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1. 发明授权

US4039333A Photographic materials having improved anti-halation layers 失效
标题翻译：具有改进的防晕层的照相材料
公开(公告)号：US4039333A
公开(公告)日：1977-08-02
申请号：US676785
申请日：1976-04-14
申请人： Yukio Shinagawa , Yasumasa Yamaguchi , Shuichi Shindo
发明人： Yukio Shinagawa , Yasumasa Yamaguchi , Shuichi Shindo
IPC分类号： G03C1/825 , G03C1/835 , G03C1/84
CPC分类号： G03C1/835
摘要： An anti-halation layer for photographic materials comprising at least one first binder which is swollen by an aqueous alkaline solution and comprises about 10 to about 25% by weight of alkyl acrylate units, 52 to 65% by weight of alkyl methacrylate units and about 18 to about 30% by weight of suitable acid monomer units, and at least a second binder agent which is soluble in an alkaline aqueous solution but which can withstand a strongly alkaline preliminary bath and is readily stripped away only at a successive rinsing operation.
摘要翻译：一种用于照相材料的防晕层，包括至少一种第一粘合剂，其由碱性水溶液溶胀而膨胀，并且包含约10至约25重量％的丙烯酸烷基酯单元，52至65重量％的甲基丙烯酸烷基酯单元和约18 至约30重量％的合适的酸单体单元，以及至少第二粘合剂，其可溶于碱性水溶液中，但可耐受强碱性初步浴，并且仅在连续漂洗操作时容易剥离。

2. 发明授权

US06743944B1 Process for producing optically active aminoalcohol 失效
标题翻译：光学活性氨基醇的制备方法
公开(公告)号：US06743944B1
公开(公告)日：2004-06-01
申请号：US10070365
申请日：2002-03-06
申请人： Eiji Ozaki , Takakazu Endou , Yasumasa Yamaguchi , Mitsuharu Hamanaka
发明人： Eiji Ozaki , Takakazu Endou , Yasumasa Yamaguchi , Mitsuharu Hamanaka
IPC分类号： C07C5948
CPC分类号： C07C215/08 , C07B2200/07 , C07C51/412 , C07C213/10 , Y02P20/582 , C07C59/56 , C07C59/48 , C07C59/50
摘要： An industrially advantageous process for producing optically active 4-amino-2-methylbutane-1-ol which is useful as an intermediate in synthesizing optically active medicines and pesticides. Racemic 4-amino-2-methylbutane-1-ol is treated with an optically active organic acid. The diastereomeric salt thus obtained is crystallized out and subjected to solid-liquid separation to give optically active 4-amino-2-methylbutane-1-ol. The diastereomeric salt of optically active 4-amino-2-methylbutane-1-ol with an optically active reagent for optical resolution is decomposed by bringing into contact with a solvent and an alkali and subjected to solid-liquid separation, thereby recovering the optically active 4-amino-2-methylbutane-1-ol from the filtrate. Further, the filtration residue containing the alkali salt of the reagent for optical resolution obtained by the solid-liquid separation is brought into contact with a solvent and an acid. Then the reagent for optical resolution thus crystallized out is subjected to solid-liquid separation and recovered.
摘要翻译：用于制备光学活性4-氨基-2-甲基丁-1-醇的工业上有利的方法，其可用作合成光学活性药物和农药的中间体。外消旋4-氨基-2-甲基丁-1-醇用光学活性有机酸处理。将所得非对映体盐结晶出来，进行固液分离，得到光学活性的4-氨基-2-甲基丁-1-醇。光学活性的4-氨基-2-甲基丁烷-1-醇与光学活性剂的光学拆分的非对映盐通过与溶剂和碱接触进行分解，进行固液分离，由此回收光学活性物质 4-氨基-2-甲基丁烷-1-醇。此外，含有通过固液分离获得的用于光学拆分的试剂的碱金属盐的过滤残渣与溶剂和酸接触。然后将由此结晶的光学拆分试剂进行固液分离并回收。

3. 发明授权

US4188339A Process for preparing acrylamide aqueous solution 失效
标题翻译：制备丙烯酰胺水溶液的方法
公开(公告)号：US4188339A
公开(公告)日：1980-02-12
申请号：US843472
申请日：1977-10-19
申请人： Yasumasa Yamaguchi , Kazuo Kohno
发明人： Yasumasa Yamaguchi , Kazuo Kohno
IPC分类号： C07C233/09 , C07C103/08
CPC分类号： C07C233/09
摘要： A process for preparing an aqueous solution of acrylamide, which comprisescatalytically hydrating acrylonitrile in the presence of a metal-containing catalyst to form a mixed aqueous solution containing about 15 to about 35% by weight of acrylamide and about 0.5 to about 20% by weight of acrylonitrile, andconcentrating the mixed aqueous solution to a high concentration aqueous solution of acrylamide having an acrylonitrile concentration of about 0.1% by weight or less using a centrifugal film evaporator in which a stream of mixed aqueous solution and a stream of evaporated vapor flow countercurrently to each other.
摘要翻译：一种制备丙烯酰胺水溶液的方法，其包括在含金属的催化剂存在下催化水合丙烯腈以形成含有约15至约35重量％的丙烯酰胺和约0.5至约20重量％的混合水溶液的丙烯腈，并且使用离心膜蒸发器将混合水溶液浓缩至丙烯腈浓度为约0.1重量％以下的高浓度丙烯酰胺水溶液，其中混合水溶液流和蒸发蒸气流逆流流动对彼此。

4. 发明授权

US5154905A Method for producing unsintered cristobalite particles 失效
标题翻译：生产未烧结方石英颗粒的方法
公开(公告)号：US5154905A
公开(公告)日：1992-10-13
申请号：US814051
申请日：1991-12-26
申请人： Iwao Ohshima , Koichi Orii , Naotake Watanabe , Yasumasa Yamaguchi
发明人： Iwao Ohshima , Koichi Orii , Naotake Watanabe , Yasumasa Yamaguchi
IPC分类号： C01B33/12 , C01B33/18 , C03B19/10 , C04B14/06
CPC分类号： C04B14/06 , C01B33/12 , C03B19/1095
摘要： A method for producing a nonsintered cristobalite particles comprising heating amorphous silica particles at a temperature of 1400.degree. to 1700.degree. C. in the presence of cristobalite particles (hereinafter referred to as cristobalite particles for addition and mixing) of at least 5 parts by weight based on 100 parts by weight of said amorphous silica particles to convert said amorphous silica particles to cristobalite particles with their particle form kept unchanged. According to the present invention, dense cristobalite having a low alkali content can be obtained in the form of particles. Such cristobalite is used as a filler, a dispersing agent, etc., and also as a material for high-quality artificial quartz, ceramics, etc., and particularly as a material for transparent quartz glass because of its generating no bubbles at the time of melt-molding.
摘要翻译：一种非烧结方英石颗粒的制造方法，其包括在方沸石颗粒（以下称为方石英颗粒添加和混合）存在下，在1400〜1700℃的温度下加热至少5重量份的无定形二氧化硅颗粒，在100重量份的所述无定形二氧化硅颗粒上将所述无定形二氧化硅颗粒转化为方英石颗粒，其颗粒形式保持不变。根据本发明，可以以颗粒的形式获得具有低碱含量的致密方英石。这种方英石作为填料，分散剂等，也可以作为高品质的人造石英，陶瓷等的材料，特别是作为透明石英玻璃的材料，因为在此时不产生气泡的熔融成型。

5. 发明授权

US5028360A Method of manufacturing spherical silica particles 失效
标题翻译：球形二氧化硅颗粒的制造方法
公开(公告)号：US5028360A
公开(公告)日：1991-07-02
申请号：US508813
申请日：1990-04-16
申请人： Yuziro Ito , Takashi Higashiogawa , Masahiro Matsuura , Koichi Orii , Yasumasa Yamaguchi
发明人： Yuziro Ito , Takashi Higashiogawa , Masahiro Matsuura , Koichi Orii , Yasumasa Yamaguchi
IPC分类号： C01B33/12 , C01B33/18 , C01B33/187
CPC分类号： C01B33/12 , C01B33/18 , C01B33/187 , C01P2002/02 , C01P2004/03 , C01P2004/10 , C01P2004/32 , C01P2004/34 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/80
摘要： A method of manufacturing spherical silica particles comprising the steps of processing in an acid-containing solution and then washing with water the coagulant derived from an aqueous alkali metal silicate solution extruded through pores in a water-miscible organic medium or acid solution, wet-grinding the amorphous silica thus obtained in a liquid dispersion medium to obtain a fine particle silica suspension with a weight average particle size of 10 .mu.m or less, spray-drying this fine particle silica suspension with hot air and sintering the spherical granulated silica thus obtained. According to the present invention, the high-purity spherical silica particles can be obtained with high solidity and adjusted surface smoothness without any complicated operation or waste water treatment for use as a sealant filler for highly-integrated IC electronic parts.
摘要翻译：一种制造球形二氧化硅颗粒的方法，包括以下步骤：在含酸溶液中加工，然后用水洗涤衍生自水溶性有机介质或酸溶液中的孔的水性碱金属硅酸盐溶液的凝结剂，湿磨在液体分散介质中获得的无定形二氧化硅，得到重均粒径为10μm以下的微粒二氧化硅悬浮液，用热风喷雾干燥该微粒二氧化硅悬浮液，烧结得到的球状粒状二氧化硅。根据本发明，高纯度球形二氧化硅颗粒可以获得高固体度和调节表面平滑度，而无需任何复杂的操作或废水处理，用作高度集成的IC电子部件的密封剂填料。

6. 发明授权

US4883897A Process for producing 2,6-dichlorobenzonitrile 失效
标题翻译： 2,6-二氯苄腈的制备方法
公开(公告)号：US4883897A
公开(公告)日：1989-11-28
申请号：US135353
申请日：1987-12-21
申请人： Yutaka Kiyomiya , Yasumasa Yamaguchi , Masahiro Ushigome , Hiroshi Murata
发明人： Yutaka Kiyomiya , Yasumasa Yamaguchi , Masahiro Ushigome , Hiroshi Murata
IPC分类号： C07C253/28 , C07C255/49 , C07C255/50
CPC分类号： C07C255/00
摘要： A process for producing 2,6-dichlorobenzonitrile by ammoxidation comprising contacting a starting gas consisting of 2,6-dichlorotoluene, air and ammonia, which comprises carrying out this reaction under the following conditions:(a) the concentration of 2,6-dichlorotoluene in the starting gas is 2.6 mole % or more.(b) the reactor effluent gas is contacting with water to cool to a temperature in the range of 50.degree. to 90.degree. C., whereby 2,6-dichlorobenzonitrile in the reactor effluent gas is collected as a slurry in which solidified 2,6-dichlorobenzonitrile is dispersed in water, and 2,6-dichlorobenzonitrile is obtained from the slurry, and(c) the cooled reactor effluent gas from which 2,6-dichlorobenzonitrile has been removed is contacted with water again to cool to a temperature in the range of 0.degree. to 40.degree. C., whereby unreacted 2,6-dichlorotoluene in the gas is collected as a dispersion in which it is dispersed in water and 2,6-dichlorotoluene is recovered from the dispersion.Also, there is disclosed a process for purifying 2,6-dichlorobenzonitrile obtained by subjecting 2,6-dichlorotoluene to ammoxidation, which comprises subjecting the 2,6-dichlorobenzonitrile to solid-liquid separation procedure in a molten state.

7. 发明授权

US4701558A Method for purifying aqueous acrylamide solution 失效
标题翻译：纯化丙烯酰胺水溶液的方法
公开(公告)号：US4701558A
公开(公告)日：1987-10-20
申请号：US799051
申请日：1985-11-18
申请人： Yasumasa Yamaguchi , Masashi Nishida
发明人： Yasumasa Yamaguchi , Masashi Nishida
IPC分类号： B01D15/00 , C07C231/24 , C07C233/09 , C07C102/08 , C12P13/02
CPC分类号： C07C233/09
摘要： A method for purifying an aqueous acrylamide solution by using activated carbon is disclosed. The method comprises contacting activated carbon with water having oxygen dissolved therein until the dissolved oxygen concentration in water after the contact increases to at least 0.5 ppm, and then contacting the aqueous acrylamide solution with the thus treated activated carbon. The method can prevent polymerization of acrylamide around activated carbon, and the resulting purified aqueous acrylamide solution requires no further purification, such as ion-exchanging.
摘要翻译：公开了一种使用活性炭净化丙烯酰胺水溶液的方法。该方法包括使活性炭与溶解有氧气的水接触，直到接触后水中的溶解氧浓度增加至至少0.5ppm，然后使丙烯酰胺水溶液与如此处理的活性炭接触。该方法可以防止丙烯酰胺在活性炭周围的聚合，并且所得纯化的丙烯酰胺水溶液不需要进一步的纯化，例如离子交换。

8. 发明授权

US4440858A Process for the continuous production of acrylamide or methacrylamide using microorganisms 失效
标题翻译：使用微生物连续生产丙烯酰胺或甲基丙烯酰胺的方法
公开(公告)号：US4440858A
公开(公告)日：1984-04-03
申请号：US146937
申请日：1980-05-02
申请人： Yasumasa Yamaguchi , Ichiro Watanabe , Yoshiaki Satoh
发明人： Yasumasa Yamaguchi , Ichiro Watanabe , Yoshiaki Satoh
IPC分类号： C07C233/09 , C12N11/02 , C12P13/00 , C12P13/02 , C12R1/01 , C12R1/07 , C12R1/13 , C12R1/15 , C12R1/265 , C12R1/365 , C12N11/00 , C12N11/04
CPC分类号： C12P13/02 , Y10S435/822 , Y10S435/832 , Y10S435/84 , Y10S435/843 , Y10S435/859 , Y10S435/872
摘要： A process for the continuous production of acrylamide or methacrylamide from acrylonitrile or methacrylonitrile by use of a microorganism capable of promoting the hydration of acrylonitrile or methacrylonitrile into the corresponding amide.Said process comprising immobilizing the microorganism or enzyme extracted therefrom, continuously bringing the acrylonitrile or methacrylonitrile into contact with the immobilized microorganism or enzyme in at least one reactor containing an aqueous medium at a pH pf 6 to 10 to cause the hydration reaction, and recycling a part of the reacted solution to dilute the unreacted acrylonitrile or methacrylonitrile and water therewith.
摘要翻译：通过使用能够促进丙烯腈或甲基丙烯腈水合成相应酰胺的微生物从丙烯腈或甲基丙烯腈连续生产丙烯酰胺或甲基丙烯酰胺的方法。所述方法包括固定微生物或从其中提取的酶，连续使丙烯腈或甲基丙烯腈与固定的微生物或酶在至少一个反应器中接触，所述至少一个反应器含有pH6〜10的水性介质，引起水合反应，反应溶液的一部分，以稀释未反应的丙烯腈或甲基丙烯腈和水。

9. 发明授权

US4844809A Method for purifying reaction solution obtained by using microbial cell, immobilized microbial cell, or immobilized enzyme 失效
标题翻译：通过使用微生物细胞，固定化微生物细胞或固定化酶获得的反应溶液的纯化方法
公开(公告)号：US4844809A
公开(公告)日：1989-07-04
申请号：US799059
申请日：1985-11-18
申请人： Ashina Yoshiro , Yasumasa Yamaguchi , Masashi Nishida , Toshiaki Doi
发明人： Ashina Yoshiro , Yasumasa Yamaguchi , Masashi Nishida , Toshiaki Doi
IPC分类号： C07B63/00 , B01D71/24 , C07B31/00 , C07C67/00 , C07C231/00 , C07C231/24 , C07C233/09 , C12P1/00 , C12P13/02
CPC分类号： C12P13/02 , B01D61/14 , B01D63/02 , B01D65/02 , B01D71/26 , C12P1/00 , B01D2321/04 , B01D2321/164
摘要： A method for purifying a reaction solution obtained by using a microbial cell, an immobilized microbial cell, or an immobilized enzyme as a catalyst in a water medium is disclosed. The method comprises repeatedly filtering the reaction solution to remove fine solid matter using a polyethylene porous hollow fiber membrane having a bubble point of from 1 to 20 kg/cm.sup.2, and repeatedly washing the hollow fiber membrane before it has been clogged to such an extent that a differential pressure thereof exceeds 3 kg/cm.sup.2. By this method, a filter membrane can be repeatedly regenerated at high efficiency and can stably be used for a long period of time.
摘要翻译：公开了一种在水介质中纯化通过使用微生物细胞，固定化微生物细胞或固定化酶作为催化剂获得的反应溶液的方法。该方法包括使用泡点为1至20kg / cm2的聚乙烯多孔中空纤维膜，反复过滤反应溶液以除去细小的固体物质，并且在中空纤维膜被堵塞之前反复洗涤至如此程度，其压差超过3kg / cm 2。通过这种方法，可以高效率地重复地再生过滤膜，并且可以长时间稳定地使用。

10. 发明授权

US4414331A Process for producing a highly concentrated aqueous acrylamide solution by means of microorganisms 失效
标题翻译：通过微生物生产高浓度丙烯酰胺水溶液的方法
公开(公告)号：US4414331A
公开(公告)日：1983-11-08
申请号：US160792
申请日：1980-06-19
申请人： Ichiro Watanabe , Yoshiaki Satoh , Yasumasa Yamaguchi
发明人： Ichiro Watanabe , Yoshiaki Satoh , Yasumasa Yamaguchi
IPC分类号： C07C233/09 , C12P13/02 , C12N11/04 , C12R1/00 , C12R1/07 , C12R1/13 , C12R1/15 , C12R1/265 , C12R1/365
CPC分类号： C12P13/02 , Y10S435/813 , Y10S435/819 , Y10S435/822 , Y10S435/832 , Y10S435/84 , Y10S435/843 , Y10S435/859 , Y10S435/872
摘要： A process for producing acrylamide from acrylonitrile by utilizing a microorganism or enzyme capable of hydrating acrylonitrile into acrylamide in the form of a highly concentrated aqueous solution of acrylamide which comprises bringing acrylonitrile in contact with the microorganism or enzyme in an aqueous medium at a pH of from 6 to 10, at a temperature of from the freezing point to 50.degree. C., and under such conditions that the concentration of acrylamide in the reaction solution after the completion of the reaction is from 5% by weight to less than 20% by weight, and concentrating the resulting reaction solution; this invention further includes an embodiment wherein the reaction solution is concentrated by cooling the reaction solution after the reaction to from -4.degree. C. to -9.degree. C. to crystallize ice, separating the ice, and using the ice so separated for cooling during the hydration reaction. In addition, this invention includes an embodiment wherein the concentrated solution obtained by the above embodiment is further concentrated by evaporating the water contained in the concentrated solution.
摘要翻译：通过使用能够将丙烯腈水合至丙烯酰胺的微生物或酶以丙烯酰胺的高度浓缩水溶液的形式从丙烯腈制备丙烯酰胺的方法，其包括使丙烯腈与微生物或酶接触的水性介质中，pH为在冰点至50℃的温度下，在反应溶液中丙烯酰胺浓度为5重量％至小于20重量％的条件下，并浓缩得到的反应溶液; 本发明还包括一个实施方案，其中通过将反应溶液冷却至-4℃至-9℃来浓缩反应溶液，使冰结晶，分离冰，并使用冰分离以冷却水化反应。此外，本发明包括其中通过蒸发浓缩溶液中包含的水进一步浓缩由上述实施方案获得的浓缩溶液的实施方案。

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