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1. 发明授权

US06337060B1 Hydrophilic diamond particles and method of producing the same 失效
标题翻译：亲水性金刚石颗粒及其制备方法
公开(公告)号：US06337060B1
公开(公告)日：2002-01-08
申请号：US08662022
申请日：1996-06-12
申请人： Akio Hiraki , Toshimichi Ito , Akimitsu Hatta , Hiroshi Makita , Kazuhito Nishimura , Hiroshi Ishizuka , Satoru Hosomi
发明人： Akio Hiraki , Toshimichi Ito , Akimitsu Hatta , Hiroshi Makita , Kazuhito Nishimura , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： C01B3106
CPC分类号： C01B32/28
摘要： The principal objects of the invention is to provide diamond fine particles with a surface nature so improved as to form a stable, uniform suspension or dispersion in a common medium such as water and alcohol. Another object is to provide an effective technique for producing hydrophilic diamond fine particles by chemically modifying the particle surface nature, while removing at the same time contaminants and foreign materials which coexist with the diamond. In the invention, diamond particles are treated by boiling in the treatment fluid of sulfuric acid solution, which is in particular of concentrated or fuming nature, at a temperature more than 200° C., which is preferably 250° C. or more.
摘要翻译：本发明的主要目的是提供具有如此改进的表面性质的金刚石细颗粒，以在普通介质如水和醇中形成稳定的均匀悬浮液或分散体。另一个目的是提供通过化学改性颗粒表面性质同时同时除去与金刚石共存的污染物和异物来生产亲水性金刚石细颗粒的有效技术。在本发明中，金属颗粒在温度超过200℃，优选为250℃以上的温度下，在特别浓缩或发烟性质的硫酸溶液的处理液中沸腾处理。

2. 发明授权

US5510157A Method of producing diamond of controlled quality 失效
标题翻译：生产控制质量钻石的方法
公开(公告)号：US5510157A
公开(公告)日：1996-04-23
申请号：US789441
申请日：1991-11-06
申请人： Chia-Fu Chen , Kazuhito Nishimura , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
发明人： Chia-Fu Chen , Kazuhito Nishimura , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： C01B31/06 , C23C16/27 , C23C16/52
CPC分类号： C23C16/27 , C01B31/06 , C23C16/278 , C23C16/279 , C23C16/52
摘要： Making a diamond substance exhibiting a cathodoluminescence spectrum with the peak at a photon energy greater than 2.8 eV (electron volt), the half-value and 20%-value width not exceeding 0.5 eV and 0.8 eV, respectively, comprising: providing a substrate in a closed chamber, introducing a matrix gas comprising H.sub.2 and one selected from hydrocarbon and CO to said chamber, exciting the gas to create a plasma while heating said substrate to a temperature of at least 700.degree. C. and, thus, causing deposition and growth of diamond substance which is crystallographically diamond, controlling parameters of the deposition by means of the cathodoluminescence record and recovering the diamond substance from the chamber.
摘要翻译：制备具有阴极发光光谱的金刚石物质，其光子能量大于2.8eV（电子伏特）的峰值，半值和20％值的宽度分别不超过0.5eV和0.8eV，包括：提供基底封闭的室，将包含H 2和选自烃和CO的一种基质气体引入所述室，激发气体以产生等离子体，同时将所述衬底加热到至少700℃的温度，从而引起沉积和生长通过阴极发光记录控制沉积参数，并从室中回收金刚石物质。

3. 发明授权

US5882740A Method of producing diamond of controlled quality and product produced thereby 失效
标题翻译：生产受控质量的金刚石的方法和由此生产的产品
公开(公告)号：US5882740A
公开(公告)日：1999-03-16
申请号：US627320
申请日：1996-04-01
申请人： Chia-Fu Chen , Kazuhito Nishimura , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
发明人： Chia-Fu Chen , Kazuhito Nishimura , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： C01B31/06 , C23C16/27 , C23C16/52
CPC分类号： C23C16/27 , C01B31/06 , C23C16/278 , C23C16/279 , C23C16/52
摘要： A method is provided for efficiently producing an entirely quality-controlled CVD diamond. A CVD process is interrupted at an early stage and the deposit is taken out of the reaction chamber, before a significant mass is accumulated, and is inspected by means of cathodoluminescence. The spectrum are compared with a given reference in terms of peak position, half width and 20%-value width in coordination. The observed deviation allows to determine whether to maintain or alter the settings.A diamond substance of acceptable quality which is properly specified in terms of the CL parameters is also provided.
摘要翻译：提供了一种有效地生产完全质量控制的CVD金刚石的方法。 CVD过程在早期中断，并且在积累显着质量之前将沉积物从反应室中取出，并通过阴极发光进行检查。将频谱与峰值位置，半宽度和20％值宽度协调的给定参考值进行比较。观察到的偏差允许确定是否维护或更改设置。还提供了根据CL参数适当指定的可接受质量的钻石物质。

4. 发明授权

US09663851B2 Substrate for CVD deposition of diamond and method for the preparation thereof 有权
公开(公告)号：US09663851B2
公开(公告)日：2017-05-30
申请号：US13884369
申请日：2010-11-09
申请人： Evgeny A. Levashov , Ekaterina V. Azarova , Victor G. Ralchenko , Andrey Bol'Shakov , Evgeny E. Ashkinazi , Hiroshi Ishizuka , Satoru Hosomi
发明人： Evgeny A. Levashov , Ekaterina V. Azarova , Victor G. Ralchenko , Andrey Bol'Shakov , Evgeny E. Ashkinazi , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： C23C4/12 , C23C4/06 , C23C16/27 , C23C4/131 , C23C10/28 , C23C16/02 , C23C4/10 , C23C4/18 , C23C4/067
CPC分类号： C23C4/131 , C23C4/067 , C23C4/10 , C23C4/18 , C23C10/28 , C23C16/0272 , C23C16/271 , Y10T428/25
摘要： A substrate for depositing diamond by CVD, comprising a base body of hard material and a coating layer that holds diamond particles as seed crystal in a matrix and is deposited joined thereto on a surface of said base body, wherein: the seed diamond particles have an average particle size of 1 μm or smaller; the matrix comprises a first metal selected from a first group of Si, Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and W and/or a first compound between said first metal and a non-metallic substance selected from boron, carbon and nitrogen, said matrix holding the diamond particles distributed therein; and a joint zone developed as a result of a diffusion process and extending over said base body and coating layer comprises either or both atoms of said first metal and a component metal of the hard material.

5. 发明授权

US5061292A Diamond abrasive and method for producing the same 失效
标题翻译：金刚石磨料及其制造方法
公开(公告)号：US5061292A
公开(公告)日：1991-10-29
申请号：US379219
申请日：1989-07-13
申请人： Chia-Fu Chen , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
发明人： Chia-Fu Chen , Ensei Ko , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： B24D3/00 , C01B31/06 , C09K3/14 , C23C16/26
CPC分类号： C23C16/26 , B24D3/005 , B24D3/007 , C09K3/1436
摘要： Diamond abrasive comprising a mass of idiomorphic crystal grits which each have an irregular shaped core of diamond formed under pressure where diamond is thermodynamically favored phase, and a growth layer of diamond and/or diamond-like carbon formed over said core by chemical vapor deposition.
摘要翻译：金刚石研磨剂包括大量的同晶晶粒，每个具有金刚石在热力学上有利相的金刚石形成的不规则形状的金刚石芯，以及通过化学气相沉积在所述芯上形成的金刚石和/或类金刚石碳的生长层。

6. 发明申请

US20130230715A1 SUBSTRATE FOR CVD DEPOSITION OF DIAMOND AND METHOD FOR THE PREPARATION THEREOF 有权
标题翻译：用于金刚石沉积的基材及其制备方法
公开(公告)号：US20130230715A1
公开(公告)日：2013-09-05
申请号：US13884369
申请日：2010-11-09
申请人： Evgeny A. Levashov , Ekaterina V. Azarova , Victor G. Ralchenko , Andrey Bol'Shakov , Evgeny E. Ashkinazi , Hiroshi Ishizuka , Satoru Hosomi
发明人： Evgeny A. Levashov , Ekaterina V. Azarova , Victor G. Ralchenko , Andrey Bol'Shakov , Evgeny E. Ashkinazi , Hiroshi Ishizuka , Satoru Hosomi
IPC分类号： C23C4/10 , C23C4/12
CPC分类号： C23C4/131 , C23C4/067 , C23C4/10 , C23C4/18 , C23C10/28 , C23C16/0272 , C23C16/271 , Y10T428/25
摘要： A substrate for depositing diamond by CVD, comprising a base body of hard material and a coating layer that holds diamond particles as seed crystal in a matrix and is deposited joined thereto on a surface of said base body, wherein: the seed diamond particles have an average particle size of 1 μm or smaller; the matrix comprises a first metal selected from a first group of Si, Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and W and/or a first compound between said first metal and a non-metallic substance selected from boron, carbon and nitrogen, said matrix holding the diamond particles distributed therein; and a joint zone developed as a result of a diffusion process and extending over said base body and coating layer comprises either or both atoms of said first metal and a component metal of the hard material.
摘要翻译： 1.一种用于通过CVD沉积金刚石的基底，包括硬质材料的基体和将金刚石颗粒作为晶种保持在基体中并在其上沉积在所述基体的表面上的涂层，其中：所述种子金刚石颗粒具有平均粒径为1um或更小; 所述基体包括选自第一组Si，Ti，Zr，Hf，V，Nb，Ta，Cr，Mo和W中的第一金属和/或所述第一金属和选自硼的非金属物质之间的第一化合物，碳和氮，所述基质保持分布在其中的金刚石颗粒; 并且由于扩散过程而开发并且在所述基体和涂层之上延伸的接合区包括所述第一金属的任一原子或两者的原子和硬材料的组分金属。

7. 发明授权

US06203897B1 Sintered composites containing superabrasive particles 失效
标题翻译：含超级磨料颗粒的烧结复合材料
公开(公告)号：US06203897B1
公开(公告)日：2001-03-20
申请号：US08617904
申请日：1996-08-12
申请人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny A. Levashov , Alexander V. Trotsue , Inna P. Borovinskaya
发明人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny A. Levashov , Alexander V. Trotsue , Inna P. Borovinskaya
IPC分类号： C22C2900
CPC分类号： C22C26/00 , B22F3/23 , B22F2999/00 , C04B35/117 , C04B35/56 , C04B35/5607 , C04B35/5611 , C04B35/563 , C04B35/565 , C04B35/573 , C04B35/58007 , C04B35/58014 , C04B35/58064 , C04B35/58071 , C04B35/58092 , C04B35/581 , C04B35/584 , C04B35/591 , C04B35/64 , C04B35/651 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/3891 , C04B2235/402 , C04B2235/404 , C04B2235/405 , C04B2235/425 , C04B2235/427 , C04B2235/66 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C22C1/053 , C22C1/055 , C22C1/058 , C22C2026/005 , Y10T428/25 , Y10T428/265 , Y10T428/31678 , B22F3/14 , B22F3/15
摘要： This invention provides a composite product and an effective method for producing the same, based on an SHS or intense heat producing process. Said composite essentially comprises either (1) one or more skeletal structures of three dimensionally joined pieces of at least one ceramic material selected from carbide, boride, nitride and silicide of titanium, zirconium, tantalum, niobium, silicon, chromium, tungsten, and molybdenum, and metallic material of alloy and/or intermetallic compound which fills the gaps within each and between adjacent skeletal structures, or (2) a matrix consisting of SHS products of metallic and/or ceramic substances, and particles of superabrasive selected from diamond and high pressure polymorphism of boron nitride, which are held and distributed in the matrix in the whole, in the surface or surface area comprising the portion corresponding to the end working face. Also effective is the use of superabrasive particles coated with metallic and/or non-metallic materials by some specific techniques.
摘要翻译：本发明提供了一种基于SHS或强烈制热工艺的复合产品及其生产方法。所述复合材料基本上包括（1）一种或多种三维接合的至少一种陶瓷材料的骨架结构，所述陶瓷材料选自钛，锆，钽，铌，硅，铬，钨和钼的碳化物，硼化物，氮化物和硅化物，以及填充每个和相邻骨架结构之间的间隙的合金和/或金属间化合物的金属材料，或（2）由金属和/或陶瓷物质的SHS产物组成的基体以及选自金刚石和高分子的超级磨料颗粒包含对应于末端工作面的部分的表面或表面区域中保持和分布在整个基质中的氮化硼的高压多晶型物。使用通过某些特定技术涂覆金属和/或非金属材料的超级磨料颗粒也是有效的。

8. 发明授权

US06500557B1 Composite and method for producing the same 失效
标题翻译：复合材料及其制造方法
公开(公告)号：US06500557B1
公开(公告)日：2002-12-31
申请号：US09663671
申请日：2000-09-18
申请人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny A. Levashov , Alexander V. Trotsue , Inna P. Borovinskaya
发明人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny A. Levashov , Alexander V. Trotsue , Inna P. Borovinskaya
IPC分类号： G32B900
CPC分类号： C22C26/00 , B22F3/23 , B22F2999/00 , C04B35/117 , C04B35/56 , C04B35/5607 , C04B35/5611 , C04B35/563 , C04B35/565 , C04B35/573 , C04B35/58007 , C04B35/58014 , C04B35/58064 , C04B35/58071 , C04B35/58092 , C04B35/581 , C04B35/584 , C04B35/591 , C04B35/64 , C04B35/651 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/3891 , C04B2235/402 , C04B2235/404 , C04B2235/405 , C04B2235/425 , C04B2235/427 , C04B2235/66 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C22C1/053 , C22C1/055 , C22C1/058 , C22C2026/005 , Y10T428/25 , Y10T428/265 , Y10T428/31678 , B22F3/14 , B22F3/15
摘要： This invention provides a composite product and an effective method for producing the same, based on an SHS or intense heat producing process. Said composite essentially comprises either (1) one or more skeletal structures of three dimensionally joined pieces of at least one ceramic material selected from carbide, boride, nitride and silicide of titanium, zirconium, tantalum, niobium, silicon, chromium, tungsten, and molybdenum, and metallic material of alloy and/or intermetallic compound which fills the gaps within each and between adjacent skeletal structures, or (2) a matrix consisting of SHS products of metallic and/or ceramic substances, and particles of superabrasive selected from diamond and high pressure polymorphism of boron nitride, which are held and distributed in the matrix in the whole, in the surface or surface area comprising the portion corresponding to the end working face. Also effective is the use of superabrasive particles coated with metallic and/or non-metallic materials by some specific techniques.
摘要翻译：本发明提供了一种基于SHS或强烈制热工艺的复合产品及其生产方法。所述复合材料基本上包括（1）一种或多种三维接合的至少一种陶瓷材料的骨架结构，所述陶瓷材料选自钛，锆，钽，铌，硅，铬，钨和钼的碳化物，硼化物，氮化物和硅化物，以及填充每个和相邻骨架结构之间的间隙的合金和/或金属间化合物的金属材料，或（2）由金属和/或陶瓷物质的SHS产物组成的基体以及选自金刚石和高分子的超级磨料颗粒包含对应于末端工作面的部分的表面或表面区域中保持和分布在整个基质中的氮化硼的高压多晶型物。使用通过某些特定技术涂覆金属和/或非金属材料的超级磨料颗粒也是有效的。

9. 发明授权

US06432150B1 Diamond-containing stratified composite material and method of manufacturing the same 失效
标题翻译：含金刚石层状复合材料及其制造方法
公开(公告)号：US06432150B1
公开(公告)日：2002-08-13
申请号：US09462889
申请日：2000-05-12
申请人： Evgeny Alexandrovich Levashov , Alexander Sergeevich Rogatchov , Boris Vladmirovich Spitsin , Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi
发明人： Evgeny Alexandrovich Levashov , Alexander Sergeevich Rogatchov , Boris Vladmirovich Spitsin , Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi
IPC分类号： B24D306
CPC分类号： C22C1/053 , B22F3/23 , B22F7/06 , B22F2998/00 , B24D3/08 , B22F2207/03
摘要： A superabrasive containing layered composite is provided which comprises a substrate block consisting of either ceramic material and metallic or several metallic materials, and a superabrasive containing body adjacent said substrate block. The superabrasive contains superabrasive particles, and a metallic ingredient which is distributed in the superabrasive containing layer, including a working surface. The superabrasive material may be formed using a compression cell wherein the compression cell comprises a die defined by a vertical wall and a flat closed bottom. Placed in the die, in order from bottom upward, comprises a formed pallet of single body or layers of mixed powder forming a refractory compound, a material mass of a working layer containing diamond particles, a mass of ignition material comprising an SHS composition, and an electrical heating element.
摘要翻译：提供了一种含超级磨料的层状复合材料，其包括由陶瓷材料和金属或几种金属材料组成的基底块，以及与所述基底块相邻的超级磨料容纳体。超级磨料包含超研磨颗粒和分布在包含工作表面的超级磨料含有层中的金属成分。超研磨材料可以使用压缩单元形成，其中压缩单元包括由垂直壁和平的封闭底部限定的模具。放置在模具中，从底部向上依次包括形成难熔化合物的单体或混合粉末层的成形托盘，包含金刚石颗粒的工作层的材料块，包含SHS组合物的点燃材料块，以及电加热元件。

10. 发明授权

US06336950B1 Electrode rod for spark deposition, process for the production thereof, and process for covering with superabrasive-containing layer 失效
标题翻译：用于火花沉积的电极棒，其制造方法以及用含超级磨料层的覆盖物的方法
公开(公告)号：US06336950B1
公开(公告)日：2002-01-08
申请号：US09509666
申请日：2000-05-05
申请人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny Alexandrovich Levashov , Alexander Gennadievich Nikolaev , Alexander Evgenievich Kudryashov
发明人： Mitsue Koizumi , Manshi Ohyanagi , Satoru Hosomi , Evgeny Alexandrovich Levashov , Alexander Gennadievich Nikolaev , Alexander Evgenievich Kudryashov
IPC分类号： C22C2900
CPC分类号： C23C26/00 , C23C4/06
摘要： An aspect of this invention is an electrode rod for spark alloying, comprising a compact of a first powder of a first component which comprises a metal selected from a group of Fe, Co, Ni, metals of 4a, 5a and 6a of the periodic table and Si, and a second powder of a second component which is capable of self-propagating high temperature synthesis to form with said first component carbide, nitride, boride, silicide or intermetallic compound, said first and second powders being mixed intimately with each other and formed into an axial rod. Another aspect is a method for the production of the electrospark alloying rod, comprising: mixing intimately a first powder of first component and a second powder of second component, said first component comprising at least one selected from Fe, Co, Ni, metals of groups 4a, 5a and 6a, Sn, Zn, Pb, Al and Cu, said second component comprising materials capable of SHS process to form a refractory (or intermetallic) compound, compressing said mixture, followed or not by further firing, and thereby forming an axial body with a bulk density 0.50 to 0.86 time the theoretical values for the corresponding substances. Still another aspect is a method for the deposition of a coating on a work by causing and holding an electric spark between said electrode rod and work, whereby transferring the materials of said first and second components to the surface of said work, and depositing thereon as a layer or more layers of such compound.
摘要翻译：本发明的一个方面是一种用于火花合金化的电极棒，包括第一组分的第一粉末的压块，该第一组分包含选自Fe，Co，Ni的金属，周期表的4a，5a和6a的金属和Si，以及能够自发传播高温合成以与所述第一组分碳化物，氮化物，硼化物，硅化物或金属间化合物形成的第二组分的第二粉末，所述第一和第二粉末彼此紧密混合，形成轴向杆。另一方面是一种用于生产电火花合金棒的方法，包括：将第一组分的第一粉末和第二组分的第二粉末紧密混合，所述第一组分包含选自Fe，Co，Ni中的至少一种，基团金属 4a，5a和6a，Sn，Zn，Pb，Al和Cu，所述第二组分包括能够进行SHS工艺的材料以形成耐火材料（或金属间化合物），压缩所述混合物，随后进行或不再进一步烧制，从而形成轴向体的体积密度为0.50〜0.86倍，相应物质的理论值。另一方面是一种通过在所述电极棒和工件之间引起和保持电火花将工件上的涂层沉积在工件上的方法，由此将所述第一和第二部件的材料转移到所述工件的表面上，并将其上沉积在其上一层或多层这样的化合物。

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