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1. 发明授权

US06379814B1 Cyclic urea-formaldehyde prepolymer for use in phenol-formaldehyde and melamine-formaldehyde resin-based binders 有权
标题翻译：用于苯酚 - 甲醛和三聚氰胺 - 甲醛树脂的粘合剂的环状脲 - 甲醛预聚物
公开(公告)号：US06379814B1
公开(公告)日：2002-04-30
申请号：US09948047
申请日：2001-09-07
申请人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
发明人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
IPC分类号： B32B2158
CPC分类号： C08L61/28 , C08G12/422 , C08G14/12 , C08L61/06 , C08L75/02 , Y10T428/2826 , Y10T428/31888 , Y10T428/31895 , Y10T428/31957 , C08L2666/20 , C08L61/20
摘要： The preparation of phenol-formaldehyde and melamine-formaldehyde resin-based binders extended with a cyclic urea-formaldehyde prepolymer and to products prepared using the binders. More particularly, the invention relates to a cyclic urea prepolymer comprising urea, formaldehyde, and ammonia or a primary amine which, when added to a phenol-formaldehyde or melamine-formaldehyde based resin, results in a useful binder for the manufacturer numerous articles.
摘要翻译：用环状脲 - 甲醛预聚物制备苯酚 - 甲醛和三聚氰胺 - 甲醛树脂基粘合剂以及使用粘合剂制备的产品。更具体地说，本发明涉及包含尿素，甲醛和氨或伯胺的环状脲预聚物，当加入到苯酚 - 甲醛或三聚氰胺 - 甲醛基树脂中时，可以制造出许多制品的有用的粘合剂。

2. 发明授权

US06706845B2 Low formaldehyde emission phenol-formaldehyde resin and method for manufacture thereof 有权
标题翻译：低甲醛释放酚醛树脂及其制造方法
公开(公告)号：US06706845B2
公开(公告)日：2004-03-16
申请号：US09989692
申请日：2001-11-21
申请人： W. Hayes Ingram , Ted M. McVay , Mary Letchas
发明人： W. Hayes Ingram , Ted M. McVay , Mary Letchas
IPC分类号： C08G1404
CPC分类号： C08G14/10 , C08G8/10 , C08G8/28 , C08G14/08 , C08L61/06 , C08L61/14
摘要： Phenol formaldehyde resins that have low free formaldehyde when produced, that maintain their low free formaldehyde levels during storage, and that demonstrate low levels of formaldehyde emissions during processing, curing, and thereafter.
摘要翻译：苯甲醛树脂在生产时具有低游离甲醛，在储存期间维持其低游离甲醛水平，并且在加工，固化和此后显示低水平的甲醛释放。

3. 发明授权

US06432254B1 Wood composite prepared with a B-stageable resin 失效
标题翻译：用B级树脂制备木材复合材料
公开(公告)号：US06432254B1
公开(公告)日：2002-08-13
申请号：US08979759
申请日：1997-11-26
申请人： Eric P. Black , Michael E. Hittmeier , W. Hayes Ingram , R. Scott Johnson
发明人： Eric P. Black , Michael E. Hittmeier , W. Hayes Ingram , R. Scott Johnson
IPC分类号： C09J502
CPC分类号： B27N3/002 , C08L97/02 , C08L2666/16
摘要： A method for making a consolidated wood product comprising coating wood components with a B-stageable, phenol-formaldehyde resole resin; heating the coated wood components to about 80 to 140° C. for a time sufficient to advance the resin to a B-stage; forming a mat or stack of the wood components coated with the B-stage resin; exposing the mat or stack of coated wood components to a saturated or superheated steam atmosphere in a hot press; and compressing the layup to form the consolidated wood product. The phenol-formaldehyde resole resin used in the method has a number average molecular weight of between about 200 and 600, has a F:P mole ratio of about 1.3:1 to 2.0:1, and has been modified with 0 to about 5.5 wt % of caustic based on resin solids.
摘要翻译：一种用于制备固结木制品的方法，包括用B阶段的苯酚 - 甲醛甲阶酚醛树脂涂覆木材组分; 将涂覆的木质部件加热至约80至140℃，持续一段足以将树脂推进到B阶段的时间; 形成涂有B阶树脂的木材组分的垫子或叠层; 在热压机中将涂覆的木质部件的垫或堆叠暴露于饱和或过热蒸汽气氛中; 并压制叠层以形成固结木制品。该方法中使用的苯酚 - 甲醛甲阶酚醛树脂的数均分子量为约200-600，F:P摩尔比为约1.3:1至2.0:1，并用0至约5.5重量％基于树脂固体的苛性碱的百分比。

4. 发明授权

US06369171B1 Cyclic urea-formaldehyde prepolymer for use in phenol-formaldehyde and melamine-formaldehyde resin-based binders 有权
公开(公告)号：US06369171B1
公开(公告)日：2002-04-09
申请号：US09735624
申请日：2000-12-14
申请人： Frederick C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
发明人： Frederick C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
IPC分类号： C08G828
摘要： The preparation of phenol-formaldehyde and melamine formaldehyde resin-based binders extended with a cyclic urea-formaldehyde prepolymer and to products prepared using the binders. More particularly, the invention relates to a cyclic urea prepolymer comprising urea, formaldehyde, and ammonia or a primary amine which, when added to a phenol-formaldehyde or melamine-formaldehyde based resin, results in a useful binder for the manufacturer numerous articles.

5. 发明授权

US06245438B1 Cyclic urea-formaldehyde prepolymer for use in phenol-formaldehyde and melamine-formaldehyde resin-based binders 有权
公开(公告)号：US06245438B1
公开(公告)日：2001-06-12
申请号：US09598894
申请日：2000-06-22
申请人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M. McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
发明人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M. McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
IPC分类号： B32B2308
CPC分类号： C08L61/06 , C08G12/422 , C08G14/12 , C08L61/28 , C08L75/02 , Y10T428/12146 , Y10T428/12153 , Y10T428/31862 , Y10T428/31873 , Y10T428/31877 , Y10T428/31895 , Y10T428/31957 , C08L61/20 , C08L2666/20
摘要： The preparation of phenol-formaldehyde and melamine-formaldehyde resin-based binders extended with a cyclic urea-formaldehyde prepolymer and to products prepared using the binders. More particularly, the invention relates to a cyclic urea prepolymer comprising urea, formaldehyde, and ammonia or a primary amine which, when added to a phenol-formaldehyde or melamine-formaldehyde based resin, results in a useful binder for the manufacturer numerous articles.

6. 发明授权

US06706809B2 Resin/binder system for preparation of low odor fiberglass products 有权
标题翻译：用于制备低气味玻璃纤维制品的树脂/粘合剂体系
公开(公告)号：US06706809B2
公开(公告)日：2004-03-16
申请号：US09989708
申请日：2001-11-21
申请人： Kim Tutin , W. Hayes Ingram , Mary L. Epling , Kurt D. Gabrielson , James T. Wright , Carl R. White
发明人： Kim Tutin , W. Hayes Ingram , Mary L. Epling , Kurt D. Gabrielson , James T. Wright , Carl R. White
IPC分类号： C08L6134
CPC分类号： C03C25/26 , C03C25/34 , C08G8/06 , C08G8/28 , C08G14/06 , C08L61/14
摘要： Infinitely water soluble, storage stable, low molecular weight, amine-modified resins/binders (e.g., phenol-formaldehyde resole resins and binders made therefrom) are used to produce low odor fiberglass products, such as fiberglass insulation for automobile headliners and room dividers. The cured, bonded fiberglass products have low TMA (trimethylamine) emission because the free formaldehyde in the resin has been scavenged with melamine, which resists thermal decomposition, and because the binder contains a relatively low urea content, which is a TMA contributor. The resole resin production process includes adding two different formaldehyde scavengers (e.g., melamine and urea) to produce a modified phenol-formaldehyde resole resin. This resole resin is produced into a binder by mixing with water, optionally in the presence of a latent acid catalyst (e.g., an ammonium salt of a strong acid). The binder can be applied to a fiberglass base material, dried, stored for an extended time period, and then cured and shaped into a final desired shape.
摘要翻译：无机水溶性，储存稳定的低分子量胺改性树脂/粘合剂（例如苯酚 - 甲醛甲阶酚醛树脂和由其制成的粘合剂）用于生产低气味玻璃纤维产品，例如用于汽车头饰和室内分隔器的玻璃纤维绝缘体。固化的粘合玻璃纤维产品具有低TMA（三甲胺）排放，因为树脂中的游离甲醛已经被三聚氰胺清除，因此耐热分解，并且由于粘合剂含有较低的尿素含量，这是TMA贡献者。甲阶酚醛树脂的生产方法包括加入两种不同的甲醛清除剂（如三聚氰胺和尿素）以生产改性的酚醛树脂树脂。任选地在潜酸催化剂（例如强酸的铵盐）的存在下，将该甲阶酚醛树脂与水混合制成粘合剂。粘合剂可以应用于玻璃纤维基材，干燥，长时间储存，然后固化并成型为最终所需的形状。

7. 发明授权

US6114491A Cyclic urea-formaldehyde prepolymer for use in phenol-formaldehyde and melamine-formaldehyde resin-based binders 有权
公开(公告)号：US6114491A
公开(公告)日：2000-09-05
申请号：US215742
申请日：1998-12-17
申请人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M. McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
发明人： F. C. Dupre , Millard E. Foucht , William P. Freese , Kurt D. Gabrielson , Benjamin D. Gapud , W. Hayes Ingram , Ted M. McVay , Richard A. Rediger , Kelly A. Shoemake , Kim K. Tutin , James T. Wright
IPC分类号： C08G12/42 , C08G14/12 , C08L61/06 , C08L61/10 , C08L61/28 , C08L75/02 , C08G14/04 , C08G8/10 , C08G8/28
CPC分类号： C08L61/06 , C08G12/422 , C08G14/12 , C08L61/28 , C08L75/02 , Y10T428/12146 , Y10T428/12153
摘要： The preparation of phenol-formaldehyde and melamine-formaldehyde resin-based binders extended with a cyclic urea-formaldehyde prepolymer and to products prepared using the binders. More particularly, the invention relates to a cyclic urea prepolymer comprising urea, formaldehyde, and ammonia or a primary amine which, when added to a phenol-formaldehyde or melamine-formaldehyde based resin, results in a useful binder for the manufacturer numerous articles.

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