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1. 发明申请

WO2009087362A3 METHOD FOR THE PRODUCTION OF SUCRALOSE 审中-公开
标题翻译：用于生产蔗糖的方法
公开(公告)号：WO2009087362A3
公开(公告)日：2009-09-17
申请号：PCT/GB2009000006
申请日：2009-01-02
申请人： BAIADA ANTHONY , CAMBORIEUX SEBASTIEN , JANSEN ROBERT , KERR JOHN , LEINHOS DUANE , MAFFEZONI CARLO , WALKER GORDON , WILEY JAMES EDWIN , TATE & LYLE TECHNOLOGY LTD
发明人： BAIADA ANTHONY , CAMBORIEUX SEBASTIEN , JANSEN ROBERT , KERR JOHN , LEINHOS DUANE , MAFFEZONI CARLO , WALKER GORDON , WILEY JAMES EDWIN
IPC分类号： C07H1/06 , C07H5/02
CPC分类号： C07H1/06 , C07H5/02
摘要： The present invention provides a method for producing sucralose from a feed stream resulting from the chlorination of a sucrose-6-acylate in a reaction vehicle, said feed stream comprising a sucralose-6-acylate, the reaction vehicle, water, and salts, said salts including one or more selected from the group consisting of alkali metal or alkaline earth metal chlorides and ammonium chloride, wherein said method comprises: (i) deacylation of the sucralose-6-acylate by treatment with a base to afford a product stream comprising sucralose; (ii) partial removal of water and, optionally, reaction vehicle from the product stream of (i) in order to cause precipitation of the salts from the product stream; (iii) removal of the precipitated salts from the product stream of (ii); and (iv) isolation of sucralose from the product stream of (iii).
摘要翻译：本发明提供了由反应媒介物中蔗糖-6-酰化物氯化产生的进料流生产三氯半乳蔗糖的方法，所述进料流包含三氯半乳蔗糖-6-酰化物，反应介质，水和盐，所述包括选自碱金属或碱土金属氯化物和氯化铵中的一种或多种的盐，其中所述方法包括：（i）通过用碱处理使三氯半乳蔗糖-6-酰化物脱酰化以提供包含三氯半乳蔗糖的产物流 ; （ii）从（i）的产物流中部分除去水和任选的反应媒介物，以便使盐从产物流中沉淀出来; （iii）从（ii）的产物流中除去沉淀的盐; 和（iv）从（iii）的产物流中分离三氯半乳蔗糖。

2. 发明专利

GB2469157B Process for removing dimethylamine during sucralose production 未知
公开(公告)号：GB2469157B
公开(公告)日：2011-07-06
申请号：GB0918691
申请日：2009-10-23
申请人： KERR JOHN , JANSEN ROBERT , BAIADA ANTHONY , LEINHOS DUANE , WILEY JAMES EDWIN , TATE & LYLE TECHNOLOGY LTD
发明人： KERR JOHN , JANSEN ROBERT , BAIADA ANTHONY , LEINHOS DUANE , WILEY JAMES EDWIN
IPC分类号： C07H5/02
摘要： A process for removing dimethylamine (DMA) before and/or during and/or after deacylation in a reaction vessel of a feed stream comprising a sucralose-6-acylate resulting from the chlorination of a sucrose-6-acylate in the presence of dimethyl formamide (DMF), wherein the deacylation is conducted at a first set of conditions of temperature, pH and pressure, the process comprising: (a) providing a side stream loop from and to the reaction vessel; (b) adjusting the conditions of one or more of temperature, pH, and pressure in the loop, and setting the flow rate through the loop, to remove DMA while minimising carbohydrate degradation.

3. 发明专利

GB2469157A Process for the removal of dimethylamine in the manufacture of sucralose 未知
公开(公告)号：GB2469157A
公开(公告)日：2010-10-06
申请号：GB0918691
申请日：2009-10-23
申请人： KERR JOHN , JANSEN ROBERT , BAIADA ANTHONY , LEINHOS DUANE , WILEY JAMES EDWIN , TATE & LYLE TECHNOLOGY LTD
发明人： KERR JOHN , JANSEN ROBERT , BAIADA ANTHONY , LEINHOS DUANE , WILEY JAMES EDWIN
IPC分类号： C07H5/02
摘要： A process for removing dimethylamine (DMA) before and/or during and/or after deacylation in a reaction vessel of a feed stream comprising a sucralose-6-acylate resulting from the chlorination of a sucrose-6-acylate in the presence of dimethyl formamide (DMF), wherein the deacylation is conducted at a first set of conditions of temperature, pH and pressure, the process comprising:(a) providing a side stream loop from and to the reaction vessel;(b) adjusting the conditions of one or more of temperature, pH, and pressure in the loop, and setting the flow rate through the loop, to remove DMA while minimising carbohydrate degradation.

4. 发明申请

WO2009137192A3 PURIFICATION OF SUCRALOSE CONTAINING FEED STREAMS FOR SUCRALOSE CRYSTALLIZATION 审中-公开
标题翻译：含有包含进料溶液的SUCRALOSE进行硫化结晶的纯化
公开(公告)号：WO2009137192A3
公开(公告)日：2010-02-11
申请号：PCT/US2009039099
申请日：2009-04-01
申请人： TATE & LYLE TECHNOLOGY LTD , WILEY JAMES EDWIN JR , KERR JOHN , JANSEN ROBERT , WALKER GORDON
发明人： WILEY JAMES EDWIN JR , KERR JOHN , JANSEN ROBERT , WALKER GORDON
IPC分类号： C07H1/06 , C07H5/02
CPC分类号： C07H1/06 , C07H5/02
摘要： A process for the recovery of a carbohydrate selected from sucralose and sucralose-6-esters from an aqueous feed stream is disclosed. The process comprises extracting the feed stream with an organic solvent, such as ethyl acetate, back extracting the resulting carbohydrate-containing organic extract with an aqueous solvent, and either crystallizing the carbohydrate from the organic solvent or replacing the organic solvent with water and crystallizing the carbohydrate from water. The process results in an increased overall yield of the carbohydrate.
摘要翻译：公开了从含水进料流中回收选自三氯蔗糖和三氯蔗糖-6-酯的碳水化合物的方法。该方法包括用有机溶剂如乙酸乙酯萃取进料流，用水溶剂反萃取所得含碳水化合物的有机萃取物，并将碳水化合物从有机溶剂中结晶或用水代替有机溶剂，并使来自水的碳水化合物该方法导致碳水化合物的总收率提高。

5. 发明申请

WO2006119206A3 GRAIN WET MILLING PROCESS FOR PRODUCING ETHANOL 审中-公开
标题翻译：用于生产乙醇的颗粒磨细工艺
公开(公告)号：WO2006119206A3
公开(公告)日：2007-01-11
申请号：PCT/US2006016661
申请日：2006-05-02
申请人： TATE & LYLE INGREDIENTS , JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTIEN
发明人： JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTIEN
IPC分类号： A23L7/10 , C12P7/10 , C12R1/865
CPC分类号： C12P7/06 , Y02E50/16 , Y02E50/17
摘要： Whole grain, such as wheat, barley, rye, and/or rice, can be processed by (a) steeping the grain in aqueous liquid to produce softened grain, (b) milling the softened grain to produce milled grain, (c) liquefying the milled grain by contacting it with amylase and heating it to a temperature of at least about 50°C, producing a liquefied material, (d) at least partially saccharifying the liquefied material by contacting it with amyloglucosidase at a temperature of at least about 50°C, producing a first saccharified material, and (e) separating fiber and germ from the first saccharified material, producing a screened material that is substantially free of fiber and germ. The process also includes the steps of (f) further saccharifying and fermenting the screened material with a microorganism that produces ethanol, thereby producing a broth that comprises ethanol, soluble protein, and insoluble protein, and (g) separating ethanol from the broth. A protein-rich product can be recovered from the broth that comprises both gluten from the grain and microorganism from the fermenting step.
摘要翻译：可以通过（a）在水性液体中浸渍谷物以产生软化的谷物，（b）研磨软化的谷物以产生碾磨的谷物，（c）液化（例如，麦粒，大麦，黑麦和/或米）研磨的颗粒通过使其与淀粉酶接触并将其加热至至少约50℃的温度，产生液化材料，（d）至少部分地使液化材料与淀粉葡糖苷酶接触，其中所述液化物质与至少约50℃的温度产生第一糖化材料，和（e）从第一糖化物质分离纤维和胚芽，产生基本上不含纤维和细菌的筛选材料。该方法还包括以下步骤：（f）用生产乙醇的微生物进一步对筛选的材料进行糖化和发酵，从而产生包含乙醇，可溶性蛋白质和不溶性蛋白质的肉汤，和（g）从肉汤中分离乙醇。富含蛋白质的产物可以从含有谷物的谷蛋白和发酵步骤的微生物的肉汤中回收。

6. 发明申请

WO2008097878A2 IMPROVED SUCROSE INVERSION PROCESS 审中-公开
标题翻译：改进的SUCROSE反转过程
公开(公告)号：WO2008097878A2
公开(公告)日：2008-08-14
申请号：PCT/US2008052877
申请日：2008-02-04
申请人： TATE & LYLE INGREDIENTS , JANSEN ROBERT , KERR JOHN , BAIADA ANTHONY
发明人： JANSEN ROBERT , KERR JOHN , BAIADA ANTHONY
IPC分类号： C13B20/14 , C13K3/00 , C13B35/06
CPC分类号： C13K3/00 , C13B20/14
摘要： We disclose a method of inverting sucrose, including (i) determining an initial solids concentration of an aqueous sucrose solution (SoHdS1), an initial bed volume (BV1) of a sucrose inversion resin system, a minimum target inversion percentage (invert%min), a maximum target inversion percentage (invert%max), a target maximum hydroxymethylfuran (HMF) concentration (HMFmdX), a minimum target pH (pHmm), or a maximum target pH (pHmax); (ii) contacting the sucrose inversion resin system with the aqueous sucrose solution under conditions of aqueous solution flow rate in BV,/hr (ratep) and aqueous solution temperature in 0C (temperaturep) to produce an inverted sucrose solution having an inversion percentage (invert%product), an HMF concentration (HMFprocduct), and a pH (pHproduct); (iii) observing an instantaneous inversion percentage (invert%m!>t), an instantaneous HMF concentration (HMFmst), or an instantaneous pH (pHmst) of the inverted sucrose solution; and, if invert%m,t invert%max, HMFm%t > HMFmax, pHmst pHmax; (iv) changing at least one of the aqueous solution flow rate or the aqueous solution temperature such that invert%mm
摘要翻译：我们公开了蔗糖反转的方法，包括（i）测定蔗糖反相树脂体系的初始固体浓度（SoHdS1），初始床体积（BV1），最小目标反转百分比（反转百分比），最大目标反转百分比（反转百分比最大值），目标最大羟甲基呋喃浓度（HMFmdX），最小目标pH（pHmm）或最大目标pH（pHmax））; （ii）在水溶液流速BV，/ hr（速率）和0℃（温度p）的水溶液温度条件下，将蔗糖反转树脂体系与蔗糖水溶液接触，得到反转百分比反转蔗糖溶液％产品），HMF浓度（HMFprocduct）和pH（pH值））。（iii）观察反转蔗糖溶液的瞬时反转百分比（反相％m> t），瞬时HMF浓度（HMFmst）或瞬时pH（pHmst）; 并且如果反转％m，t <反转％mm，反转％m％t>反相％max，HMFm％t> HMFmax，pHmst pHmax; （iv）改变水溶液流速或水溶液温度中的至少一个，使得转换百分比mm <反转％piodUct =反转％max，HMFprodllct = HMF1113x或pHimu

7. 发明申请

WO2006119217A2 GRAIN WET MILLING PROCESS FOR PRODUCING DEXTROSE 审中-公开
标题翻译：用于生产甜味剂的谷物湿法生产工艺
公开(公告)号：WO2006119217A2
公开(公告)日：2006-11-09
申请号：PCT/US2006016679
申请日：2006-05-02
申请人： TATE & LYLE INGREDIENTS , JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTEIN
发明人： JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTEIN
IPC分类号： A23J1/12 , A23J3/18 , A23J3/34 , A23K1/14 , C13B20/14 , C13K1/08
CPC分类号： C12Y302/00 , A23J1/125 , A23J3/18 , A23K10/30 , A23K20/179 , A23K50/80 , A23L7/104 , A23L29/35 , C13B20/142 , C13K1/08 , Y02A40/818
摘要： Whole grain, such as wheat, barley, rye, and/or rice, can be processed by (a) steeping the grain or at least partially dehulled grain in an aqueous liquid to produce softened grain, (b) milling the softened grain to produce milled grain, (c) liquefying the milled grain by contacting it with amylase and heating it to a temperature of at least about 5O°C, producing a liquefied material, (d) at least partially saccharifying the liquefied material by contacting it with amyloglucosidase at a temperature of at least about 5O°C, producing a first saccharified material, and (e) separating fiber and germ from the first saccharified material, producing a screened material that is substantially free of fiber and wheat germ. The process also includes the steps of (f) further saccharifying the screened material by contacting it with amyloglucosidase at a temperature of at least about 5O°C, producing a second saccharified material, (g) membrane filtering the second saccharified material, producing a permeate that comprises primarily dextrose and other soluble components and a retentate that comprises insoluble protein, and (h) purifying the permeate by chromatographic separation, producing a purified dextrose stream. The chromatographic separation can also produce a raffinate, and the process can further include the steps of (i) combining the retentate from the membrane filtration and the raffinate from the chromatographic separation to form a fermentation medium, (j) fermenting the fermentation medium aerobically with a microorganism, (k) separating a protein product that comprises insoluble protein and microorganism from the medium, and (1) drying the protein product.
摘要翻译：可以通过（a）在水性液体中浸渍颗粒或至少部分脱壳的颗粒以产生软化的颗粒，（b）研磨软化的颗粒以产生（例如，小麦，大麦，黑麦和/或米）磨碎的谷物，（c）通过使其与淀粉酶接触并将其加热至至少约50℃的温度来液化碾磨的谷粒，产生液化物质，（d）至少部分地使液化物质与淀粉葡糖苷酶接触，至少约50℃的温度，产生第一糖化物质，和（e）从第一糖化物质分离纤维和胚芽，产生基本上不含纤维和小麦胚芽的筛选材料。该方法还包括以下步骤：（f）通过使筛选的材料与淀粉葡糖苷酶在至少约50℃的温度下接触进一步糖化，产生第二糖化物质，（g）膜过滤第二糖化物质，产生渗透物其主要包括葡萄糖和其他可溶性组分以及包含不溶性蛋白质的渗余物，和（h）通过色谱分离纯化渗透物，产生纯化的葡萄糖流。色谱分离还可以产生萃余液，并且该方法还可以包括以下步骤：（i）将来自膜过滤的残留物和来自色谱分离的萃余液组合以形成发酵培养基，（j）有氧地发酵发酵培养基，微生物，（k）从培养基中分离含有不溶性蛋白质和微生物的蛋白质产物，（1）干燥蛋白质产物。

8. 发明申请

WO2007015741A3 CORN WET MILLING PROCESS 审中-公开
标题翻译：玉米湿磨工艺
公开(公告)号：WO2007015741A3
公开(公告)日：2007-12-06
申请号：PCT/US2006027296
申请日：2006-07-14
申请人： TATE & LYLE INGREDIENTS , JANSEN ROBERT , SASS DAVID , WALKER GORDON , LUTZ ERIC
发明人： JANSEN ROBERT , SASS DAVID , WALKER GORDON , LUTZ ERIC
IPC分类号： A23L1/105 , A23J1/12 , A23K1/00 , A23L1/308 , C13K1/06 , C13K1/08
CPC分类号： A23K20/163 , A23J1/12 , A23K10/37 , A23L7/104 , A23L29/35 , A23L33/22 , Y02P60/877
摘要： A corn wet-milling process comprises steeping corn kernels in an aqueous liquid, which produces softened corn; milling the softened corn in a first mill, which produces a first milled corn; separating germ from the first milled corn, thereby producing a germ-depleted first milled corn; milling the germ-depleted first milled corn in a second mill, producing a second milled corn; separating the second milled corn into a first starch/protein portion that comprises starch and protein and a first fiber portion that comprises fiber, starch, and protein; milling the first fiber portion in a third mill, which produces a milled fiber material that comprises fiber, starch, ' and protein; separating at least some of the starch and protein in the milled fiber material from the fiber therein, producing a second fiber portion that comprises fiber and starch and a second starch/protein portion that comprises starch and protein; and contacting the second fiber portion with at least one enzyme to convert at least some of the starch therein to dextrose. The converted material is screened using one or more screens to separate the fiber from the liquor. The liquor can be fermented to ethanol, or refined to dextrose. The fiber can be pressed and dried as an animal feed.
摘要翻译：玉米湿磨工艺包括将玉米粒浸渍在水性液体中，其产生软化的玉米; 在第一磨机中磨碎软化的玉米，其产生第一磨碎的玉米; 从第一个研磨的玉米中分离胚芽，由此产生消耗细菌的第一个研磨的玉米; 在第二研磨机中研磨消毒的第一研磨玉米，产生第二研磨玉米; 将第二研磨玉米分离成包含淀粉和蛋白质的第一淀粉/蛋白质部分和包含纤维，淀粉和蛋白质的第一纤维部分; 在第三研磨机中研磨第一纤维部分，其产生包含纤维，淀粉和蛋白质的研磨纤维材料; 将碾磨的纤维材料中的至少一些淀粉和蛋白质与其中的纤维分离，产生包含纤维和淀粉的第二纤维部分和包含淀粉和蛋白质的第二淀粉/蛋白质部分; 和使第二纤维部分与至少一种酶接触以将其中的至少一些淀粉转化为右旋糖。使用一个或多个筛网筛选转化的材料以从液体中分离纤维。酒可以发酵成乙醇，或精制成右旋糖。纤维可以作为动物饲料压制和干燥。

9. 发明申请

WO2009094418A3 CORN WET MILLING PROCESS 审中-公开
公开(公告)号：WO2009094418A3
公开(公告)日：2010-04-01
申请号：PCT/US2009031652
申请日：2009-01-22
申请人： TATE AND LYLE INGREDIENTS AMER , JANSEN ROBERT , KERR JOHN , JONES PETER-LLOYD , TANNER RICHARD
发明人： JANSEN ROBERT , KERR JOHN , JONES PETER-LLOYD , TANNER RICHARD
IPC分类号： C08B30/04 , C12P7/08 , C12P19/20 , C13K1/06
CPC分类号： C13K1/06 , C08B30/044 , C12P7/06 , C12P19/14 , Y02E50/17
摘要： A corn wet-milling process comprises steeping corn kernels in an aqueous liquid, which produces softened corn; milling the softened corn in a first mill, which produces a first milled corn; separating germ from the first milled corn, thereby producing a germ-depleted first milled corn; milling the germ-depleted first milled corn in a second mill, producing a second milled corn; separating the second milled corn into a first starch/protein portion that comprises starch and protein and a first fiber portion that comprises fiber, starch, and protein; milling the first fiber portion in a third mill, which produces a milled fiber material that comprises fiber, starch, and protein; separating at least some of the starch and protein in the milled fiber material from the fiber therein, producing a second fiber portion that comprises fiber and starch and a second starch/protein portion that comprises starch and protein; and contacting the second fiber portion with at least one enzyme to convert at least some of the starch therein to dextrose. The converted material is screened using one or more screens to separate the fiber from the liquor. The liquor can be fermented to ethanol, or refined to dextrose. The fiber can be pressed and dried as an animal feed.
摘要翻译：玉米湿法研磨方法包括在含水液体中浸泡玉米粒，产生软化的玉米; 在第一磨机中研磨软化的玉米，其生产第一研磨的玉米; 将胚芽与第一磨碎的玉米分离，从而产生一种无菌的第一磨碎的玉米; 在第二磨机中研磨灭菌的第一批玉米，生产第二批玉米; 将第二研磨的玉米分离成包含淀粉和蛋白质的第一淀粉/蛋白质部分和包含纤维，淀粉和蛋白质的第一纤维部分; 在第三磨机中研磨第一纤维部分，其产生包含纤维，淀粉和蛋白质的研磨纤维材料; 将磨碎的纤维材料中的至少一些淀粉和蛋白质与其中的纤维分离，产生包含纤维和淀粉的第二纤维部分和包含淀粉和蛋白质的第二淀粉/蛋白质部分; 以及使所述第二纤维部分与至少一种酶接触以将其中的至少一些淀粉转化成葡萄糖。使用一个或多个筛网筛选转化的材料以将纤维与液体分离。酒可以发酵成乙醇，或精制成葡萄糖。纤维可以作为动物饲料被压制和干燥。

10. 发明申请

WO2009020740A3 IMPROVED PROCESS FOR EFFICIENT ENERGY RECOVERY FROM BIOMASS 审中-公开
标题翻译：改进生物质能源回收方法
公开(公告)号：WO2009020740A3
公开(公告)日：2010-11-18
申请号：PCT/US2008070067
申请日：2008-07-15
申请人： TATE AND LYLE INGREDIENTS AMER , GANGA RAYMOND C , IMIG GREG , MCBURNEY BLAKE , JANSEN ROBERT , KERR JOHN , REUST STEVEN J
发明人： GANGA RAYMOND C , IMIG GREG , MCBURNEY BLAKE , JANSEN ROBERT , KERR JOHN , REUST STEVEN J
IPC分类号： F23G5/12 , F23G5/46 , F23G7/10 , F23J7/00
CPC分类号： F23G7/10 , F23G5/12 , F23G5/46 , F23G2202/106 , F23G2206/20 , F23G2900/00001 , F23G2900/7012 , F23J7/00
摘要： A method for extracting energy from biomass depleted of at least some carbohydrate, at least some oil, or both by a) introducing the biomass into a vertically elongated combustion chamber having i) at least one suspension burner at the top of the combustion chamber which is capable of projecting a flame down the axis of the combustion chamber, ii) a heat transfer apparatus having at least a portion of a heat collection surface located radially from the flame and below the burner, and iii) an exhaust opening located below the flame and below at least a portion of the heat collection surface; b) combusting the biomass to yield a mixture containing hot flue gas and molten ash above the exhaust opening; c) transferring heat from the hot flue gas to at least a portion of the heat collection surface substantially by radiation prior to any substantial contact of ash to a surface of the combustion chamber, to yield a mixture containing warm flue gas and non-molten ash and having a lower molten ash content than the mixture yielded by the combusting step; and d) cooling the warm flue gas with cold gas, to yield a mixture containing cool flue gas and non-molten ash and having a lower molten ash content than the mixture yielded by the transferring step.
摘要翻译：一种用于从生物量中提取能量的方法，该方法是通过以下步骤从至少一些碳水化合物，至少一些油或两者中消耗的能量：a）将生物质引入垂直细长的燃烧室，所述燃烧室具有：i）在燃烧室顶部的至少一个悬浮燃烧器，能够沿着燃烧室的轴线向下突出火焰，ii）传热装置，其具有位于燃烧器的径向与火焰之下的集热表面的至少一部分，以及iii）位于火焰下方的排气口，在集热面的至少一部分的下方; b）燃烧生物质以产生在排气口上方含有热烟道气和熔融灰渣的混合物; c）在灰分与燃烧室的任何实质接触之前，基本上通过辐射将热量从热烟道气传递到至少一部分集热表面，以产生含有热烟气和非熔融灰的混合物并且具有比通过燃烧步骤产生的混合物更低的熔融灰分含量; 和d）用冷气体冷却暖烟道气，得到含有冷烟道气和非熔融灰分的混合物，其熔融灰分含量低于转移步骤产生的混合物。

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