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1. 发明申请

WO2009087362A3 METHOD FOR THE PRODUCTION OF SUCRALOSE 审中-公开
标题翻译：用于生产蔗糖的方法
公开(公告)号：WO2009087362A3
公开(公告)日：2009-09-17
申请号：PCT/GB2009000006
申请日：2009-01-02
申请人： BAIADA ANTHONY , CAMBORIEUX SEBASTIEN , JANSEN ROBERT , KERR JOHN , LEINHOS DUANE , MAFFEZONI CARLO , WALKER GORDON , WILEY JAMES EDWIN , TATE & LYLE TECHNOLOGY LTD
发明人： BAIADA ANTHONY , CAMBORIEUX SEBASTIEN , JANSEN ROBERT , KERR JOHN , LEINHOS DUANE , MAFFEZONI CARLO , WALKER GORDON , WILEY JAMES EDWIN
IPC分类号： C07H1/06 , C07H5/02
CPC分类号： C07H1/06 , C07H5/02
摘要： The present invention provides a method for producing sucralose from a feed stream resulting from the chlorination of a sucrose-6-acylate in a reaction vehicle, said feed stream comprising a sucralose-6-acylate, the reaction vehicle, water, and salts, said salts including one or more selected from the group consisting of alkali metal or alkaline earth metal chlorides and ammonium chloride, wherein said method comprises: (i) deacylation of the sucralose-6-acylate by treatment with a base to afford a product stream comprising sucralose; (ii) partial removal of water and, optionally, reaction vehicle from the product stream of (i) in order to cause precipitation of the salts from the product stream; (iii) removal of the precipitated salts from the product stream of (ii); and (iv) isolation of sucralose from the product stream of (iii).
摘要翻译：本发明提供了由反应媒介物中蔗糖-6-酰化物氯化产生的进料流生产三氯半乳蔗糖的方法，所述进料流包含三氯半乳蔗糖-6-酰化物，反应介质，水和盐，所述包括选自碱金属或碱土金属氯化物和氯化铵中的一种或多种的盐，其中所述方法包括：（i）通过用碱处理使三氯半乳蔗糖-6-酰化物脱酰化以提供包含三氯半乳蔗糖的产物流 ; （ii）从（i）的产物流中部分除去水和任选的反应媒介物，以便使盐从产物流中沉淀出来; （iii）从（ii）的产物流中除去沉淀的盐; 和（iv）从（iii）的产物流中分离三氯半乳蔗糖。

2. 发明申请

WO2006119206A3 GRAIN WET MILLING PROCESS FOR PRODUCING ETHANOL 审中-公开
标题翻译：用于生产乙醇的颗粒磨细工艺
公开(公告)号：WO2006119206A3
公开(公告)日：2007-01-11
申请号：PCT/US2006016661
申请日：2006-05-02
申请人： TATE & LYLE INGREDIENTS , JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTIEN
发明人： JANSEN ROBERT , KERR JOHN , FARLEY EDWARD , WALKER GORDON , CAMBORIEUX SEBASTIEN
IPC分类号： A23L7/10 , C12P7/10 , C12R1/865
CPC分类号： C12P7/06 , Y02E50/16 , Y02E50/17
摘要： Whole grain, such as wheat, barley, rye, and/or rice, can be processed by (a) steeping the grain in aqueous liquid to produce softened grain, (b) milling the softened grain to produce milled grain, (c) liquefying the milled grain by contacting it with amylase and heating it to a temperature of at least about 50°C, producing a liquefied material, (d) at least partially saccharifying the liquefied material by contacting it with amyloglucosidase at a temperature of at least about 50°C, producing a first saccharified material, and (e) separating fiber and germ from the first saccharified material, producing a screened material that is substantially free of fiber and germ. The process also includes the steps of (f) further saccharifying and fermenting the screened material with a microorganism that produces ethanol, thereby producing a broth that comprises ethanol, soluble protein, and insoluble protein, and (g) separating ethanol from the broth. A protein-rich product can be recovered from the broth that comprises both gluten from the grain and microorganism from the fermenting step.
摘要翻译：可以通过（a）在水性液体中浸渍谷物以产生软化的谷物，（b）研磨软化的谷物以产生碾磨的谷物，（c）液化（例如，麦粒，大麦，黑麦和/或米）研磨的颗粒通过使其与淀粉酶接触并将其加热至至少约50℃的温度，产生液化材料，（d）至少部分地使液化材料与淀粉葡糖苷酶接触，其中所述液化物质与至少约50℃的温度产生第一糖化材料，和（e）从第一糖化物质分离纤维和胚芽，产生基本上不含纤维和细菌的筛选材料。该方法还包括以下步骤：（f）用生产乙醇的微生物进一步对筛选的材料进行糖化和发酵，从而产生包含乙醇，可溶性蛋白质和不溶性蛋白质的肉汤，和（g）从肉汤中分离乙醇。富含蛋白质的产物可以从含有谷物的谷蛋白和发酵步骤的微生物的肉汤中回收。

3. 发明专利

BRPI0806922A2 未知
公开(公告)号：BRPI0806922A2
公开(公告)日：2014-04-29
申请号：BRPI0806922
申请日：2008-01-18
申请人： TATE & LYLE TECHNOLOGY LTD
发明人： LEINHOS DUANE , KERR JOHN , JANSEN BOB , CAMBORIEUX SEBASTIEN , BAIADA ANTHONY , LLOYD-JONES PETER
IPC分类号： C07H5/02
摘要： There is provided a method for the production of sucralose from a feed stream resulting from the chlorination of a sucrose-6-acylate in a reaction vehicle, said feed stream comprising a sucralose-6-acylate, the reaction vehicle, and by-products including high molecular weight coloured material, said method comprising: deacylation of the sucralose-6-acylate by treatment with a base to afford sucralose, and, before or after said deacylation, removal of the reaction vehicle and isolation of the sucralose characterised in that immediately before the removal of the reaction vehicle, the reaction stream is subjected to a precipitation step comprising treatment with a metal or ammonium hydroxide and carbon dioxide to form a precipitate of the corresponding metal or ammonium carbonate in which at least a portion of said high molecular weight coloured material is trapped, followed by separation of said precipitate.

4. 发明专利

CA2675526A1 IMPROVED SUCRALOSE PRODUCTION METHOD 未知
公开(公告)号：CA2675526A1
公开(公告)日：2008-07-24
申请号：CA2675526
申请日：2008-01-18
申请人： TATE & LYLE TECHNOLOGY LTD
发明人： KERR JOHN , LEINHOS DUANE , JANSEN BOB , CAMBORIEUX SEBASTIEN , BAIADA ANTHONY , LLOYD-JONES PETER
IPC分类号： C07H5/02
摘要： There is provided a method for the production of sucralose from a feed st ream resulting from the chlorination of a sucrose-6-acylate in a reaction ve hicle, said feed stream comprising a sucralose-6-acylate, the reaction vehic le, and by-products including high molecular weight coloured material, said method comprising: deacylation of the sucralose-6-acylate by treatment with a base to afford sucralose, and, before or after said deacylation, removal o f the reaction vehicle and isolation of the sucralose characterised in that immediately before the removal of the reaction vehicle, the reaction stream is subjected to a precipitation step comprising treatment with a metal or am monium hydroxide and carbon dioxide to form a precipitate of the correspondi ng metal or ammonium carbonate in which at least a portion of said high mole cular weight coloured material is trapped, followed by separation of said pr ecipitate.

5. 发明专利

NZ578741A Improved sucralose production method 未知
公开(公告)号：NZ578741A
公开(公告)日：2010-12-24
申请号：NZ57874108
申请日：2008-01-18
申请人： TATE & LYLE TECHNOLOGY LTD
发明人： LEINHOS DUANE , KERR JOHN , JANSEN BOB , CAMBORIEUX SEBASTIEN , BAIADA ANTHONY , LLOYD-JONES PETER
IPC分类号： C07H5/02
摘要： Disclosed is a method for the production of sucralose from a feed stream resulting from the chlorination of a sucrose-6-acylate in a reaction vehicle, said feed stream comprising a sucralose-6-acylate, the reaction vehicle, and by-products including high molecular weight coloured material, said method comprising: deacylation of the sucralose-6-acylate by treatment with a base to afford sucralose, and, before or after said deacylation, removal of the reaction vehicle, and isolation of the sucralose, wherein immediately before the removal of the reaction vehicle, the reaction stream is subjected to a precipitation step comprising treatment with a metal or ammonium hydroxide and carbon dioxide to form a precipitate of the corresponding metal or ammonium carbonate in which at least a portion of said high molecular weight coloured material is trapped, followed by separation of said precipitate. Also disclosed is the sucralose product produced by the above method.

6. 发明专利

MX2009007578A METODO MEJORADO DE PRODUCCION DE SUCRALOSA. 未知
公开(公告)号：MX2009007578A
公开(公告)日：2009-07-22
申请号：MX2009007578
申请日：2008-01-18
申请人： TATE & LYLE TECHNOLOGY LTD
发明人： BAIADA ANTHONY , LEINHOS DUANE , KERR JOHN , JANSEN BOB , CAMBORIEUX SEBASTIEN , LLOYD-JONES PETER
IPC分类号： C07H5/02
摘要： Se proporciona un método para la producción de sucralosa a partir de una corriente de alimentación que resulta de la cloración de sucrosa-6-acilato en un vehículo de reacción, la corriente de alimentación comprende sucralosa-6-acilato, vehículo de reacción y subproductos que incluyen material coloreado de alto peso molecular, el método comprende: la desacilación de sucralosa-6-acilato por tratamiento con una base para producir la sucralosa, y, antes o después de la desacilación, la eliminación del vehículo de reacción y aislamiento de sucralosa caracterizado en que inmediatamente antes de la eliminación del vehículo de reacción, la corriente de reacción se somete a una etapa de precipitación que comprende el tratamiento con un hidróxido de amonio o metal para formar un precipitado de carbonato de amonio o metal correspondiente en el cual por lo menos una porción de material coloreado de alto peso molecular se retiene, seguido por la separación del precipitado.

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