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1. 发明授权

US4292141A Isolation of butadiene from a C.sub.4 -hydrocarbon mixture 失效
标题翻译：从C4烃混合物中分离丁二烯
公开(公告)号：US4292141A
公开(公告)日：1981-09-29
申请号：US68741
申请日：1979-08-22
申请人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner , Dieter Pommer , Klaus-Juergen Schneider , Harald Schwentker
发明人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner , Dieter Pommer , Klaus-Juergen Schneider , Harald Schwentker
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C11/167 , C07C67/00 , B01D3/40
CPC分类号： C07C7/005
摘要： A process for isolating butadiene, with the aid of a selective solvent, from a C.sub.4 -hydrocarbon mixture which contains butadiene and small amounts of styrene and may contain oxygen, hydrocarbons more soluble than butadiene in the selective solvent and hydrocarbons less soluble than butadiene in the selective solvent, in which process the C.sub.4 -hydrocarbon mixture is separated by extractive distillation into a distillate which contains the less soluble hydrocarbons, a stream of butadiene and a stream containing the more soluble hydrocarbons, and in which a mixture of styrene and C.sub.4 -hydrocarbons is removed from the C.sub.4 -hydrocarbon mixture in a distillation zone upstream of the extractive distillation, the top product of the said distillation zone being fed to the extractive distillation.
摘要翻译：在选择性溶剂的帮助下，从含有丁二烯和少量苯乙烯的C4-烃混合物中分离丁二烯的方法，并且可以含有氧，在选择性溶剂中比丁二烯更可溶的烃和比丁二烯更难溶解的烃选择性溶剂，其中C4烃混合物通过萃取蒸馏分离成含有较少可溶性烃的馏出物，丁二烯流和含有较可溶性烃的物流，其中苯乙烯和C 4烃的混合物在萃取蒸馏上游的蒸馏区中从C4烃混合物中除去，将所述蒸馏区的顶部产物进料至萃取蒸馏。

2. 发明授权

US4310388A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 hydrocarbon 失效
标题翻译：从C4-或C5烃分离共轭二烯烃
公开(公告)号：US4310388A
公开(公告)日：1982-01-12
申请号：US126898
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
发明人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 50 to 99 percent by weight of a selective solvent boiling at from 140.degree. C. to 260.degree. C. and(b) from 1 to 50 percent by weight of an organic solvent boiling at from 45.degree. C. to 125.degree. C.
摘要翻译：一种通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）50 至99重量％的在140℃至260℃沸腾的选择性溶剂和（b）1至50重量％的沸点为45℃至125℃的有机溶剂。

3. 发明授权

US4277315A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C4或C5烃混合物中分离共轭二烯烃
公开(公告)号：US4277315A
公开(公告)日：1981-07-07
申请号：US126897
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
发明人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 1 to 99 percent by weight of an N-alkyl-substituted lower aliphatic acid amide or of an N-alkyl-substituted alicyclic acid amide having 5 ring members and(b) from 1 to 99 percent by weight of an lower aliphatic carboxylic acid ester or carbonic acid ester boiling at from 30.degree. C. to 200.degree. C.
摘要翻译：通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）1 至99重量％的N-烷基取代的低级脂肪酸酰胺或具有5个环成员的N-烷基取代的脂环酸酰胺和（b）1至99重量％的低级脂族羧酸酯或碳酸酯在30〜200℃下沸腾。

4. 发明授权

US4647344A Recovery of isoprene from a C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C5烃混合物中回收异戊二烯
公开(公告)号：US4647344A
公开(公告)日：1987-03-03
申请号：US662602
申请日：1984-10-19
申请人： Alfred Lindner , Ulrich Wagner , Klaus Volkamer , Walter Rebafka
发明人： Alfred Lindner , Ulrich Wagner , Klaus Volkamer , Walter Rebafka
IPC分类号： C07B61/00 , C07C1/00 , C07C7/08 , C07C7/10 , C07C7/163 , C07C11/18 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08 , C07C7/10 , Y10S203/20
摘要： Isoprene is recovered from a C.sub.5 -hydrocarbon mixture containing isoprene, penta-1,3-diene and cyclopentadiene by separating the said mixture by liquid-liquid extraction or extractive distillation with the aid of a selective solvent, in combination with a distillation upstream or downstream from the liquid-liquid extraction or extractive distillation, by a method in which a stream containing penta-1,3-diene and cyclopentadiene is separated off in the upstream or downstream distillation and is catalytically hydrogenated, and the hydrogenated stream is fed to the upper part of the liquid-liquid extraction or extractive distillation.
摘要翻译：通过使用选择性溶剂的液 - 液萃取或萃取蒸馏分离所述混合物，与上游或下游的蒸馏相结合，从含有异戊二烯，五-1,3-二烯和环戊二烯的C5-烃混合物回收异戊二烯从液 - 液萃取或萃取蒸馏中，通过在上游或下游蒸馏中分离出含有五-1,3-二烯和环戊二烯的物流并进行催化氢化的方法，并将氢化流进料至上层液体萃取或萃取蒸馏的一部分。

5. 发明授权

US4277314A Isolation of 1,3-butadiene from a C4-hydrocarbon mixture 失效
标题翻译：从C4烃混合物中分离出1,3-丁二烯
公开(公告)号：US4277314A
公开(公告)日：1981-07-07
申请号：US40283
申请日：1979-05-18
申请人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
发明人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C7/05 , C07C11/167 , C07C67/00 , B01D3/40
CPC分类号： C07C7/005 , C07C7/05
摘要： A process for isolating 1,3-butadiene by means of a selective solvent from a C.sub.4 -hydrocarbon mixture which contains 1,3-butadiene, propyne, hydrocarbons which are more soluble than 1,3-butadiene in the selective solvent and hydrocarbons which are less soluble than 1,3-butadiene in the selective solvent, wherein the C.sub.4 -hydrocarbon mixture is separated, using one or more extractive distillation zones, into a distillate containing the less soluble hydrocarbons, a stream of 1,3-butadiene and a stream containing the more soluble hydrocarbons, and the propyne is separated off either by distillation of the C.sub.4 -hydrocarbon mixture in a distillation zone upstream of the extractive distillation zone or zones or by distillation of the stream of 1,3-butadiene, obtained from the extractive distillation zone or zones, in a downstream distillation zone, giving a stream of hydrocarbons containing propyne and 1,3-butadiene, which stream is fed to an additional distillation zone, while at the same time a second stream of liquid or gaseous hydrocarbons is fed to the additional distillation zone, and the bottom product from the additional distillation zone is recycled to the extractive distillation.
摘要翻译：通过选择性溶剂从含有1,3-丁二烯，丙炔，在选择性溶剂中比1,3-丁二烯更可溶的烃的C 4烃混合物分离1,3-丁二烯的方法和烃，其为在选择性溶剂中比1,3-丁二烯更难溶解，其中使用一个或多个萃取蒸馏区将C4-烃混合物分离成含有较不溶性烃的馏出物，1,3-丁二烯流和流含有较多的可溶性烃，丙炔通过在萃取蒸馏区或蒸馏区上游的蒸馏区中蒸馏出C4烃混合物，或通过蒸馏萃取物获得的1,3-丁二烯来分离。蒸馏区或区域，在下游蒸馏区中，产生含有丙炔和1,3-丁二烯的烃流，该料流被供给到另外的蒸馏区，同时a 液体或气态烃的第二流进料到另外的蒸馏区，并且来自附加蒸馏区的底部产物被再循环至萃取蒸馏。

6. 发明授权

US4448643A Isolation of isobutene from C.sub.4 -hydrocarbon mixtures containing isobutene 失效
标题翻译：从含有异丁烯的C4烃混合物中分离异丁烯
公开(公告)号：US4448643A
公开(公告)日：1984-05-15
申请号：US282746
申请日：1981-07-13
申请人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
发明人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
IPC分类号： C07C1/00 , C07C7/148 , C07C11/09 , C07C41/06 , C07C41/44 , C07C67/00 , B01D3/32
CPC分类号： C07C41/44 , C07C41/06 , C07C7/14891 , Y10S203/06 , Y10S203/20
摘要： A process for isolating isobutene from C.sub.4 -hydrocarbon mixtures containing isobutene by reacting the mixture with a primary alcohol in the presence of an acid condensing agent, to form the tertiary ether, separating off the unconverted hydrocarbons and decomposing the tertiary ether in the presence of an acid catalyst at an elevated temperature, wherein a primary C.sub.3 - or C.sub.4 -alcohol is used and the temperature at which the reaction mixture leaves the etherification stage, in which the tertiary ether is formed, is lower than the mean temperature in the etherification stage.
摘要翻译：一种通过在酸缩合剂的存在下使该混合物与伯醇反应来分离含有异丁烯的C 4烃混合物的异丁烯的方法，以形成叔乙醚，分离出未转化的烃并在存在下分解叔乙醚酸催化剂，其中使用初级C3-或C4-醇，并且反应混合物离开形成叔乙醚的醚化阶段的温度低于醚化阶段的平均温度。

7. 发明授权

US4278504A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C4或C5烃混合物中分离共轭二烯烃
公开(公告)号：US4278504A
公开(公告)日：1981-07-14
申请号：US126903
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Brollos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Jurgen Schneider
发明人： Klaus Volkamer , Klaus Brollos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Jurgen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 1 to 99 percent by weight of an N-alkyl-substituted lower aliphatic acid amide or of an N-alkyl-substituted alicyclic acid amide having 5 ring members and(b) from 1 to 99 percent by weight of an aliphatic or alicyclic ether boiling at from 30.degree. C. to 200.degree. C.
摘要翻译：通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）1 至99重量％的N-烷基取代的低级脂肪酸酰胺或具有5个环成员的N-烷基取代的脂环族酰胺酰胺，和（b）1至99重量％的沸腾的脂族或脂环族醚从30℃至200℃

8. 发明授权

US4320232A Process for conjointly preparing methyl tert.-butyl ether and obtaining isobutene 失效
标题翻译：共同制备甲基叔丁基醚并获得异丁烯的方法
公开(公告)号：US4320232A
公开(公告)日：1982-03-16
申请号：US161041
申请日：1980-06-19
申请人： Klaus Volkamer , Alfred Lindner , Franz Merger , Ulrich Wagner , Erwin Brunner , Gerhard Sandrock , Max Strohmeyer
发明人： Klaus Volkamer , Alfred Lindner , Franz Merger , Ulrich Wagner , Erwin Brunner , Gerhard Sandrock , Max Strohmeyer
IPC分类号： C07C41/05 , C07C1/00 , C07C7/148 , C07C11/09 , C07C41/00 , C07C41/06 , C07C43/04 , C07C67/00
CPC分类号： C07C41/06 , C07C7/14891
摘要： A process for conjointly preparing methyl tert.-butyl ether and obtaining isobutene from an isobutene-containing C.sub.4 -hydrocarbon mixture. In the process the C.sub.4 -hydrocarbon mixture is reacted, in one or more etherification stages, with methanol and a primary C.sub.3 - or C.sub.4 -alcohol in the presence of an acid condensing agent, the resulting reaction mixture or mixtures are then separated into a fraction containing the unconverted hydrocarbons, the methyl tert.-butyl ether and a fraction containing the C.sub.3 - or C.sub.4 -alkyl tert.-butyl ether. Thereafter, the C.sub.3 - or C.sub.4 -alkyl tert.-butyl ether is decomposed at an elevated temperature, in the presence of an acid catalyst, into isobutene and primary C.sub.3 - or C.sub.4 -alcohol.
摘要翻译：一种联合制备甲基叔丁基醚并从含异丁烯的C4-烃混合物中获得异丁烯的方法。在该过程中，C4-烃混合物在一个或多个醚化阶段中，在酸缩合剂存在下与甲醇和伯C3或C4-醇反应，然后将所得反应混合物或混合物分离成馏分含有未转化的烃，甲基叔丁基醚和含有C3-或C4-烷基叔丁基醚的级分。此后，C3-或C4-烷基叔丁基醚在酸催化剂存在下在升高的温度下分解成异丁烯和伯C 3 - 或C 4 - 醇。

9. 发明授权

US4237330A Isolation of butadiene from a C.sub.4 -hydrocarbon mixture 失效
标题翻译：从C4烃混合物中分离丁二烯
公开(公告)号：US4237330A
公开(公告)日：1980-12-02
申请号：US44029
申请日：1979-05-31
申请人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
发明人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C11/167 , C07C67/00
CPC分类号： C07C7/005
摘要： A process for isolating butadiene by means of a selective solvent from a C.sub.4 -hydrocarbon mixture which contains butadiene, small amounts of oxygen, hydrocarbons which are more soluble than butadiene in the selective solvent and hydrocarbons which are less soluble than butadiene in the selective solvent, wherein the C.sub.4 -hydrocarbon mixture is separated, by extractive distillation, into a distillate containing the less soluble hydrocarbons, a stream of butadiene and a stream containing the more soluble hydrocarbons, a mixture of oxygen and C.sub.4 -hydrocarbons is separated out of the C.sub.4 -hydrocarbon mixture in a distillation zone upstream of the extractive distillation, and the bottom product is fed to the extractive distillation.
摘要翻译：通过选择性溶剂从含有丁二烯，少量氧的C 4烃混合物，在选择性溶剂中比丁二烯更易溶的烃和在选择性溶剂中比丁二烯更难溶解的烃分离丁二烯的方法，其中通过萃取蒸馏将C 4烃混合物分离成含有较不溶的烃，含有较可溶性烃的丁二烯流和含有较多可溶性烃的物流的馏出物，将C 4 - 烃的混合物从C4- 烃混合物在萃取蒸馏上游的蒸馏区中，并将底部产物进料至萃取蒸馏。

10. 发明授权

US4287379A Process for obtaining isobutene from C.sub.4 -hydrocarbon mixtures containing isobutene 失效
标题翻译：从含有异丁烯的C 4烃混合物中获得异丁烯的方法
公开(公告)号：US4287379A
公开(公告)日：1981-09-01
申请号：US137750
申请日：1980-04-07
申请人： Erwin Brunner , Eckart Schubert , Alfred Lindner , Franz Merger , Klaus Volkamer , Max Strohmeyer , Gerhard Sandrock
发明人： Erwin Brunner , Eckart Schubert , Alfred Lindner , Franz Merger , Klaus Volkamer , Max Strohmeyer , Gerhard Sandrock
IPC分类号： B01J31/00 , C07B61/00 , C07C1/00 , C07C7/148 , C07C11/09 , C07C41/42 , C07C67/00 , C07C7/00
CPC分类号： C07C41/42 , C07C11/09 , C07C41/06 , C07C7/14891
摘要： A process for obtaining isobutene from a C.sub.4 -hydrocarbon mixture containing isobutene, by reacting the mixture with a primary alcohol in the presence of an acid condensing agent and decomposing the resulting tertiary ether in the presence of an acid catalyst at an elevated temperature, wherein a primary C.sub.3 - or C.sub.4 -alcohol is used.
摘要翻译：通过在酸缩合剂存在下使该混合物与伯醇反应并在酸催化剂存在下在升高的温度下分解得到的叔乙醚，从含有异丁烯的C 4烃混合物中获得异丁烯的方法，其中a 使用初级C3-或C4-醇。

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