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1. 发明授权

US06455219B1 Semicontinuous emulsion polymerization process for making silica-containing latex for toners 失效
标题翻译：用于制造调色剂的二氧化硅胶乳的半连续乳液聚合方法
公开(公告)号：US06455219B1
公开(公告)日：2002-09-24
申请号：US09885957
申请日：2001-06-22
申请人： Allan K. Chen , Tie Hwee Ng , Arthur Helbrecht , Kimberly D. Nosella , Danielle C. Boils-Boissier , Paul J. Gerroir , Rosa M. Duque
发明人： Allan K. Chen , Tie Hwee Ng , Arthur Helbrecht , Kimberly D. Nosella , Danielle C. Boils-Boissier , Paul J. Gerroir , Rosa M. Duque
IPC分类号： G03G500
CPC分类号： C08K3/36 , C08F2/44 , G03G9/0806 , G03G9/09716 , G03G9/09725
摘要： A process for making silica-containing latex particles involves polymerizing monomer in an emulsion comprising the monomer, water, silica particles, and optionally at least one surfactant, by adding at least one free radical initiator to the emulsion to form the silica-containing latex particles. In a preferred method, semicontinuous polymerization employing a seed latex is used to form the latex resin. The process achieves a silica-containing latex in which the silica is chemically incorporated therein that is ideally suited for use in the manufacture of toner and developer for xerographic use.
摘要翻译：制造含二氧化硅的胶乳颗粒的方法包括通过在乳液中加入至少一种自由基引发剂来形成含二氧化硅的胶乳颗粒，在包含单体，水，二氧化硅颗粒和任选的至少一种表面活性剂的乳液中聚合单体。在优选的方法中，使用使用种子胶乳的半连续聚合来形成胶乳树脂。该方法实现了含二氧化硅的胶乳，其中二氧化硅化学地掺入其中，其理想地适用于制造用于静电印刷使用的调色剂和显影剂。

2. 发明授权

US06664018B2 In-situ method of forming zinc stearate dispersion and use thereof in toners 失效
公开(公告)号：US06664018B2
公开(公告)日：2003-12-16
申请号：US10063428
申请日：2002-04-23
申请人： Allan K. Chen , Tie Hwee Ng , Lu Jiang , Kimberly D. Nosella , Paul J. Gerroir , Michael Damato
发明人： Allan K. Chen , Tie Hwee Ng , Lu Jiang , Kimberly D. Nosella , Paul J. Gerroir , Michael Damato
IPC分类号： G03G500
CPC分类号： G03G9/09791
摘要： A method of forming an aqueous dispersion of particles of zinc stearate includes the steps of forming a mixture of at least one surfactant and water, heating the mixture to a temperature of from about 40° C. to less than a melting temperature of zinc stearate, adding a metal-containing stearate to the mixture under agitation, adding to the mixture a solution of a zinc salt in water, whereby upon inclusion of both the metal-containing stearate and the zinc salt in the mixture, the zinc salt reacts with the metal-containing stearate to form the particles of zinc stearate, continuing the heating and agitation following completion of the latter of the adding of the solution of zinc salt or the adding of the metal-containing stearate to continue the reaction, and cooling to obtain the aqueous dispersion of particles of zinc stearate. The method forms a stable aqueous dispersion of nanometer sized zinc stearate particles particularly useful in coating toner particles.

3. 发明申请

US20110097665A1 TONER PARTICLES AND COLD HOMOGENIZATION METHOD 有权
标题翻译：调色剂颗粒和冷均匀方法
公开(公告)号：US20110097665A1
公开(公告)日：2011-04-28
申请号：US12604040
申请日：2009-10-22
申请人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , Melanie L. Davis
发明人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , Melanie L. Davis
IPC分类号： G03G9/08
CPC分类号： G03G9/0804 , G03G9/0812 , G03G9/0819 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A method of making toner particles, including cold homogenizing at a temperature below room temperature a resin emulsion, a colorant, an optional wax, and optional additives with a coagulant to form a toner slurry; heating the toner slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles.
摘要翻译：一种制备调色剂颗粒的方法，包括在低于室温的温度下冷均质树脂乳液，着色剂，任选的蜡和任选的添加剂与凝结剂形成调色剂浆料; 加热调色剂浆料以形成聚集的调色剂颗粒; 将浆料中的颗粒冻结一次，以期望的聚集粒度; 并且进一步加热浆料中的聚集颗粒以将聚集的颗粒聚结成调色剂颗粒。

4. 发明授权

US08486602B2 Toner particles and cold homogenization method 有权
标题翻译：调色剂颗粒和冷均质化方法
公开(公告)号：US08486602B2
公开(公告)日：2013-07-16
申请号：US12604040
申请日：2009-10-22
申请人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , Melanie L. Davis
发明人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , Melanie L. Davis
IPC分类号： G03G9/08
CPC分类号： G03G9/0804 , G03G9/0812 , G03G9/0819 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A method of making toner particles, including cold homogenizing at a temperature below room temperature a resin emulsion, a colorant, an optional wax, and optional additives with a coagulant to form a toner slurry; heating the toner slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles.
摘要翻译：一种制备调色剂颗粒的方法，包括在低于室温的温度下冷均质树脂乳液，着色剂，任选的蜡和任选的添加剂与凝结剂形成调色剂浆料; 加热调色剂浆料以形成聚集的调色剂颗粒; 将浆料中的颗粒冻结一次，以期望的聚集粒度; 并且进一步加热浆料中的聚集颗粒以将聚集的颗粒聚结成调色剂颗粒。

5. 发明授权

US07977025B2 Emulsion aggregation methods 有权
标题翻译：乳液聚集方法
公开(公告)号：US07977025B2
公开(公告)日：2011-07-12
申请号：US12629996
申请日：2009-12-03
申请人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , David Kurceba , Shigang Qiu , Santiago Faucher
发明人： Kimberly D. Nosella , Tie Hwee Ng , Allan K. Chen , Abdisamed Sheik-Qasim , David Kurceba , Shigang Qiu , Santiago Faucher
IPC分类号： G03G9/08
CPC分类号： G03G9/0819 , G03G9/0806 , G03G9/0827 , G03G9/08755 , G03G9/08797
摘要： A method of making toner particles, including: mixing, at less than about 17° C. and without homogenizing, a resin emulsion with a coagulant, a colorant, an optional wax, and optional additives, to form pre-aggregated particles in a slurry; heating the slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles.
摘要翻译：一种制备调色剂颗粒的方法，包括：在低于约17℃下混合树脂乳液与凝结剂，着色剂，任选的蜡和任选的添加剂，以在浆料中形成预凝聚颗粒 ; 加热浆料以形成聚集的调色剂颗粒; 将浆料中的颗粒冻结一次，以期望的聚集粒度; 并且进一步加热浆料中的聚集颗粒以将聚集的颗粒聚结成调色剂颗粒。

6. 发明授权

US06447974B1 Polymerization processes 失效
标题翻译：聚合工艺
公开(公告)号：US06447974B1
公开(公告)日：2002-09-10
申请号：US09896293
申请日：2001-07-02
申请人： Allan K. Chen , George Liebermann , Tie Hwee Ng , Arthur Helbrecht , Abdisamed Sheik-qasim , David Kurceba , Chieh-Min Cheng , Emily L. Moore
发明人： Allan K. Chen , George Liebermann , Tie Hwee Ng , Arthur Helbrecht , Abdisamed Sheik-qasim , David Kurceba , Chieh-Min Cheng , Emily L. Moore
IPC分类号： G03G9093
CPC分类号： G03G9/0806
摘要： A process for the preparation of a latex polymer by (i) preparing or providing a water aqueous phase containing an anionic surfactant in an optional amount of less than or equal to about 20 percent by weight of the total amount of anionic surfactant used in forming the latex polymer; (ii) preparing or providing a monomer emulsion in water which emulsion contains an anionic surfactant; (iii) adding about 50 percent or less of said monomer emulsion to said aqueous phase to thereby initiate seed polymerization and to form a seed polymer, said aqueous phase containing a free radical initiator; and (iv) adding the remaining percent of said monomer emulsion to the composition of (iii) and heating to complete an emulsion polymerization thus forming a latex polymer.
摘要翻译：一种制备胶乳聚合物的方法，该方法是（i）制备或提供含有阴离子表面活性剂的水相，其任选量小于或等于形成所述阴离子表面活性剂所用阴离子表面活性剂的总量的约20重量％胶乳聚合物;（ii）在水中制备或提供单体乳液，该乳液含有阴离子表面活性剂;（iii）向所述水相中加入约50％或更少的所述单体乳液，从而引发种子聚合并形成种子聚合物，所述水相含有自由基引发剂; 和（iv）将所述单体乳液的剩余百分比加入到（iii）的组合物中并加热以完成乳液聚合，从而形成胶乳聚合物。

7. 发明授权

US06503680B1 Latex processes 失效
标题翻译：乳胶工艺
公开(公告)号：US06503680B1
公开(公告)日：2003-01-07
申请号：US09940926
申请日：2001-08-29
申请人： Allan K. Chen , George Liebermann , Tie Hwee Ng , Arthur Helbrecht , Emily L. Moore , Abdisamed Sheik-qasim , Patricia A. Burns , Nam S. Ro
发明人： Allan K. Chen , George Liebermann , Tie Hwee Ng , Arthur Helbrecht , Emily L. Moore , Abdisamed Sheik-qasim , Patricia A. Burns , Nam S. Ro
IPC分类号： G03G9087
CPC分类号： G03G9/08702 , C08F291/00 , G03G9/0806 , G03G9/081 , C08F2/22
摘要： A process for the preparation of a latex polymer consistent with E/A (emulsion/aggregation/coalescence) toner manufacture. The process utilizes a standard (universal) latex composition and involves chain-transfer agent partitioning, emulsion polymerization that provides a latex polymer with a wide range of molecular properties. In particular, the process customizes a wide range Mw (weight average molecular weight) latex, without substantially varying the Mn (number average molecular weight) and hence, without substantially varying Tg (glass transition temperature) such that good toner performance is maintained. In a preferred process, a latex polymer is prepared by mixing a seed particle latex, generated by aqueous emulsion polymerization of a first portion of a monomer emulsion, with a second portion of the monomer emulsion and at least one chain-transfer agent. The mixing is done in the presence of a free-radical initiator and heated, and wherein the monomer emulsion comprises a mixture of polymerization reagents of at least one monomer, at least one chain-transfer agent, at least one surfactant, and water. This process may be applied to core-shell polymerization as well. These latex polymers are ideally suited in the manufacture of toner and developer for electrophotographic imaging and printing.
摘要翻译：制备与E / A（乳液/聚集/聚结）调色剂制造一致的胶乳聚合物的方法。该方法使用标准（通用）胶乳组合物，并涉及链转移剂分配，乳液聚合，其提供具有广泛分子性质的胶乳聚合物。特别地，该方法定制了宽范围的Mw（重均分子量）胶乳，而基本上不改变Mn（数均分子量），因此没有实质上改变的Tg（玻璃化转变温度），使得维持良好的调色剂性能。在优选的方法中，通过混合通过单体乳液的第一部分的水乳液聚合产生的种子颗粒胶乳与第二部分单体乳液和至少一种链转移剂来制备胶乳聚合物。混合在自由基引发剂的存在下进行并加热，其中单体乳液包含至少一种单体，至少一种链转移剂，至少一种表面活性剂和水的聚合试剂的混合物。该方法也可以应用于核 - 壳聚合。这些胶乳聚合物非常适用于制造用于电子照相成像和印刷的调色剂和显影剂。

8. 发明授权

US09201324B2 Processes for producing polyester latexes via solvent-based and solvent-free emulsification 有权
标题翻译：通过溶剂型和无溶剂乳化法生产聚酯胶乳的方法
公开(公告)号：US09201324B2
公开(公告)日：2015-12-01
申请号：US12707693
申请日：2010-02-18
申请人： Shigang S. Qiu , Kimberly D. Nosella , Tie Hwee Ng , Santiago Faucher , Fumii Higuchi
发明人： Shigang S. Qiu , Kimberly D. Nosella , Tie Hwee Ng , Santiago Faucher , Fumii Higuchi
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/0827 , G03G9/08 , G03G9/0806 , G03G9/0819 , G03G9/087 , G03G9/08755 , G03G9/08795 , G03G9/08797 , G03G9/09733
摘要： A process for making a latex emulsion suitable for use in a toner composition includes contacting at least one polyester resin optionally with an organic solvent to form a resin mixture, adding a primary amine, optionally a surfactant, and deionized water to the mixture.
摘要翻译：制备适用于调色剂组合物的胶乳乳液的方法包括将至少一种聚酯树脂任选地与有机溶剂接触以形成树脂混合物，向混合物中加入伯胺，任选的表面活性剂和去离子水。

9. 发明申请

US20120308925A1 Hyperpigmented black low melt toner 审中-公开
标题翻译：色素沉着黑色低熔融碳粉
公开(公告)号：US20120308925A1
公开(公告)日：2012-12-06
申请号：US13118483
申请日：2011-05-30
申请人： Daryl W. Vanbesien , Magid Kamel , Cuong Vong , Suxia Yang , Kimberly D. Nosella , Richard P.N. Veregin , Tie Hwee Ng
发明人： Daryl W. Vanbesien , Magid Kamel , Cuong Vong , Suxia Yang , Kimberly D. Nosella , Richard P.N. Veregin , Tie Hwee Ng
IPC分类号： G03G9/09
摘要： The present disclosure describes a hyperpigmented low melt black toner containing a thermal carbon black which exhibits reduced dielectric loss and improved tribo charging.
摘要翻译：本公开内容描述了一种色素沉着的含有热炭黑的低熔点黑色调色剂，其表现出降低的介电损耗和改进的摩擦带电。

10. 发明申请

US20110200930A1 PROCESSES FOR PRODUCING POLYESTER LATEXES VIA SOLVENT-BASED AND SOLVENT-FREE EMULSIFICATION 有权
标题翻译：通过溶剂型和无溶剂型生产聚酯酯类的方法
公开(公告)号：US20110200930A1
公开(公告)日：2011-08-18
申请号：US12707693
申请日：2010-02-18
申请人： Shigang S. Qiu , Kimberly D. Nosella , Tie Hwee Ng , Santiago Faucher , Fumii Higuchi
发明人： Shigang S. Qiu , Kimberly D. Nosella , Tie Hwee Ng , Santiago Faucher , Fumii Higuchi
IPC分类号： G03G9/08 , C08G63/00 , G03G9/087
CPC分类号： G03G9/0827 , G03G9/08 , G03G9/0806 , G03G9/0819 , G03G9/087 , G03G9/08755 , G03G9/08795 , G03G9/08797 , G03G9/09733
摘要： A process for making a latex emulsion suitable for use in a toner composition includes contacting at least one polyester resin optionally with an organic solvent to form a resin mixture, adding a primary amine, optionally a surfactant, and deionized water to the mixture.
摘要翻译：制备适用于调色剂组合物的胶乳乳液的方法包括将至少一种聚酯树脂任选地与有机溶剂接触以形成树脂混合物，向混合物中加入伯胺，任选的表面活性剂和去离子水。

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