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1. 发明申请

WO2009141377A1 PROCESS FOR PREPARING AN 1,2-ALKYLENE CARBONATE 审中-公开
标题翻译：制备1,2-亚烷基碳酸酯的方法
公开(公告)号：WO2009141377A1
公开(公告)日：2009-11-26
申请号：PCT/EP2009/056134
申请日：2009-05-20
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis Leonardus Maria
发明人： VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis Leonardus Maria
IPC分类号： C07D317/36 , C07D317/38 , C07C29/12
CPC分类号： C07D317/36 , C07C29/12 , C07C68/065 , C07D317/38 , C07C31/202 , C07C69/96
摘要： The invention relates to a process for producing an 1,2-alkylene carbonate comprising (i) transporting liquid carbon dioxide to an 1,2-alkylene carbonate production plant; (ii) feeding the liquid carbon dioxide to an evaporation vessel; (iii) evaporating the liquid carbon dioxide such that a partial pressure of gaseous carbon dioxide of at least 5 x 10 5 N/m 2 is generated; (iv) feeding the gaseous carbon dioxide to a reactor; and (v) contacting the gaseous carbon dioxide with an 1,2- alkylene oxide and a carbonation catalyst to produce 1,2- alkylene carbonate.
摘要翻译：本发明涉及一种生产1,2-亚烷基碳酸酯的方法，其包括（i）将液体二氧化碳输送到1,2-亚烷基碳酸酯生产设备中; （ii）将液体二氧化碳供给到蒸发容器中; （iii）蒸发液态二氧化碳，使得产生至少5×10 5 N / m 2的气态二氧化碳分压; （iv）将气态二氧化碳送入反应器; 和（v）使气态二氧化碳与1,2-环氧烷和碳酸化催化剂接触以产生1,2-亚烷基碳酸酯。

2. 发明申请

WO2011067263A1 PROCESS FOR PREPARING DIARYL CARBONATES 审中-公开
标题翻译：制备二氧化碳的方法
公开(公告)号：WO2011067263A1
公开(公告)日：2011-06-09
申请号：PCT/EP2010/068568
申请日：2010-11-30
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , NISBET, Timothy Michael , VAPORCIYAN, Garo Garbis , VROUWENVELDER, Cornelis Leonardus Maria
发明人： NISBET, Timothy Michael , VAPORCIYAN, Garo Garbis , VROUWENVELDER, Cornelis Leonardus Maria
IPC分类号： C07C68/06 , C07C69/96 , B01D3/00
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention relates to a process for preparing a diaryl carbonate from a dialkyl carbonate and an aryl alcohol comprising: (a) introducing dialkyl carbonate and aryl alcohol into a first reactive distillation column; (b) recovering from the first reactive distillation column a top stream comprising dialkyl carbonate and alkyl alcohol and a bottom stream comprising alkyl aryl carbonate, aryl alcohol and dialkyl carbonate; (c) introducing the bottom stream from the first reactive distillation column into a second reactive distillation column; (d) recovering from the second reactive distillation column a top stream comprising dialkyl carbonate and a bottom stream comprising alkyl aryl carbonate, diaryl carbonate and aryl alcohol; (e) introducing the bottom stream from the second reactive distillation column into a third reactive distillation column; and (f ) recovering from the third reactive distillation column a top stream comprising aryl alcohol and a bottom stream comprising diaryl carbonate, wherein the top stream from the third reactive distillation column is recycled to the second reactive distillation column.
摘要翻译：本发明涉及一种由碳酸二烷基酯和芳基醇制备碳酸二芳基酯的方法，该方法包括：（a）将碳酸二烷基酯和芳基醇引入第一反应蒸馏塔; （b）从第一反应蒸馏塔回收包含碳酸二烷基酯和烷基醇的顶部料流和包含碳酸烷基芳基酯，芳基醇和碳酸二烷基酯的塔底料流; （c）将来自第一反应蒸馏塔的塔底物流引入第二反应蒸馏塔; （d）从第二反应蒸馏塔回收包含碳酸二烷基酯和包含碳酸烷基芳基酯，碳酸二芳基酯和芳基醇的塔底料流; （e）将来自第二反应蒸馏塔的塔底物流引入第三反应蒸馏塔; 和（f）从第三反应蒸馏塔回收包含芳基醇的顶部料流和包含碳酸二芳基酯的塔底料流，其中来自第三反应蒸馏塔的顶部料流再循环到第二反应蒸馏塔。

3. 发明申请

WO2008129030A1 PROCESS FOR THE PREPARATION OF AN 1,2-ALKYLENE DIOL AND A DIALKYLCARBONATE 审中-公开
标题翻译：制备1,2-亚苄基二醇和二碳酸氢钠的方法
公开(公告)号：WO2008129030A1
公开(公告)日：2008-10-30
申请号：PCT/EP2008/054798
申请日：2008-04-21
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis Leonardus Maria
发明人： VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis Leonardus Maria
IPC分类号： C07C29/10 , C07C31/20
CPC分类号： C07C68/065 , C07C69/96
摘要： The present invention relates to a process for the preparation of an 1,2-alkylene diol and a dialkylcarbonate, comprising the steps of (i) contacting an 1,2-alkylene oxide with carbon dioxide in the presence of a carbonation catalyst in a downflow jet reactor to obtain a reaction mixture containing an 1,2-alkylene carbonate, wherein the downflow jet reactor further comprises a deflection means situated in between the ejector means and the outlet means in the direction of the flow path of the gas/liquid mixture generated by the ejector means; (ii) contacting at least part of the reaction mixture obtained in step (i) with an alkanol to obtain a reaction mixture containing an 1,2-alkylene diol and a dialkylcarbonate; and (iii) recovering the 1,2-alkylene diol and the dialkylcarbonate from the reaction mixture obtained in step (ii).
摘要翻译：本发明涉及一种制备1,2-亚烷基二醇和碳酸二烷基酯的方法，包括以下步骤：（i）在碳酸化催化剂存在下使1,2-环氧烷与二氧化碳在下流以获得含有1,2-亚烷基碳酸酯的反应混合物，其中所述下流喷射反应器还包括位于所述喷射装置和所述出口装置之间的偏转装置，所述偏转装置沿所述气/液混合物的流动路径的方向产生通过喷射器装置; （ii）将步骤（i）中获得的反应混合物的至少一部分与烷醇接触，得到含有1,2-亚烷基二醇和碳酸二烷基酯的反应混合物; 和（iii）从步骤（ii）中获得的反应混合物中回收1,2-亚烷基二醇和碳酸二烷基酯。

4. 发明申请

WO2010046320A1 PROCESS FOR REMOVING AN ALKANOL IMPURITY FROM AN ORGANIC CARBONATE STREAM 审中-公开
标题翻译：从有机碳酸盐流中去除碱金属污染物的方法
公开(公告)号：WO2010046320A1
公开(公告)日：2010-04-29
申请号：PCT/EP2009/063606
申请日：2009-10-16
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , VAN DER HEIDE, Evert , VAPORCIYAN, Garo , Garbis , VROUWENVELDER, Cornelis , Leonardus , Maria
发明人： VAN DER HEIDE, Evert , VAPORCIYAN, Garo , Garbis , VROUWENVELDER, Cornelis , Leonardus , Maria
IPC分类号： C07C68/08 , C07C68/06 , C07C69/96
CPC分类号： C07C68/06 , C07C68/065 , C07C68/08 , C07C69/96
摘要： The invention relates to a process for removing an alkanol impurity from a stream containing an organic carbonate and the alkanol impurity, comprising contacting the stream with a catalyst to effect reaction of the alkanol impurity with the organic carbonate.
摘要翻译：本发明涉及一种从含有机碳酸盐和链烷醇杂质的流中除去烷醇杂质的方法，包括使该物流与催化剂接触以使链烷醇杂质与有机碳酸酯反应。

5. 发明申请

WO2004089866A1 PROCESS FOR THE PREPARATION OF ALKANEDIOL 审中-公开
标题翻译：制备阿尔卡尼醇的方法
公开(公告)号：WO2004089866A1
公开(公告)日：2004-10-21
申请号：PCT/EP2004/050480
申请日：2004-04-07
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , HARMSEN, Gerrit, Jan , VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis, Leonardus, Maria
发明人： HARMSEN, Gerrit, Jan , VAN DER HEIDE, Evert , VROUWENVELDER, Cornelis, Leonardus, Maria
IPC分类号： C07C68/06
CPC分类号： C07C29/12 , C07C31/205
摘要： Process for the preparation of alkanediol, which process comprises (a) contacting alkylene oxide with carbon dioxide in the presence of catalyst to obtain a first liquid reaction mixture containing cyclic carbonate, (b) optionally removing carbon dioxide and/or alkylene oxide, (c) increasing the pressure of the liquid reaction mixture obtained in step (a) and/or (b), (d) contacting the pressurized first reaction mixture obtained in step (c) with water in the presence of catalyst to obtain a second reaction mixture containing alkanediol and carbon dioxide, (e) separating the second reaction mixture into a liquid effluent and a gaseous effluent containing carbon dioxide, and (f) recycling at least part of the gaseous effluent containing carbon dioxide to step (a), in which process the pressure in step (d) is higher than the pressure in step (a).
摘要翻译：用于制备链烷二醇的方法，该方法包括（a）在催化剂存在下使环氧烷与二氧化碳接触以获得含有环状碳酸酯的第一液体反应混合物，（b）任选地除去二氧化碳和/或氧化烯，（c ）增加步骤（a）和/或（b）中获得的液体反应混合物的压力，（d）在催化剂存在下使步骤（c）中获得的加压第一反应混合物与水接触，得到第二反应混合物（e）将第二反应混合物分离成液体流出物和含二氧化碳的气态流出物，和（f）将至少部分含有二氧化碳的气态流出物再循环到步骤（a）中，其中在该过程中步骤（d）中的压力高于步骤（a）中的压力。

6. 发明申请

WO2002098829A1 SEPARATION METHOD 审中-公开
标题翻译：分离方法
公开(公告)号：WO2002098829A1
公开(公告)日：2002-12-12
申请号：PCT/EP2002/006315
申请日：2002-06-06
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , VROUWENVELDER, Cornelis, Leonardus, Maria
发明人： VROUWENVELDER, Cornelis, Leonardus, Maria
IPC分类号： C07C29/80
CPC分类号： C07C29/80 , C07C31/205
摘要： Method for separating monopropylene glycol from a mixture comprising monopropylene glycol and propylene carbonate, wherein the mixture is subjected to distillation at such temperature and pressure that a monopropylene glycol product is distilled off and condensed, which monopropylene glycol product comprises less than 1.0 wt% propylene carbonate.
摘要翻译：从包含单丙二醇和碳酸亚丙酯的混合物中分离单丙二醇的方法，其中将混合物在这样的温度和压力下进行蒸馏，从而蒸馏出并缩合单丙二醇产物，该单丙二醇产物包含小于1.0重量％的碳酸亚丙酯。

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