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1. 发明申请

WO2009045606A1 MULTI-METAL HYDROGENATION CATALYSTS 审中-公开
标题翻译：多金属氢化催化剂
公开(公告)号：WO2009045606A1
公开(公告)日：2009-04-09
申请号：PCT/US2008/070786
申请日：2008-07-22
申请人： BATTELLE MEMORIAL INSTITUTE , FRYE, John, G. , HOLLADAY, Johnathan, E. , MUZATKO, Danielle, S. , WHITE, James, F. , ZACHER, Alan, H.
发明人： FRYE, John, G. , HOLLADAY, Johnathan, E. , MUZATKO, Danielle, S. , WHITE, James, F. , ZACHER, Alan, H.
IPC分类号： B01J23/46 , B01J23/60 , B01J23/62 , B01J23/89 , C07C29/00
CPC分类号： B01J23/626 , B01J23/462 , B01J23/464 , B01J23/466 , B01J23/48 , B01J23/60 , B01J23/62 , B01J23/628 , B01J23/6447 , B01J23/656 , B01J23/80 , B01J23/85 , B01J23/889 , B01J23/89 , B01J23/8906 , B01J23/8926 , B01J23/8986 , B01J27/045 , B01J27/0576 , B01J37/18 , C07C29/60 , C07C31/205
摘要： A reduction catalyst having a first metal component comprising one of Co, Os, Fe, Re, Rh and Ru. The first metal component is present in the catalyst at from 0.5 percent to 20 percent, by weight. A second metal component differing from the first metal component present in the catalyst with the second metal component being selected from the group consisting of Fe, Mn, Ru, Os, Rh, Ir, Ni, Pd, Pt, Ag, Au, Zn, Co, Re, Cu, Pb, Cr, W, Mo, Sn, Nb, Cd, Te, V, Bi, Ga and Na. A hydrogenation catalyst comprising one or both of Ni and Co and one or more elements selected from the group consisting of Mn, Fe, Ag, Au, Mo and Rh.
摘要翻译：一种具有包含Co，Os，Fe，Re，Rh和Ru中的一种的第一金属组分的还原催化剂。催化剂中第一种金属组分以重量百分比为0.5％至20％存在。不同于催化剂中存在的第一金属组分的第二金属组分，其中第二金属组分选自Fe，Mn，Ru，Os，Rh，Ir，Ni，Pd，Pt，Ag，Au，Zn， Co，Re，Cu，Pb，Cr，W，Mo，Sn，Nb，Cd，Te，V，Bi，Ga及Na。包含Ni和Co中的一种或两种以及选自Mn，Fe，Ag，Au，Mo和Rh中的一种或多种元素的氢化催化剂。

2. 发明申请

WO2007106100A1 METHOD AND APPARATUS FOR CONVERSION OF β -HYDROXY CARBONYL COMPOUNDS 审中-公开
标题翻译：用于转化β-羟基碳化合物的方法和装置
公开(公告)号：WO2007106100A1
公开(公告)日：2007-09-20
申请号：PCT/US2006/012697
申请日：2006-04-04
申请人： BATTELLE MEMORIAL INSTITUTE , CARGILL, INCORPORATED , ZACHER, Alan, H. , HOLLADAY, Johnathan, E. , LILGA, Michael, A. , WHITE, James, F. , MUZATKO, Danielle, S. , ORTH, Rick, J. , TSOBANAKIS, Paraskevas , MENG, Xiangsheng , ABRAHAM, Timothy, W.
发明人： ZACHER, Alan, H. , HOLLADAY, Johnathan, E. , LILGA, Michael, A. , WHITE, James, F. , MUZATKO, Danielle, S. , ORTH, Rick, J. , TSOBANAKIS, Paraskevas , MENG, Xiangsheng , ABRAHAM, Timothy, W.
IPC分类号： C07C57/065 , C07C231/12
CPC分类号： C07C51/377 , C07C57/04
摘要： A process and apparatus are disclosed for conversion of β-hydroxy carbonyl compounds forming useful conversion products including, e.g., acrylic acid [CAS No. 79-10-7], acrylates, and acrylamide [CAS No. 79-06-01]. Conversion products find use, e.g., as feedstock and/or end-use chemicals.
摘要翻译：公开了用于转化形成有用转化产物的β-羟基羰基化合物的方法和装置，包括例如丙烯酸[CAS No.79-10-7]，丙烯酸酯和丙烯酰胺[CAS No.79-06-01]。转化产物可用作例如原料和/或最终用途的化学品。

3. 发明申请

WO2007106099A1 METHOD FOR THE PREPARATION OF ALPHA-BETA-UNSATURATED CARBONYL COMPOUNDS 审中-公开
标题翻译：制备阿尔法 - 不饱和碳化合物的方法
公开(公告)号：WO2007106099A1
公开(公告)日：2007-09-20
申请号：PCT/US2006/012696
申请日：2006-04-04
申请人： BATTELLE MEMORIAL INSTITUTE , CARGILL INCORPORATED , HOLLADAY, Johnathan, E. , ZACHER, Alan, H. , LILGA, Michael, A. , WHITE, James, F. , MUZATKO, Danielle, S. , ORTH, Rick, J. , TSOBANAKIS, Paraskevas , MENG, Xiangsheng , ABRAHAM, Timothy, W.
发明人： HOLLADAY, Johnathan, E. , ZACHER, Alan, H. , LILGA, Michael, A. , WHITE, James, F. , MUZATKO, Danielle, S. , ORTH, Rick, J. , TSOBANAKIS, Paraskevas , MENG, Xiangsheng , ABRAHAM, Timothy, W.
IPC分类号： C07C51/377 , C07C57/04
CPC分类号： C07C231/14 , C07C51/377 , Y02P20/127 , C07C57/04 , C07C233/09
摘要： A process is disclosed for conversion of ammonium salts of β-hydroxy carbonyl compounds forming useful conversion products including, e.g., α, β-unsaturated carbonyl compounds and/or ammonium salts of α, β-unsaturated carbonyl compounds recovered at a high molar yield. Conversion products find use, e.g., as feedstock and/or end-use chemicals.
摘要翻译：公开了用于转化形成有用转化产物的β-羟基羰基化合物的铵盐的方法，包括例如以高摩尔收率回收的β-不饱和羰基化合物和/或β-不饱和羰基化合物的铵盐。转化产物可用于例如原料和/或最终用途的化学品。

4. 发明申请

WO2009129325A2 HYDROGENOLYSIS PROCESSES AND HYDROGENOLYSIS CATALYST PREPARATION METHODS 审中-公开
标题翻译：氢化方法和氢化催化剂制备方法
公开(公告)号：WO2009129325A2
公开(公告)日：2009-10-22
申请号：PCT/US2009/040695
申请日：2009-04-15
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Johnathan, E. , WHITE, James, F. , PETERSON, Thomas, H. , FRYE, John, G. , MUZATKO, Danielle, S. , BARE, Simon, R. , VASSILAKIS, James, G. , ROSIN, Richard, R.
发明人： HOLLADAY, Johnathan, E. , WHITE, James, F. , PETERSON, Thomas, H. , FRYE, John, G. , MUZATKO, Danielle, S. , BARE, Simon, R. , VASSILAKIS, James, G. , ROSIN, Richard, R.
IPC分类号： B01J21/18 , B01J23/889 , B01J23/89 , B01J37/18 , C07C17/23
CPC分类号： B01J21/18 , B01J23/8896 , B01J23/8986 , B01J37/18
摘要： Hyd rogenolysis processes are p rovided that can include providing a hyd rogenolysis reactor havin g a catalyst therein. Th e catalyst can be exposed to a reducing agent in the absence of polyhyd ric alcohol co mpou nd wh ile maintain in g a temperature of the catalyst above 290°C. Hydrogenolysis processes can also include providing a passivated catalyst to within a reactor and exposin g th e catalyst to a reducing atmosphere wh ile mai ntain ing the catalyst at a temperatu re less than 210°C. Hyd rogenolysis catalyst preparation methods are p rovided that can incl ude exposin g the catalyst to a f i rst red ucing atmosphere wh ile maintai ning the catalyst at a f i rst temperatu re to reduce at least a portion of the catalyst. Th e method can also incl ude passivati ng at least the portion of the catalyst and depassivatin g the po rtion of the catalyst in the presence of a second reducing atmosphere while maintaining the portion of the catalyst at a second temperatu re less than the f i rst temperatu re.
摘要翻译：水解法分解过程包括提供含有催化剂的水解酶反应器。催化剂可以在不存在多元醇的情况下暴露于还原剂，保持在290℃以上的催化剂温度。氢解方法还可以包括在反应器内提供钝化的催化剂，并将催化剂暴露于温度低于210℃的催化剂中的还原气氛中。水解催化剂的制备方法可以包括将催化剂暴露于在第一个温度下首先还原催化剂的至少一部分催化剂的第一个红色环境。这种方法还可以包括至少部分催化剂的钝化，并在第二还原气氛存在的情况下使催化剂沉淀，同时保持催化剂部分的第二温度低于第一个温暖的

5. 发明申请

WO2004058708A1 PROCESS FOR PRODUCING N-METHYL SUCCINIMIDE 审中-公开
标题翻译：生产N-甲基磺酰胺的方法
公开(公告)号：WO2004058708A1
公开(公告)日：2004-07-15
申请号：PCT/US2003/040106
申请日：2003-12-16
申请人： BATTELLE MEMORIAL INSTITUTE , WERPY, Todd, A. , FRYE, John, G., Jr. , WHITE, James, F. , HOLLADAY, Johnathan, E. , ZACHER, Alan, H.
发明人： WERPY, Todd, A. , FRYE, John, G., Jr. , WHITE, James, F. , HOLLADAY, Johnathan, E. , ZACHER, Alan, H.
IPC分类号： C07D207/40
CPC分类号： C07D207/404 , C07D207/267
摘要： The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkyating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Amonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100 °C to about 400 °C to produce N-methyl succinimide which is purified and hydrogenated to form NMP.
摘要翻译：本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。本发明包括生产N-烷基产物的方法。调节溶液的阿莫尼亚含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。加入烷基化剂并将该初始化合物烷基化并环化。本发明包括制备N-甲基吡咯烷酮（NMP）的方法。将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。甲基化剂与琥珀酸盐在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

6. 发明申请

WO2007146836A1 HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL 审中-公开
标题翻译：羟丙基纤维素还原方法及其制备方法
公开(公告)号：WO2007146836A1
公开(公告)日：2007-12-21
申请号：PCT/US2007/070802
申请日：2007-06-08
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA, Michael, A. , HALLEN, Richard, T. , WERPY, Todd, A. , WHITE, James, F. , HOLLADAY, Johnathan, E. , FRYE, John, G. , ZACHER, Alan, H.
发明人： LILGA, Michael, A. , HALLEN, Richard, T. , WERPY, Todd, A. , WHITE, James, F. , HOLLADAY, Johnathan, E. , FRYE, John, G. , ZACHER, Alan, H.
IPC分类号： C07D307/12 , C07D307/40
CPC分类号： C07D307/12 , C07D307/40
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H 2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250°C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H 2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30°C. A method of producing tetrahydofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh中的至少一种金属的催化剂接触，温度小于或等于250℃。氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

7. 发明申请

WO2009129256A1 PROCESSES AND SYSTEMS FOR PRODUCING PRODUCTS OF HYDROGENOLYSIS OF POLYHYDRIC ALCOHOLS 审中-公开
标题翻译：生产多元醇的氢化产物的方法和系统
公开(公告)号：WO2009129256A1
公开(公告)日：2009-10-22
申请号：PCT/US2009/040551
申请日：2009-04-14
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Johnathan, E. , MUZATKO, Danielle, S. , WHITE, James, F. , ZACHLER, Alan, H.
发明人： HOLLADAY, Johnathan, E. , MUZATKO, Danielle, S. , WHITE, James, F. , ZACHLER, Alan, H.
IPC分类号： C07C29/60 , C07C31/20
CPC分类号： C07C29/132 , C07C29/60 , C07C31/205
摘要： Hydrogenolysis systems are provided that can include a reactor housing an Ru-comprising hydrogenolysis catalyst and wherein the contents of the reactor is maintained at a neutral or acidic pH. Reactant reservoirs within the system can include a polyhydric alcohol compound and a base, wherein a weight ratio of the base to the compound is less than 0.05. Systems also include the product reservoir comprising a hydrogenolyzed polyhydric alcohol compound and salts of organic acids, and wherein the moles of base are substantially equivalent to the moles of salts or organic acids. Processes are provided that can include an Ru-comprising catalyst within a mixture having a neutral or acidic pH. A weight ratio of the base to the compound can be between 0.01 and 0.05 during exposing.
摘要翻译：提供了氢解系统，其可以包括容纳含Ru的氢解催化剂的反应器，并且其中反应器的内容物保持在中性或酸性pH。系统内的反应物储存器可以包括多元醇化合物和碱，其中碱与化合物的重量比小于0.05。系统还包括包含氢解的多元醇化合物和有机酸的盐的产物储存器，其中碱的摩尔数基本上等于盐或有机酸的摩尔数。提供了可以在具有中性或酸性pH的混合物中包含含Ru的催化剂的方法。在曝光期间，碱与化合物的重量比可以在0.01和0.05之间。

8. 发明申请

WO2009029540A2 CHEMICAL PRODUCTION PROCESSES, SYSTEMS, AND CATALYST COMPOSITIONS 审中-公开
标题翻译：化学生产过程，系统和催化剂组合物
公开(公告)号：WO2009029540A2
公开(公告)日：2009-03-05
申请号：PCT/US2008/074090
申请日：2008-08-22
申请人： BATTELLE MEMORIAL INSTITUTE , PETERSON, Thomas, H. , HOLLADAY, Johnathan, E. , ZACHER, Alan, H. , GRAY, Michel, J. , WERPY, Todd, A. , WHITE, James, F.
发明人： PETERSON, Thomas, H. , HOLLADAY, Johnathan, E. , ZACHER, Alan, H. , GRAY, Michel, J. , WERPY, Todd, A. , WHITE, James, F.
IPC分类号： C07C45/52 , C07C47/22 , B01J27/16
CPC分类号： C07C45/52 , C07C49/17 , C07C47/22
摘要： Chemical production processes are provided that include exposing a reactant composition to a catalyst composition to form a product composition, with the reactant composition including a multihydric alcohol compound and the catalyst composition being effective to dehydrate at least a portion of the multihydric alcohol compound. Embodiments of the process provide that the reactant composition is exposed to the catalyst composition for less than about 0.25 seconds and/or that the catalyst is maintained at a temperature of from about 2800C to about 3200C. Processes utilizing a reactant composition including a multihydric alcohol compound and an inert compound are also provided.
摘要翻译：提供了化学生产方法，其包括将反应物组合物暴露于催化剂组合物以形成产物组合物，反应物组合物包含多元醇化合物，催化剂组合物有效地使至少一部分多元醇化合物脱水。该方法的实施方案提供反应物组合物暴露于催化剂组合物少于约0.25秒和/或催化剂保持在约2800℃至约3200℃的温度。还提供了利用包含多元醇化合物和惰性化合物的反应物组合物的方法。

9. 发明申请

WO2009029541A1 DEHYDRATION PRODUCTION PROCESS, SYSTEM, AND CATALYST COMPOSITIONS 审中-公开
标题翻译：脱水生产过程，系统和催化剂组合物
公开(公告)号：WO2009029541A1
公开(公告)日：2009-03-05
申请号：PCT/US2008/074094
申请日：2008-08-22
申请人： BATTELLE MEMORIAL INSTITUTE , PETERSON, Thomas, H. , ZACHER, Alan, H. , GRAY, Michel, J. , WHITE, James, F. , HOLLADAY, Johnathan, E. , WERPY, Todd, A.
发明人： PETERSON, Thomas, H. , ZACHER, Alan, H. , GRAY, Michel, J. , WHITE, James, F. , HOLLADAY, Johnathan, E. , WERPY, Todd, A.
IPC分类号： C07C45/52 , B01J23/20 , B01J23/24 , B01J27/188 , B01J27/195
CPC分类号： B01J27/188 , B01J8/025 , B01J23/20 , B01J23/24 , B01J23/34 , B01J23/8474 , B01J27/195 , B01J37/0236 , B01J2208/00212 , B01J2208/00256 , C07C45/52 , C07C47/22
摘要： Chemical production processes are provided than can include exposing a reactant composition to a catalyst composition to form a product composition, with the reactant composition including a multihydric alcohol compound and product composition including a carbonyl compound. The catalyst composition can include one or more elements of groups 5 and 6 of the periodic table of elements. Catalyst compositions are provided that can include one or more of niobia, hydrated niobia, tungstic acid, phosphotungstic acid, and phosphomolybdic acid.
摘要翻译：提供化学生产方法可以包括将反应物组合物暴露于催化剂组合物以形成产物组合物，反应物组合物包含多元醇化合物和包含羰基化合物的产物组合物。催化剂组合物可以包括元素周期表第5和6族的一个或多个元素。提供的催化剂组合物可以包括铌，氧化铌，钨酸，磷钨酸和磷钼酸中的一种或多种。

10. 发明申请

WO2007089526A1 METHOD OF PERFORMING SUGAR DEHYDRATION AND CATALYST TREATMENT 审中-公开
标题翻译：执行糖脱水和催化处理的方法
公开(公告)号：WO2007089526A1
公开(公告)日：2007-08-09
申请号：PCT/US2007/001995
申请日：2007-01-25
申请人： BATTELLE MEMORIAL INSTITUTE , HU, Jianli , HOLLADAY, Johnathan, E. , ZHANG, Xinjie , WANG, Yong
发明人： HU, Jianli , HOLLADAY, Johnathan, E. , ZHANG, Xinjie , WANG, Yong
IPC分类号： C07H1/00
CPC分类号： C07H1/00
摘要： The invention includes a method of treating a solid acid catalyst. After exposing the catalyst to a mixture containing a sugar alcohol, the catalyst is washed with an organic solvent and is then exposed to a second reaction mixture. The invention includes a process for production of anhydrosugar alcohol. A solid acid catalyst is provided to convert sugar alcohol in a first sample to an anhydrosugar alcohol. The catalyst is then washed with an organic solvent and is subsequently utilized to expose a second sample. The invention includes a method for selective production of an anhydrosugar. A solid acid catalyst is provided within a reactor and anhydrosugar alcohol is formed by flowing a starting sugar alcohol into the reactor. The acid catalyst is then exposed to an organic solvent which allows a greater amount of additional anhydrosugar to be produced than would occur without exposing the acid catalyst to the organic solvent.
摘要翻译：本发明包括一种处理固体酸催化剂的方法。在将催化剂暴露于含有糖醇的混合物之后，将催化剂用有机溶剂洗涤，然后暴露于第二反应混合物。本发明包括生产脱水葡萄糖醇的方法。提供固体酸催化剂以将第一样品中的糖醇转化成脱水葡萄糖醇。然后将催化剂用有机溶剂洗涤，随后用于暴露第二个样品。本发明包括选择性生产脱水糖的方法。在反应器内提供固体酸催化剂，并通过将起始糖醇流入反应器而形成脱水葡萄糖醇。然后将酸催化剂暴露于有机溶剂，其允许比不会将酸催化剂暴露于有机溶剂的情况下产生更多量的额外的脱水糖。

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