丙基纤维素还原方法及其制备方法
公开(公告)号：WO2007146836B1
公开(公告)日：2008-03-06
申请号：PCT/US2007070802
申请日：2007-06-08
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
发明人： LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
IPC分类号： C07D307/12 , C07D307/40
CPC分类号： C07D307/12 , C07D307/40
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H 2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250°C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H 2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30°C. A method of producing tetrahydofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh中的至少一种金属的催化剂接触，温度小于或等于250℃。氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

3. 发明专利

PL3102554T3 KONWERSJA 2,3-BUTANODIOLU DO BUTADIENU 未知
公开(公告)号：PL3102554T3
公开(公告)日：2022-07-18
申请号：PL15742636
申请日：2015-01-28
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： LILGA MICHAEL A , FRYE JR JOHN G , LEE SUH-JANE , ALBRECHT KARL O

4. 发明专利

AR053585A1 METODO Y APARATO PARA LA CONVERSION DE COMPUESTOS DE (BETA)-HIDROXICARBONILO 未知
公开(公告)号：AR053585A1
公开(公告)日：2007-05-09
申请号：ARP060101510
申请日：2006-04-17
申请人： BATTELLE MEMORIAL INSTITUTE , CARGILL INC
发明人： ZACHER ALAN H , HOLLADAY JOHNATHAN E , LILGA MICHAEL A , WHITE JAMES F , MUZATKO DANIELLE S , ORTH RICK J , TSOBANAKIS PARASKEVAS , MENG XLANGSHENG , ABRAHAM TIMOTHY W
IPC分类号： C07C57/04 , C07C233/09 , C07C69/54
摘要： Proceso para conversion de compuestos de beta-hidroxicarbonilo que comprende: proveer en un reactor material con compuesto de beta-hidroxicarbonilo líquido seleccionado entre ácido 3-hidroxipropionico, ácidos 3-hidroxipropionicos sustituidos, éteres 3- hidroxipropionicos, dímeros de ésteres 3-hidroxipropionicos, ésteres 3-hidroxipropionicos, dímeros de éter 3-hidroxipropionicos, sales de ácido 3-hidroxipropionico, amidas 3-hidroxipropionicas, propionaldehídos 3-hidroxipropionicos, o sus combinaciones, a velocidad de flujo y temperatura de 90 a 250 degree C para que reaccione dentro del reactor en ausencia de un flujo de gas inerte, composicion o sin solvente y se convierta en productos vaporizables comprendiendo un compuesto carbonilo alfa,beta-insaturado como ser ácido acrílico o metacrílico, sus sales, éteres, acroleína, que se recuperan con alto rendimiento por enfriado y/o condensacion. Puede usar un catalizador de oxidos o ácidos solidos, básicos, resinas de intercambio ionico, gases ácidos o básicos, como ser TiO2, Al2O3, SiO2, ZnO2, SnO2, WO3, MnO2, Fe2O3, SiO2/Al2O3, ZrO2/WO3, ZrO2/Fe2O3, ZrO2/MnO2, etc..Aparato correspondiente que comprende lecho escurridizo, fijo o fluido, tanque agitado, tanque con agitacion continua, membrana, Berty, flujo taponado, columna de burbuja, columna de destilacion reactiva. Los productos se usan como alimento animal y/o productos químicos de uso final.

5. 发明专利

NO881817L 未知
公开(公告)号：NO881817L
公开(公告)日：1988-06-23
申请号：NO881817
申请日：1988-04-26
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： JAMES BRIAN R , LI-LEE CHUNG , LILGA MICHAEL A , NELSON DAVID A
IPC分类号： B01D53/00 , B01D53/14 , C01B3/02

6. 发明专利

BR0114593A 未知
公开(公告)号：BR0114593A
公开(公告)日：2005-01-11
申请号：BR0114593
申请日：2001-10-09
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WERPY TODD A , LILGA MICHAEL A
IPC分类号： C07C57/065 , C07C67/327 , C07C69/67 , C07C67/08 , C07C69/54

7. 发明专利

AU1307802A Ester compounds and their use in forming acrylates 未知
公开(公告)号：AU1307802A
公开(公告)日：2002-04-29
申请号：AU1307802
申请日：2001-10-09
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WERPY TODD A , LILGA MICHAEL A
IPC分类号： C07C57/065 , C07C67/327 , C07C69/67 , C07C67/08 , C07C69/54

8. 发明专利

CA2107109A1 METHOD AND REACTION PATHWAY FOR SELECTIVELY OXIDIZING ORGANIC COMPOUNDS 未知
公开(公告)号：CA2107109A1
公开(公告)日：1992-10-04
申请号：CA2107109
申请日：1992-02-25
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： CAMAIONI DONALD M , LILGA MICHAEL A
IPC分类号： C07B33/00 , C07C67/035 , C07C69/63 , C07C27/02 , C07C35/08 , C07C1/20 , C07C13/20 , C07C67/39 , C07C29/48
摘要： 2107109 9217425 PCTABS00016 A method of selectively oxidizing an organic compound in a single vessel comprises: a) combining an organic compound, an acid solution in which the organic compound is soluble, a compound containing two oxygen atoms bonded to one another, and a metal ion reducing agent capable of reducing one of such oxygen atoms, and thereby forming a mixture; b) reducing the compound containing the two oxygen atoms by reducing one of such oxygen atoms with the metal ion reducing agent to, 1) oxidizing the metal ion reducing agent to a higher valence state, and 2) produce an oxygen containing intermediate capable of oxidizing the organic compound; c) reacting the oxygen containing intermediate with the organic compound to oxidize the organic compound into an oxidized organic intermediate, the oxidized organic intermediate having an oxidized carbon atom; d) reacting the oxidized organic intermediate with the acid counter ion and higher valence state metal ion to bond the acid counter ion to the oxidized carbon atom and thereby produce a quantity of an ester incorporating the organic intermediate and acid counter ion; and e) reacting the oxidized organic intermediate with the higher valence state metal ion and water to produce a quantity of alcohol which is less than the quantity of ester, the acid counter ion incorporated in the ester rendering the carbon atom bonded to the counter ion less reactive with the oxygen containing intermediate in the mixture than is the alcohol with the oxygen containing intermediate.

9. 发明专利

NO881817A 未知
公开(公告)号：NO881817A
公开(公告)日：1988-06-23
申请号：NO881817
申请日：1988-04-26
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： JAMES BRIAN R , LI-LEE CHUNG , LILGA MICHAEL A , NELSON DAVID A
IPC分类号： B01D53/00 , B01D53/14 , C01B3/02

10. 发明专利

AR054030A1 METODO PARA LA CONVERSION DE COMPUESTOS DE (BETA)-HIDROXICARBONILO 未知
公开(公告)号：AR054030A1
公开(公告)日：2007-05-30
申请号：ARP060101509
申请日：2006-04-17
申请人： CARGILL INC , BATTELLE MEMORIAL INSTITUTE
发明人： LILGA MICHAEL A , WHITE JAMES F , MUZATKO DANIELLE S , ORTH RICK J , HOLLADAY JOHNATHAN E , ZACKER ALAN H , TSOBANAKIS PARASKEVAS , MENG XLANGSHENG , ABRAHAM TIMOTHY W
IPC分类号： C07C57/04 , C07C233/09 , C07C69/54
摘要： Proceso que comprende proveer material de sal de amonio o beta-hidroxicarbonilo, líquido, como ser ácido 3-hidroxipropionico, dímeros de ésteres 3-hidroxipropionicos, dímeros de éteres 3-hidroxipropionicos, o sus combinaciones en un reactor a velocidad de flujo y temperatura para que reaccione dentro del reactor, sin gas inerte y se convierta en productos de amidas o acrilamida, capaces de vaporizarse, que comprenden compuestos carbonilo alfa,beta-insaturado y/o una sal de amonio de compuesto carbonilo alfa, beta-insaturado para ser recuperado con alto rendimiento. Puede usar catalizador de deshidratacion como ser oxidos o ácidos solidos como ser TiO2, ZrO2, Al2O3, SiO2, ZnO2, SnO2, WO3, MnO2, Fe2O3, SiO2/Al2O3, ZrO2/WO3, ZrO2/Fe2O3, ZrO2/MnO2, catalizadores ácidos, básicos, resinas de intercambio ionico, gases ácidos, gases básicos, como ser amoníaco, polivinilpiridina, hidroxidos de metal, Zr(OH)4 o aminas de la forma NR1R2R3, amoníaco, polivinilpiridina, hidroxidos de metal, Zr(OH)4 o aminas o sus combinaciones. Comprende un inhibidor de formacion de polímeros y un solvente.

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