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    • 2. 发明申请
    • LOW PRESSURE HIGH FREQUENCY PULSED PLASMA REACTOR FOR PRODUCING NANOPARTICLES
    • 低压高频脉冲等离子体反应器生产纳米二氧化碳
    • US20130189446A1
    • 2013-07-25
    • US13060722
    • 2009-09-01
    • James A. CaseyVasgen Shamamian
    • James A. CaseyVasgen Shamamian
    • C23C16/24B01F13/00
    • C23C16/24B01F13/0001B01J2/04B82Y40/00H01J37/32082H01J2237/339Y10S977/891
    • The present invention provides a low-pressure very high frequency pulsed plasma reactor system for synthesis of nanoparticles. The system includes a chamber configured to receive at least one substrate and capable of being evacuated to a selected pressure. The system also includes a plasma source for generating a plasma from at least one precursor gas and a very high frequency radio frequency power source for providing continuous or pulsed radio frequency power to the plasma at a selected frequency. The frequency is selected based on a coupling efficiency between the pulsed radio frequency power and the plasma. Parameters of the VHF discharge and gas precursors are selected based on nanoparticle properties. The nanoparticle average size and particle size distribution are manipulated by controlling the residence time of the glow discharge (pulsing plasma) relative to the gas molecular residence time through the discharge and the mass flow rates of the nanoparticle precursor gas (or gases).
    • 本发明提供了一种用于合成纳米颗粒的低压超高频脉冲等离子体反应器系统。 该系统包括被配置为容纳至少一个基板并能够被抽空到选定压力的腔室。 该系统还包括用于从至少一个前体气体产生等离子体的等离子体源和用于以选定频率向等离子体提供连续或脉冲射频功率的非常高频率的射频电源。 基于脉冲射频功率和等离子体之间的耦合效率选择频率。 基于纳米颗粒性质选择VHF排放和气体前体的参数。 通过控制辉光放电(脉冲等离子体)相对于通过放电的气体分子停留时间和纳米颗粒前体气体(或气体)的质量流量的停留时间来操纵纳米颗粒平均尺寸和粒度分布。