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1. 发明授权

US08505478B2 Apparatus for high-efficiency synthesis of carbon nanostructure 有权
标题翻译：碳纳米结构高效合成装置
公开(公告)号：US08505478B2
公开(公告)日：2013-08-13
申请号：US12805528
申请日：2010-08-04
申请人： Osamu Suekane , Toshikazu Nosaka , Yoshikazu Nakayama , Lujun Pan , Takeshi Nagasaka , Toru Sakai , Hiroyuki Tsuchiya , Toshiki Goto , Xu Li
发明人： Osamu Suekane , Toshikazu Nosaka , Yoshikazu Nakayama , Lujun Pan , Takeshi Nagasaka , Toru Sakai , Hiroyuki Tsuchiya , Toshiki Goto , Xu Li
IPC分类号： C23C16/52 , C23C16/455 , C23F1/00 , H01L21/306 , C23C16/06 , C23C16/22
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/30
摘要： Developed is high-efficiency synthesis method and apparatus capable of promoting the initial growth of carbon nanostructure by eliminating the initial fluctuation time and rising time in raw gas flow quantity.-A high-efficiency synthesis method of carbon nanostructure according to the present invention is a high-efficiency synthesis method of carbon nanostructure, the method comprising: bringing raw material gas and a catalyst into contact with each other under reactive conditions so as to produce a carbon nanostructure, wherein: the initiation of contact of the raw material gas with the catalyst is carried out instantaneously. Reaction conditions such as temperature and raw material gas concentration are set so as to meet those for catalyst growth, and under the reaction conditions, the initiation of contact of raw material gas G with catalyst 6 is carried out instantaneously. Consequently, the initial growth of carbon nanostructure is positively carried out, and the height growth and thickness growth thereof can be effected in high efficiency. Further, high-density growth and short-time high-speed growth can be realized. The catalyst includes any forms of catalyst such as catalyst substrate, catalyst structure, catalyst powders and catalyst pellet. It is especially preferred to employ a system wherein the feed and interruption of the raw material gas G are intermittently controlled by means of an electromagnetic three-way valve 24.
摘要翻译：开发了能够通过消除原始气体流量的初始波动时间和上升时间来促进碳纳米结构的初始生长的高效合成方法和装置。根据本发明的碳纳米结构的高效合成方法是碳纳米结构的高效合成方法，其特征在于，在反应条件下使原料气体和催化剂相互接触，制成碳纳米结构体，其中：原料气与催化剂的接触开始是瞬间进行的。反应条件如温度和原料气体浓度设定为满足催化剂生长的条件，在反应条件下，原料气体G与催化剂6的接触开始立即进行。因此，积极地进行碳纳米结构的初始生长，并且可以高效率地实现其高度生长和厚度生长。此外，可以实现高密度生长和短时高速生长。催化剂包括任何形式的催化剂，如催化剂底物，催化剂结构，催化剂粉末和催化剂颗粒。特别优选采用通过电磁三通阀24间歇地控制原料气体G的进料和中断的系统。

2. 发明授权

US07790228B2 Method for high-efficiency synthesis of carbon nanostructure 有权
标题翻译：碳纳米结构高效合成方法
公开(公告)号：US07790228B2
公开(公告)日：2010-09-07
申请号：US10551051
申请日：2004-03-23
申请人： Osamu Suekane , Toshikazu Nosaka , Yoshikazu Nakayama , Lujun Pan , Takeshi Nagasaka , Toru Sakai , Hiroyuki Tsuchiya , Toshiki Goto , Xu Li
发明人： Osamu Suekane , Toshikazu Nosaka , Yoshikazu Nakayama , Lujun Pan , Takeshi Nagasaka , Toru Sakai , Hiroyuki Tsuchiya , Toshiki Goto , Xu Li
IPC分类号： C23C16/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/30
摘要： Developed is high-efficiency synthesis method and apparatus capable of promoting the initial growth of carbon nanostructure by eliminating the initial fluctuation time and rising time in raw gas flow quantity.A high-efficiency synthesis method of carbon nanostructure according to the present invention is a high-efficiency synthesis method of carbon nanostructure, the method comprising: bringing raw material gas and a catalyst into contact with each other under reactive conditions so as to produce a carbon nanostructure, wherein: the initiation of contact of the raw material gas with the catalyst is carried out instantaneously. Reaction conditions such as temperature and raw material gas concentration are set so as to meet those for catalyst growth, and under the reaction conditions, the initiation of contact of raw material gas G with catalyst 6 is carried out instantaneously. Consequently, the initial growth of carbon nanostructure is positively carried out, and the height growth and thickness growth thereof can be effected in high efficiency. Further, high-density growth and short-time high-speed growth can be realized. The catalyst includes any forms of catalyst such as catalyst substrate, catalyst structure, catalyst powders and catalyst pellet. It is especially preferred to employ a system wherein the feed and interruption of the raw material gas G are intermittently controlled by means of an electromagnetic three-way valve 24.
摘要翻译：开发了通过消除原始气体流量的初始波动时间和上升时间，可以促进碳纳米结构初始生长的高效合成方法和装置。根据本发明的碳纳米结构的高效合成方法是碳纳米结构的高效合成方法，该方法包括：使原料气体和催化剂在反应条件下彼此接触，以产生碳纳米结构，其中：原料气体与催化剂的接触开始立即进行。反应条件如温度和原料气体浓度设定为满足催化剂生长的条件，在反应条件下，原料气体G与催化剂6的接触开始立即进行。因此，积极地进行碳纳米结构的初始生长，并且可以高效率地实现其高度生长和厚度生长。此外，可以实现高密度生长和短时高速生长。催化剂包括任何形式的催化剂，如催化剂底物，催化剂结构，催化剂粉末和催化剂颗粒。特别优选采用通过电磁三通阀24间歇地控制原料气体G的进料和中断的系统。

3. 发明授权

US07651668B2 Production method and production device for carbon nano structure 失效
标题翻译：碳纳米结构的生产方法和生产装置
公开(公告)号：US07651668B2
公开(公告)日：2010-01-26
申请号：US11663451
申请日：2005-09-21
申请人： Yoshikazu Nakayama , Hiroyuki Tsuchiya , Yugo Higashi , Toshiki Goto , Keisuke Shiono , Takeshi Nagasaka , Nobuharu Okazaki
发明人： Yoshikazu Nakayama , Hiroyuki Tsuchiya , Yugo Higashi , Toshiki Goto , Keisuke Shiono , Takeshi Nagasaka , Nobuharu Okazaki
IPC分类号： B01J8/18 , F27B15/14 , B01J19/18 , B01J19/00 , C01B31/02
CPC分类号： B82Y40/00 , B01J8/008 , B01J8/1818 , B01J8/1836 , B01J23/825 , B01J23/835 , B01J2208/00212 , B01J2208/00548 , B01J2219/00006 , B82Y30/00 , C01B32/05 , C01B32/162
摘要： A material gas and a catalyst are introduced through a material supplying tube path and a catalyst supplying tube path together with a carrier gas into a reactor equipped on its outer periphery with a heat applicator for thermally decomposing the material gas. The reactor has a convention regulator fitted to the discharge end of the catalyst supplying tube path. The convection regulator covers an edge side of the reactor to regulate gas flow in the reactor so that the flow does not reach the edge side. Due to this, a convection state can be efficiently produced in a reaction region. Consequently, it becomes possible to prevent contamination defect caused by accumulation/adherence of concretion of catalyst, which was generated by aggregation of cooled catalyst in the low-temperature region of the reactor and a decomposition product of the material gas. Thus the efficiency of carbon nanostructure production can be improved.
摘要翻译：将材料气体和催化剂通过材料供给管路和催化剂供给管路与载气一起引入装配在其外周的反应器中，并具有用于热分解原料气体的热施加器。反应器具有安装在催化剂供给管路径的排出端的惯性调节器。对流调节器覆盖反应器的边缘侧，以调节反应器中的气流，使得流不到达边缘侧。由此，可以在反应区域中有效地产生对流状态。因此，可以防止由反应器的低温区域中的冷却的催化剂的聚集产生的催化剂的凝结的累积/粘附引起的污染缺陷和原料气体的分解产物。因此，可以提高碳纳米结构生产的效率。

4. 发明申请

US20080095694A1 Carbon-Based Fine Structure Array, Aggregate of Carbon-Based Fine Structures, Use Thereof and Method for Preparation Thereof 有权
标题翻译：碳基精细结构阵列，碳基精细结构聚集体及其制备方法及其制备方法
公开(公告)号：US20080095694A1
公开(公告)日：2008-04-24
申请号：US11578782
申请日：2005-04-19
申请人： Yoshikazu Nakayama , Toshikazu Nosaka , Osamu Suekane , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono
发明人： Yoshikazu Nakayama , Toshikazu Nosaka , Osamu Suekane , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono
IPC分类号： C01B31/02 , C01B31/00
CPC分类号： C01B31/00 , B82B1/00 , B82Y30/00 , B82Y40/00 , C01B32/00 , C01B32/158 , C01B32/162 , C01B2202/08 , Y10S977/742 , Y10T428/24372 , Y10T428/2918 , Y10T428/292
摘要： An aggregate of carbon-based fine structures in which a plurality of carbon-based fine structures are collected, wherein respective carbon-based fine structures are oriented in the same direction. The above aggregate of carbon-based fine structures is an aggregate of a plurality of carbon-based fine structures in a state they are pulled by one another with strong interaction, and has such a length that allows the improvement of the handleability and workability thereof.
摘要翻译：其中收集多个碳基微细结构的碳基微细结构的集合体，其中各个碳基微结构在相同方向上取向。上述碳系精细结构体的集合体是多个碳系微细结构体以彼此相互拉伸的状态相互作用的状态的集合体，并且具有允许提高其操作性和加工性的长度。

5. 发明授权

US4914260A Ceramic multi-layer printed circuit boards 失效
标题翻译：陶瓷多层印刷电路板
公开(公告)号：US4914260A
公开(公告)日：1990-04-03
申请号：US330761
申请日：1989-03-30
申请人： Go Suzuki , Toshiki Goto
发明人： Go Suzuki , Toshiki Goto
IPC分类号： H01L21/48 , H05K1/03 , H05K3/00 , H05K3/38 , H05K3/46
CPC分类号： H05K3/4667 , H01L21/4857 , H05K3/4661 , H05K1/0306 , H05K2201/09563 , H05K2201/096 , H05K3/0023 , H05K3/381
摘要： A ceramic multi-layer printed circuit board is manufactured by forming a wiring pattern layer on a ceramic substrate through copper plating and forming an insulating layer thereon and then repeating the steps for forming both layers.
摘要翻译：通过铜镀层在陶瓷基板上形成布线图案层并在其上形成绝缘层，然后重复形成两层的步骤来制造陶瓷多层印刷电路板。

6. 发明申请

US20090191352A1 Combustion-Assisted Substrate Deposition Method For Producing Carbon Nanosubstances 审中-公开
标题翻译：用于生产碳纳米管的燃烧辅助底物沉积方法
公开(公告)号：US20090191352A1
公开(公告)日：2009-07-30
申请号：US12019352
申请日：2008-01-24
申请人： Douglas P. DuFaux , Randy Vander Wal , Masato Tani , Toshiki Goto
发明人： Douglas P. DuFaux , Randy Vander Wal , Masato Tani , Toshiki Goto
IPC分类号： C23C4/04 , C23C16/01
CPC分类号： B01J37/0242 , B01J23/28 , B01J23/745 , B01J23/755 , B01J23/78 , B01J23/881 , B01J23/882 , B01J23/8892 , B01J37/0225 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/162 , C01B32/17
摘要： The present invention provides a combustion-based method and apparatus for producing and isolating carbon nanotubes. The nanotubes are formed when hot combustion gases are contacted with a catalytic surface, which is readily separated from the catalyst support and subsequently dissolved. The process is suitable for large-scale manufacture of carbon nanotubes.
摘要翻译：本发明提供一种用于制造和分离碳纳米管的基于燃烧的方法和装置。当热燃烧气体与催化剂表面接触时形成纳米管，催化表面容易与催化剂载体分离并随后溶解。该方法适用于大规模制造碳纳米管。

7. 发明申请

US20080063589A1 Production Method for Carbon Nano Structure of Catalyst Particle Diameter Control Mode, Production Device, and Carbon Nano Structure 审中-公开
标题翻译：催化剂粒径控制模式，生产装置和碳纳米结构碳纳米结构的生产方法
公开(公告)号：US20080063589A1
公开(公告)日：2008-03-13
申请号：US11632466
申请日：2005-07-13
申请人： Yoshikazu Nakayama , Takeshi Nagasaka , Toru Sakai , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono , Nobuharu Okazaki
发明人： Yoshikazu Nakayama , Takeshi Nagasaka , Toru Sakai , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono , Nobuharu Okazaki
IPC分类号： D01F9/12 , B01J8/08
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , D01F9/133
摘要： The subject invention provides a stable mass production method of carbon nano structure at low cost immune to variation of particle diameter of the catalyst microparticle in the catalyst material. The subject invention also provides a production device used for the method, and a new carbon nano structure having a conformation suitable for the mass production. The production method of carbon nano structure comprising fluidizing a material gas and catalyst microparticles in the reactor so that the material gas and the catalyst microparticles are brought into contact with each other, wherein said catalyst microparticles are suspended by the instantaneous spraying of the high-pressure gas, and then the suspension effect of the catalyst microparticles is stopped so that the catalyst microparticles naturally fall. The particle diameter of the catalyst microparticles is thus selected. With this arrangement, only the selected catalyst microparticles with the desired diameter are supplied to the reactor. Since this arrangement is immune to influence of variation in particle diameter of catalyst microparticles contained in the catalyst material, it achieves stable mass production of carbon nano structure at low cost.
摘要翻译：本发明提供一种低成本的碳纳米结构的稳定的大规模生产方法，其不受催化剂材料中催化剂微粒的粒径变化的影响。本发明还提供了一种用于该方法的生产装置和具有适于批量生产的构象的新型碳纳米结构。碳纳米结构体的制造方法，其特征在于，在所述反应器中使原料气体和催化剂微粒流化，使得原料气体和催化剂微粒相互接触，其中，所述催化剂微粒通过瞬时喷射高压气体，然后停止催化剂微粒的悬浮效果，使得催化剂微粒自然落下。因此选择催化剂微粒的粒径。利用这种布置，只有所选择的具有所需直径的催化剂微粒被提供给反应器。由于这种布置不受催化剂材料中所含的催化剂微粒的粒径变化的影响，因此以低成本实现了碳纳米结构的稳定的批量生产。

8. 发明申请

US20070098622A1 Catalyst for synthesizing carbon nanocoils, synthesizing method of the same, synthesizing method of carbon nanocoils, and carbon nanocoils 失效
标题翻译：用于合成碳纳米线的催化剂，其合成方法，碳纳米线和碳纳米薄膜的合成方法
公开(公告)号：US20070098622A1
公开(公告)日：2007-05-03
申请号：US10558291
申请日：2004-05-28
申请人： Yoshikazu Nakayama , Lujun Pan , Toshikazu Nosaka , Osamu Suekane , Nobuharu Okazaki , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Takashi Okawa , Keisuke Shiono
发明人： Yoshikazu Nakayama , Lujun Pan , Toshikazu Nosaka , Osamu Suekane , Nobuharu Okazaki , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Takashi Okawa , Keisuke Shiono
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B01J23/835 , B01J27/22 , B01J29/146 , B82Y40/00 , C01B32/18 , C01B32/90 , C01P2002/72 , C01P2004/03 , C01P2004/13 , C01P2006/16 , D01F9/127
摘要： A method for synthesizing carbon nanocoils with high efficiency, by determining the structure of carbon nuclei that have been attached to the ends of carbon nanocoils and thus specifying a true catalyst for synthesizing carbon nanocoils is implemented. The catalyst for synthesizing carbon nanocoils according to the present invention is a carbide catalyst that contains at least elements (a transition metal element, In, C) or (a transition metal element, Sn, C), and in particular, it is preferable for the transition metal element to be Fe, Co or Ni. In addition to this carbide catalyst, a metal catalyst of (Fe, Al, Sn) and (Fe, Cr, Sn) are effective. From among these, catalysts such as Fe3InC0.5, Fe3InC0.5Snw and Fe3SnC are particularly preferable. The wire diameter and the coil diameter can be controlled by using a catalyst where any of these catalysts is carried by a porous carrier.
摘要翻译：通过确定已经附着在碳纳米线的末端上的碳原子核的结构，从而确定了用于合成碳纳米线的真正的催化剂，实现了高效合成碳纳米线的方法。根据本发明的用于合成碳纳米薄膜的催化剂是至少含有元素（过渡金属元素，In，C）或（过渡金属元素Sn，C）的碳化物催化剂，特别地，优选过渡金属元素为Fe，Co或Ni。除了这种碳化物催化剂之外，（Fe，Al，Sn）和（Fe，Cr，Sn）的金属催化剂是有效的。其中，诸如Fe 3 N 3 C 5 N 3，Fe 3 InCl 0.5 Snw和Fe 3 O 3的催化剂， 3 SnC是特别优选的。线径和线圈直径可以通过使用其中任何这些催化剂由多孔载体承载的催化剂来控制。

9. 发明申请

US20130266764A1 CARBON-BASED FINE STRUCTURE ARRAY, AGGREGATE OF CARBON-BASED FINE STRUCTURES, USE THEREOF AND METHOD FOR PREPARATION THEREOF 有权
标题翻译：基于碳的精细结构阵列，基于碳的微细结构的聚集及其制备方法及其制备方法
公开(公告)号：US20130266764A1
公开(公告)日：2013-10-10
申请号：US13907276
申请日：2013-05-31
申请人： Yoshikazu NAKAYAMA , Toshikazu NOSAKA , Osamu SUEKANE , Takeshi NAGASAKA , Toshiki GOTO , Hiroyuki TSUCHIYA , Keisuke SHIONO
发明人： Yoshikazu NAKAYAMA , Toshikazu NOSAKA , Osamu SUEKANE , Takeshi NAGASAKA , Toshiki GOTO , Hiroyuki TSUCHIYA , Keisuke SHIONO
IPC分类号： C01B31/00
CPC分类号： C01B31/00 , B82B1/00 , B82Y30/00 , B82Y40/00 , C01B32/00 , C01B32/158 , C01B32/162 , C01B2202/08 , Y10S977/742 , Y10T428/24372 , Y10T428/2918 , Y10T428/292
摘要： An aggregate of carbon-based fine structures in which a plurality of carbon-based fine structures are collected, wherein respective carbon-based fine structures are oriented in the same direction. The above aggregate of carbon-based fine structures is an aggregate of a plurality of carbon-based fine structures in a state they are pulled by one another with strong interaction, and has such a length that allows the improvement of the handeability and workability thereof.
摘要翻译：其中收集多个碳基微细结构的碳基微细结构的集合体，其中各个碳基微结构在相同方向上取向。上述碳系微细组织的集合体是以相互作用强烈地拉伸的状态的多个碳系微细结构体的集合体，具有能够提高其可手性和加工性的长度。

10. 发明授权

US08481158B2 Carbon-based fine structure array, aggregate of carbon-based fine structures, use thereof and method for preparation thereof 有权
标题翻译：碳基精细结构体，碳基精细结构体，其用途及其制备方法
公开(公告)号：US08481158B2
公开(公告)日：2013-07-09
申请号：US11578782
申请日：2005-04-19
申请人： Yoshikazu Nakayama , Toshikazu Nosaka , Osamu Suekane , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono
发明人： Yoshikazu Nakayama , Toshikazu Nosaka , Osamu Suekane , Takeshi Nagasaka , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono
IPC分类号： D01F9/12
CPC分类号： C01B31/00 , B82B1/00 , B82Y30/00 , B82Y40/00 , C01B32/00 , C01B32/158 , C01B32/162 , C01B2202/08 , Y10S977/742 , Y10T428/24372 , Y10T428/2918 , Y10T428/292
摘要： An aggregate of carbon-based fine structures in which a plurality of carbon-based fine structures are collected, wherein respective carbon-based fine structures are oriented in the same direction. The above aggregate of carbon-based fine structures is an aggregate of a plurality of carbon-based fine structures in a state they are pulled by one another with strong interaction, and has such a length that allows the improvement of the handleability and workability thereof.
摘要翻译：其中收集多个碳基微细结构的碳基微细结构的集合体，其中各个碳基微结构在相同方向上取向。上述碳系精细结构体的集合体是多个碳系微细结构体以彼此相互拉伸的状态相互作用的状态的集合体，并且具有允许提高其操作性和加工性的长度。

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