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1. 发明申请

WO2008054804A3 HYDROXYMETHYL FURFURAL OXIDATION METHODS 审中-公开
标题翻译：羟丙基氧化氧化方法
公开(公告)号：WO2008054804A3
公开(公告)日：2008-09-18
申请号：PCT/US2007023063
申请日：2007-10-31
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA MICHAEL A , HALLEN RICHARD T , HU JIANLI , WHITE JAMES F , GARY MICHEL J
发明人： LILGA MICHAEL A , HALLEN RICHARD T , HU JIANLI , WHITE JAMES F , GARY MICHEL J
IPC分类号： C07D307/44 , B01J23/00 , C07D307/48
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O 2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50°C to about 200°C A method of producing an oxidation catalyst where ZrO 2 is provided and is calcined. The ZrO 2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O 2 .
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中提供包含HMF的起始材料进入反应器。将空气和O 2 2中的至少一个提供到反应器中。使起始材料与载体材料上的Pt催化剂接触，在载体材料上进行接触，反应器温度为约50℃至约200℃，制备氧化催化剂的方法，其中ZrO 2 并被煅烧。将ZrO 2 2与乙酰丙酮铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2 2的流下被钝化。

2. 发明申请

WO2007146836B1 HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL 审中-公开
标题翻译：羟丙基纤维素还原方法及其制备方法
公开(公告)号：WO2007146836B1
公开(公告)日：2008-03-06
申请号：PCT/US2007070802
申请日：2007-06-08
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
发明人： LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
IPC分类号： C07D307/12 , C07D307/40
CPC分类号： C07D307/12 , C07D307/40
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H 2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250°C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H 2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30°C. A method of producing tetrahydofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh中的至少一种金属的催化剂接触，温度小于或等于250℃。氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

3. 发明专利

AU3765589A BRIDGED TRANSITION-METAL COMPLEXES AND USES THEREOF FOR HYDROGEN SEPARATION, STORAGE AND HYDROGENATION 未知
公开(公告)号：AU3765589A
公开(公告)日：1990-01-05
申请号：AU3765589
申请日：1989-05-30
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： LILGA MICHAEL A , HALLEN RICHARD T
IPC分类号： C07F11/00 , C07F13/00 , C07F15/00 , C07F15/06 , C07F15/02 , C01B3/50
摘要： The present invention constitutes a class of organometallic complexes which reversibly react with hydrogen to form dihydrides and processes by which these compounds can be utilized. The class includes bimetallic complexes in which two cyclopentadienyl rings are bridged together and also separately pi -bonded to two transition metal atoms. The transition metals are believed to bond with the hydrogen in forming the dihydride. Transition metals such as Fe, Mn or Co may be employed in the complexes although Cr constitutes the preferred metal. A multiple number of ancilliary ligands such as CO are bonded to the metal atoms in the complexes. Alkyl groups and the like may be substituted on the cyclopentadienyl rings. These organometallic compounds may be used in absorption/desorption systems and in facilitated transport membrane systems for storing and separating out H2 from mixed gas streams such as the produce gas from coal gasification processes.

4. 发明专利

AU2021206156A1 Hydrothermal liquefaction system 未知
公开(公告)号：AU2021206156A1
公开(公告)日：2022-07-28
申请号：AU2021206156
申请日：2021-01-04
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： THORSON MICHAEL R , SNOWDEN-SWAN LESLEY J , SCHMIDT ANDREW J , HART TODD R , BILLING JUSTIN M , ANDERSON DANIEL B , HALLEN RICHARD T
IPC分类号： C10G1/00 , B09B3/00 , C02F11/00 , C10L9/08
摘要： A hydrothermal liquefaction (HTL) system can include a biomass slurry source, a first pump in fluid communication with the slurry source and configured to pressurize a biomass slurry stream from the slurry source to a first pressure, a first heat exchanger in fluid communication with the first pump and configured to heat a slurry stream received from the first pump to a first temperature, a second pump in fluid communication with the first heat exchanger and configured to pressurize a slurry stream received from the first heat exchanger to a second pressure higher than the first pressure, a second heat exchanger in fluid communication with the second pump and configured to heat a slurry stream received from the second pump to a second temperature higher than the first temperature, and a HTL reactor configured to produce biocrude from a slurry stream received from the second heat exchanger.

5. 发明专利

CA2961648A1 CATALYTIC HYDROTHERMAL LIQUEFACTION FOR BIO-OIL PRODUCTION 未知
公开(公告)号：CA2961648A1
公开(公告)日：2017-12-28
申请号：CA2961648
申请日：2017-03-22
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： HART TOOD R , ELLIOTT DOUGLAS C , SCHMIDT ANDREW J , HALLEN RICHARD T
IPC分类号： C11B3/02 , C11B1/00 , C11B1/12 , C11B3/00
摘要： Embodiments of a method for producing bio-oil include hydrothermal liquefaction of a biomass (e.g., a lignocellulosic biomass) feedstock to provide a process stream comprising crude oil and an aqueous fraction. The process stream is catalytically upgraded by contact with a sulfided-ruthenium catalyst, in the absence of added hydrogen, at a temperature and pressure effective to reduce an oxygen content of the crude oil, reduce a nitrogen content of the crude oil, reduce a total acid number of the crude oil, increase a H:C mole ratio of the crude oil, reduce a density of the crude oil, reduce a moisture content of the crude oil, reduce viscosity of the crude oil, or any combination thereof, thereby producing an upgraded oil and an upgraded aqueous fraction, which are subsequently separated. The catalytic upgrading process may be a plug-flow process and/or may be performed at or near liquefaction conditions.

6. 发明专利

BR9105944A 未知
公开(公告)号：BR9105944A
公开(公告)日：1992-11-17
申请号：BR9105944
申请日：1991-01-22
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WALKUP PAUL C , ROHRMANN A , HALLEN RICHARD T , EAKIN DAVID E
IPC分类号： C07C67/327 , C12P7/56 , C12P7/62
摘要： Processes are disclosed for producing lactic acid, esters of lactic acid, acrylic acid, and esters of acrylic acid, primarily from fermentable carbohydrate materials. An overall process for producing esters of acrylic acid comprises: a) fermenting carbohydrate material with a lactic-acid-forming organism in the presence of NH3 to produce ammonium lactate; b) combining the ammonium lactate with an alcohol; c) combining the ammonium lactate and alcohol with an effective catalyzing amount of gaseous CO2 to catalytically esterify the ammonium lactate and alcohol into a lactic acid ester containing solution; d) recovering purified lactic acid ester; and e) vaporizing the lactic acid ester and passing it through a solid catalyst bed comprised of an effective catalyzing amount of crystalline hydrated and partially calcined calcium sulfate to catalytically convert lactic acid ester into an acrylic acid ester. Step "d" would be useful in a process for making low-cost, purified lactic acid. Similarly, step "e" would be useful in a process for making low cost, purified acrylic acid.

7. 发明专利

MX9102246A 未知
公开(公告)号：MX9102246A
公开(公告)日：1992-07-01
申请号：MX9102246
申请日：1991-01-22
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WALKUP PAUL C , ROHRMANN CHARLES A , HALLEN RICHARD T , EARKIN DAVID E
IPC分类号： C12P7/56

8. 发明专利

AU7225391A PRODUCTION OF ESTERS OF LACTIC ACID, ESTERS OF ACRYLIC ACID, LACTIC ACID AND ACRYLIC ACID 未知
公开(公告)号：AU7225391A
公开(公告)日：1991-08-21
申请号：AU7225391
申请日：1991-01-22
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WALKUP PAUL C , ROHRMANN CHARLES A , HALLEN RICHARD T , EAKIN DAVID E
IPC分类号： C07C67/327 , C12P7/56 , C12P7/62
摘要： Processes are disclosed for producing lactic acid, esters of lactic acid, acrylic acid, and esters of acrylic acid, primarily from fermentable carbohydrate materials. An overall process for producing esters of acrylic acid comprises: a) fermenting carbohydrate material with a lactic-acid-forming organism in the presence of NH3 to produce ammonium lactate; b) combining the ammonium lactate with an alcohol; c) combining the ammonium lactate and alcohol with an effective catalyzing amount of gaseous CO2 to catalytically esterify the ammonium lactate and alcohol into a lactic acid ester containing solution; d) recovering purified lactic acid ester; and e) vaporizing the lactic acid ester and passing it through a solid catalyst bed comprised of an effective catalyzing amount of crystalline hydrated and partially calcined calcium sulfate to catalytically convert lactic acid ester into an acrylic acid ester. Step "d" would be useful in a process for making low-cost, purified lactic acid. Similarly, step "e" would be useful in a process for making low cost, purified acrylic acid.

9. 发明专利

AR082459A1 DESOXIGENACION DE ACIDOS GRASOS PARA LA PREPARACION DE HIDROCARBUROS 未知
公开(公告)号：AR082459A1
公开(公告)日：2012-12-12
申请号：ARP110102790
申请日：2011-08-02
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： HALLEN RICHARD T , ALBRECHT KARL O , BROWN HEATHER M , WHITE JAMES F
IPC分类号： C07C1/22
摘要： Métodos para obtener diesel renovable por desoxigenación de ácidos grasos para producir hidrocarburos. Los ácidos grasos se exponen a un catalizador que se selecciona entre a) M1/M2/M3O2 donde M1 es un metal de transición, un óxido de un metal de transición, o una combinación de los mismos, donde el metal de transición es Fe, Mn, Mo, V, o W; M2 es Pt, PtO, PtO2, o una combinación de los mismos; y M3 es Ti o Zr; o b) Pt/Ge o Pt/Sn sobre carbón, y el catalizador descarboxila por lo menos el 10% de los ácidos grasos. La desoxigenación se lleva a cabo sin agregar hidrógeno y a menos de 100 psi. Las formas de realización de los catalizadores desoxigenan por lo menos el 10% de los ácidos grasos presentes en una alimentación de ácidos grasos, y conservan la capacidad de desoxigenar ácidos grasos durante entre por lo menos 200 minutos y más de 350 horas.

10. 发明专利

AU647081B2 Production of esters of lactic acid, esters of acrylic acid, lactic acid and acrylic acid 未知
公开(公告)号：AU647081B2
公开(公告)日：1994-03-17
申请号：AU7225391
申请日：1991-01-22
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： WALKUP PAUL C , ROHRMANN CHARLES A , HALLEN RICHARD T , EAKIN DAVID E
IPC分类号： C07C67/327 , C12P7/56 , C12P7/62 , C07C67/08 , C07C69/68 , C07C69/54 , C07C59/08 , C07C27/02
摘要： Processes are disclosed for producing lactic acid, esters of lactic acid, acrylic acid, and esters of acrylic acid, primarily from fermentable carbohydrate materials. An overall process for producing esters of acrylic acid comprises: a) fermenting carbohydrate material with a lactic-acid-forming organism in the presence of NH3 to produce ammonium lactate; b) combining the ammonium lactate with an alcohol; c) combining the ammonium lactate and alcohol with an effective catalyzing amount of gaseous CO2 to catalytically esterify the ammonium lactate and alcohol into a lactic acid ester containing solution; d) recovering purified lactic acid ester; and e) vaporizing the lactic acid ester and passing it through a solid catalyst bed comprised of an effective catalyzing amount of crystalline hydrated and partially calcined calcium sulfate to catalytically convert lactic acid ester into an acrylic acid ester. Step "d" would be useful in a process for making low-cost, purified lactic acid. Similarly, step "e" would be useful in a process for making low cost, purified acrylic acid.

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