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1. 发明申请

WO2017186714A1 METHOD OF FORMING WRINKLE FINISH COATING ON A METAL SUBSTRATE 审中-公开
标题翻译：在金属基底上形成皱纹涂层的方法
公开(公告)号：WO2017186714A1
公开(公告)日：2017-11-02
申请号：PCT/EP2017/059790
申请日：2017-04-25
申请人： AKZO NOBEL COATINGS INTERNATIONAL B.V. , OBAYASHI CORPORATION
发明人： HORI, Nagao , OKUDA, Akiko , MITANI, Hitofusa , KOJO, Yuichi , KOHASHI, Taichiro , SHIBAMOTO, Tetsuya , TSUJITA, Takahiro
IPC分类号： B05D5/06 , C09D5/28
CPC分类号： C09D5/28 , B05D5/062 , C08K3/013 , C08K3/36 , C08K3/40 , C08K2201/005 , C09D7/40
摘要： The present invention relates to a method of forming a wrinkle finish coating on a metal substrate at an installation site with the appearance similar to that of the wrinkle finish formed by applying a base paint A1 in a factory, in which method a coating composition A2 is obtained by adding 0.1–20 parts by mass of silica particulate with an average particle diameter of 0.1 µm–40 µm per 100 parts by mass of the solids in base paint A1 to the base paint A1, the coating composition A2 is applied to the metal substrate at the installation site of said component that is the object of wrinkle finish coating, and then heat-cured. Using this method, scratches, etc. that occur in a patterned coating like a wrinkle finish coating during transport and work can be easily repaired at an installation site.
摘要翻译：本发明涉及一种在安装现场在金属基材上形成褶皱涂层涂层的方法，其外观类似于通过在工厂涂覆基础涂料A1而形成的皱纹涂层的外观，在该方法中，通过将0.1-20质量份平均粒径为0.1μm-40μm的二氧化硅颗粒/ 100质量份基础涂料A1中的固体加入到基底中获得涂料组合物A2 涂料A1将涂料组合物A2涂布在作为皱纹涂饰物的所述成分的设置部位的金属基材上，然后进行热固化。使用这种方法，运输和工作过程中出现在图案化涂层如皱纹涂层中的划痕等可以在安装现场轻松修复。

2. 发明申请

WO2018047014A1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD AND METHOD FOR PRODUCING A PAINTED ARTICLE 审中-公开
标题翻译：生产涂漆制品的热固性组合物，涂料整理方法和方法
公开(公告)号：WO2018047014A1
公开(公告)日：2018-03-15
申请号：PCT/IB2017/001384
申请日：2017-09-04
申请人： AKZO NOBEL COATINGS INTERNATIONAL B.V.
发明人： MIZUTANI, Hiroki , TSUDA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhaku , MIYABE, Koji
IPC分类号： C08G18/61 , C08G18/80 , C09D167/00 , C08G18/22 , C08G18/42
摘要： The present invention relates to a thermosetting composition characterized in that it contains (A) a polyester resin of number average molecular weight 1,000-10,000 and hydroxyl value 5-200 mg KOH/g and, (B) 0.5-2.0 equivalents relative to the hydroxyl groups of the aforesaid component (A) of a compound (B) which is a blocked aliphatic poly-isocyanate compound having reactivity with the hydroxyl groups of component (A), wherein the blocking is with methyl ethyl ketoxime and/or ε-caprolactam, (C) 0.05-5 parts by weight of a bismuth compound, per 100 parts by weight of total resin solids of component (A) and component (B), and (D) 0.5-50 parts by weight of an organosilicate represented by the following general formula (I) and/or a condensation product thereof, relative to 100 parts by weight of total resin solids of component (A) and component (B), wherein R 1 , R 2 , R 3 and R 4 in the formula each mean hydrogen atom or 1-10 carbon organic group, and can be the same or different, n is 1. By using the thermosetting composition, not only does the stain resistance appear a short time after painting, but also excellent stain resistance is maintained for a long period, which fulfil the paint film performance requirements for painted steel sheet such as water resistance and bending workability and which have high environmental protection qualities and safety.
摘要翻译：本发明涉及一种热固性组合物，其特征在于它含有（A）数均分子量为1,000-10,000且羟值为5-200mg KOH / g的聚酯树脂，和（B）相对于作为与组分（A）的羟基具有反应性的封端脂肪族多异氰酸酯化合物的化合物（B）的上述组分（A）的羟基的0.5-2.0当量，其中封端是甲基乙基酮肟和/或ε-己内酰胺，（C）每100重量份的组分（A）和组分（B）的总树脂固体，0.05-5重量份的铋化合物，和（D）0.5-50重量份（I）所示的有机硅酸酯和/或其缩合产物，相对于100重量份的组分（A）和组分（B）的总树脂固体，其中R 1≤1重量％式中的R 2，R 3和R 4各自表示氢原子或1-10碳或可以相同或不同，n为1.通过使用热固性组合物，不仅在涂漆后短时间内出现耐污染性，而且长期保持优异的耐污染性，这满足了涂料涂漆钢板的薄膜性能要求，如耐水性和弯曲加工性，并且具有高环境质量和安全性。

3. 发明申请

WO2017050511A1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD, AND METHOD FOR PRODUCING PAINTED ARTICLES 审中-公开
标题翻译：热固化组合物，油漆涂饰方法和生产涂料文章的方法
公开(公告)号：WO2017050511A1
公开(公告)日：2017-03-30
申请号：PCT/EP2016/069984
申请日：2016-08-24
申请人： AKZO NOBEL COATINGS INTERNATIONAL B.V.
发明人： MIZUTANI, Hiroki , TSUJITA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhiro , MIYABE, Koji
IPC分类号： C09D183/02 , C09D167/02 , C09D175/06 , C08L67/02
CPC分类号： C09D183/02 , C08G18/246 , C08G18/4219 , C08G18/807 , C08G18/8074 , C08G18/8077 , C08L2205/03 , C08L2205/05 , C09D167/00 , C09D175/06 , C08L83/02 , C08K5/06 , C08K5/5415
摘要： [Purpose ] To provide a thermosetting composition with which it is possible to obtain paint films which not only display stain resistance for a short period after application, but with which excellent stain resistance can also be expected for longer periods, and which comply with the paint film properties required for painted steel sheet such as water resistance and bending workability, and have high environmental protection and safety qualities. [Solution] The present invention relates to a thermosetting composition, wherein it contains, as essential components, (A) a polyester resin of number average molecular weight 1,000-10,000 and hydroxyl value 5-200 mg KOH/g and, (B) 0.5 to 2.0 equivalents, relative to the hydroxyl groups of the aforesaid component (A), of a compound (B) which is a blocked aliphatic polyisocyanate compound having reactivity to the hydroxyl groups of component (A), wherein the blocks are methyl ethyl ketone oxime and/or ε-caprolactam, (C) 0.05 to 5 mass %, relative to the total resin solids mass of component (A) and component (B), of an organotin compound represented by the following general formula (I) [Chem.1] R 1 -Sn- (0)C=0) -R 2 ) 3 (I) (R 1 in the formula represents an organic group wherein it has 1-24 carbons, and is directly bound to the Sn atom via a C atom. R 2 represents an organic group wherein it has 1-24 carbons, and is directly bound to the C atom of the (C=O) via a C atom), and (D) 0.5 to 50 mass %, relative to the total resin solids mass of component (A) and component (B), of an organosilicate represented by the following general formula (II) and/or a condensation product thereof [Chem.2] (R 3 , R 4 , R 5 and R 6 in the formula are each a hydrogen atom or 1- 10 carbon organic group, and may be the same or different. n is 1). [Selected drawings] None
摘要翻译： [目的]提供一种可以获得涂膜的热固性组合物，其不仅在施用后的短时间内显示耐污染性，而且还可以期待较长时间的优异的耐污性，并且符合涂料涂装钢板所需的膜性能，如耐水性和弯曲加工性，具有很高的环保性和安全性。热固性组合物本发明涉及一种热固性组合物，其中含有（A）数均分子量为1,000〜10,000，羟值为5〜200mgKOH / g的聚酯树脂作为必要成分，（B）0.5 相对于前述组分（A）的羟基为2.0当量，化合物（B）为与组分（A）的羟基具有反应性的封端脂族多异氰酸酯化合物，其中嵌段是甲基乙基酮肟和/或ε-己内酰胺，（C）相对于组分（A）和组分（B）的总树脂固体质量为0.05-5质量％的由以下通式（I）表示的有机锡化合物。 1] R1-Sn-（0）C = 0）-R2）3（I）（式中的R1表示其具有1-24个碳的有机基团，并且通过C原子直接与Sn原子结合。 R 2表示其具有1-24个碳的有机基团，并且通过C原子直接与（C = O）的C原子结合），（D）为0.5〜50mas 相对于组分（A）和组分（B））由以下通式（II）表示的有机硅酸盐和/或其缩合产物[化学式2]（R3，R4，式中的R 5和R 6各自为氢原子或1-10碳的有机基团，并且可以相同或不同。 n为1）。 [所选图纸]无

4. 发明授权

EP3353251B1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD, AND METHOD FOR PRODUCING PAINTED ARTICLES 有权
公开(公告)号：EP3353251B1
公开(公告)日：2019-07-17
申请号：EP16757226.2
申请日：2016-08-24
申请人： Akzo Nobel Coatings International B.V.
发明人： MIZUTANI, Hiroki , TSUJITA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhiro , MIYABE, Koji
IPC分类号： C09D183/02 , C09D167/02 , C09D175/06 , C08L67/02

5. 发明授权

EP3510071B1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD AND METHOD FOR PRODUCING A PAINTED ARTICLE 有权转让
公开(公告)号：EP3510071B1
公开(公告)日：2020-11-04
申请号：EP17818250.7
申请日：2017-09-04
申请人： Akzo Nobel Coatings International B.V.
发明人： MIZUTANI, Hiroki , TSUJITA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhiro , MIYABE, Koji
IPC分类号： C08G18/61 , C08G18/80 , C09D167/00 , C08G18/22 , C08G18/42

6. 发明公开

EP3510071A1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD AND METHOD FOR PRODUCING A PAINTED ARTICLE 有权转让
公开(公告)号：EP3510071A1
公开(公告)日：2019-07-17
申请号：EP17818250.7
申请日：2017-09-04
申请人： Akzo Nobel Coatings International B.V.
发明人： MIZUTANI, Hiroki , TSUJITA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhiro , MIYABE, Koji
IPC分类号： C08G18/61 , C08G18/80 , C09D167/00 , C08G18/22 , C08G18/42
摘要： The present invention relates to a thermosetting composition characterized in that it contains (A) a polyester resin of number average molecular weight 1,000-10,000 and hydroxyl value 5-200 mg KOH/g and, (B) 0.5-2.0 equivalents relative to the hydroxyl groups of the aforesaid component (A) of a compound (B) which is a blocked aliphatic poly-isocyanate compound having reactivity with the hydroxyl groups of component (A), wherein the blocking is with methyl ethyl ketoxime and/or ε-caprolactam, (C) 0.05-5 parts by weight of a bismuth compound, per 100 parts by weight of total resin solids of component (A) and component (B), and (D) 0.5-50 parts by weight of an organosilicate represented by the following general formula (I) and/or a condensation product thereof, relative to 100 parts by weight of total resin solids of component (A) and component (B), wherein R1, R2, R3 and R4 in the formula each mean hydrogen atom or 1-10 carbon organic group, and can be the same or different, n is 1. By using the thermosetting composition, not only does the stain resistance appear a short time after painting, but also excellent stain resistance is maintained for a long period, which fulfil the paint film performance requirements for painted steel sheet such as water resistance and bending workability and which have high environmental protection qualities and safety.

7. 发明公开

EP3353251A1 THERMOSETTING COMPOSITION, PAINT FINISHING METHOD, AND METHOD FOR PRODUCING PAINTED ARTICLES 有权
公开(公告)号：EP3353251A1
公开(公告)日：2018-08-01
申请号：EP16757226.2
申请日：2016-08-24
申请人： Akzo Nobel Coatings International B.V.
发明人： MIZUTANI, Hiroki , TSUJITA, Takahiro , KOHASHI, Taichiro , NISHIDA, Nobuhiro , MIYABE, Koji
IPC分类号： C09D183/02 , C09D167/02 , C09D175/06 , C08L67/02
CPC分类号： C09D175/06 , B05D1/28 , B05D3/0209 , B05D3/0254 , C08G18/242 , C08G18/246 , C08G18/3893 , C08G18/4216 , C08G18/4219 , C08G18/6633 , C08G18/73 , C08G18/755 , C08G18/807 , C08G18/8074 , C08G18/8077 , C08L2205/03 , C08L2205/05 , C09D167/00 , C09D183/02 , C08L83/02 , C08K5/06 , C08K5/5415
摘要： [Purpose ] To provide a thermosetting composition with which it is possible to obtain paint films which not only display stain resistance for a short period after application, but with which excellent stain resistance can also be expected for longer periods, and which comply with the paint film properties required for painted steel sheet such as water resistance and bending workability, and have high environmental protection and safety qualities. [Solution] The present invention relates to a thermosetting composition, wherein it contains, as essential components, (A) a polyester resin of number average molecular weight 1,000-10,000 and hydroxyl value 5-200 mg KOH/g and, (B) 0.5 to 2.0 equivalents, relative to the hydroxyl groups of the aforesaid component (A), of a compound (B) which is a blocked aliphatic polyisocyanate compound having reactivity to the hydroxyl groups of component (A), wherein the blocks are methyl ethyl ketone oxime and/or ε-caprolactam, (C) 0.05 to 5 mass %, relative to the total resin solids mass of component (A) and component (B), of an organotin compound represented by the following general formula (I) [Chem.1] R1-Sn- (0)C=0) -R2)3 (I) (R1 in the formula represents an organic group wherein it has 1-24 carbons, and is directly bound to the Sn atom via a C atom. R2 represents an organic group wherein it has 1-24 carbons, and is directly bound to the C atom of the (C=O) via a C atom), and (D) 0.5 to 50 mass %, relative to the total resin solids mass of component (A) and component (B), of an organosilicate represented by the following general formula (II) and/or a condensation product thereof [Chem.2] (R3, R4, R5 and R6 in the formula are each a hydrogen atom or 1- 10 carbon organic group, and may be the same or different. n is 1). [Selected drawings] None

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