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1. 发明授权

US08691002B2 Organic black pigments and their preparation 有权
标题翻译：有机黑色颜料及其制备方法
公开(公告)号：US08691002B2
公开(公告)日：2014-04-08
申请号：US13144940
申请日：2009-12-28
申请人： Thomas Eichenberger , Thomas Ruch , Ralf Bauer , Christoph Krebs , Ursula Luterbacher , Marc Maurer
发明人： Thomas Eichenberger , Thomas Ruch , Ralf Bauer , Christoph Krebs , Ursula Luterbacher , Marc Maurer
IPC分类号： C09D11/02 , C08K5/3417 , C07D405/14
CPC分类号： C09B57/00 , C07D405/04 , C07D493/04 , C08K5/0041 , C09B67/0034 , Y10T428/2982 , Y10T442/30
摘要： A process for preparing a black colorant, preferably a black pigment, characterized in that a compound of the Formula (I) is reacted with a compound of the Formula (II) in a molar ratio of 1:2, in the presence of a catalyst which in water at 25° C. has a pK≦4.5. For the definition of R1 to R7, refer to the description; preferably all are H. Likewise claimed are new crystal polymorphs obtainable by this process, and preferably single-phase mixed crystals. Also claimed are synergistic compositions. These compositions exhibit increased light stability in plastics stabilized with basic light stabilizers when they are pigmented with colorants of the invention rather than with known black pigments such as carbon black. The specification also relates, furthermore, to the use of the black colorants of the invention for coloring paints, printing inks and plastics in the mass, and to mulch film, instrument panels, woven fabrics, garden furniture items or elements for the construction industry that are pigmented with said colorants.
摘要翻译：一种制备黑色着色剂，优选黑色颜料的方法，其特征在于使式（I）化合物与摩尔比为1:2的式（II）化合物在催化剂存在下反应其在25℃的水中具有pK＆nlE; 4.5。关于R1〜R7的定义，请参考说明书; 优选全部为H.同样要求保护的是通过该方法可获得的新晶体多晶型物，优选单相混合晶体。还要求的是协同组合物。当用本发明的着色剂着色时，这些组合物在用碱性光稳定剂稳定的塑料中显示增强的光稳定性，而不是已知的黑色颜料如炭黑。此外，本说明书还涉及本发明的黑色着色剂用于在油漆中着色油漆，印刷油墨和塑料的用途，以及用于建筑行业的膜，仪表板，机织织物，花园家具或元件的覆盖用着色剂着色。

2. 发明申请

US20090012305A1 2-[[1-[[(2,3-Dihydro-2-Oxo-1H-Benzimidazol-5-Yl)Amino]Carbonyl]-2-Oxopropyl]Azo]-Benzoic Acid and a Process For Its Preparation 有权
标题翻译： 2 - [[1 - [[（2,3-二氢-2-氧代-1H-苯并咪唑-5-基）氨基]羰基] -2-氧代丙基]偶氮] - 苯甲酸及其制备方法
公开(公告)号：US20090012305A1
公开(公告)日：2009-01-08
申请号：US12087834
申请日：2007-01-08
申请人： Hans Reichert , Max Hugin , Ulrich Veith , Sibylle Soder , Thomas Eichenberger
发明人： Hans Reichert , Max Hugin , Ulrich Veith , Sibylle Soder , Thomas Eichenberger
IPC分类号： C07D235/26
CPC分类号： C07D235/26 , C09B29/32 , C09B67/0017
摘要： The present invention is directed to 2-[[1-[[(2,3-dihydro-2-oxo-1H-benzimidazol-5-yl)amino]carbonyl]-2-oxo-propyl]azo]-benzoic acid (C.I. Pigment Yellow 151): (I), characterized by a ΔE* (black/white) in masstone below 22.0±0.7, a process for its preparation and its use for pigmenting macromolecular organic materials of natural or synthetic origin. The pigment has high opacity and high color strength.
摘要翻译：本发明涉及2 - [[1 - [[（2,3-二氢-2-氧代-1H-苯并咪唑-5-基）氨基]羰基] -2-氧代 - 丙基]偶氮] - 苯甲酸（ CI颜料黄151）：（I），其特征在于低于22.0±0.7的熔体中的ΔE*（黑/白），其制备方法及其用于天然或合成来源的大分子有机材料的着色。该颜料具有高不透明度和高着色强度。

3. 发明授权

US07217803B2 Benzimidazole-pyridone-based azo dyes 失效
标题翻译：苯并咪唑 - 吡啶酮基偶氮染料
公开(公告)号：US07217803B2
公开(公告)日：2007-05-15
申请号：US10537063
申请日：2003-11-26
申请人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hügin
发明人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hügin
IPC分类号： C09B31/14 , C09B29/36 , C09B69/04 , D06P3/60
CPC分类号： C09B69/045 , C09B29/3617 , C09B31/14 , Y10S8/922
摘要： The present invention relates to azo dyes of formula (1) which are soluble in organic solvents, wherein R1 is —CN, —COOR5, —CONR6R7 or a heterocyclic ring, R2 is unsubstituted or substituted alkyl, unsubstituted or substituted aryl, —CF3, —COOR5, —CONR6R7 or —COR5, R3 is hydrogen, —SO3M, alkyl, alkoxy, alkylcarbonyl, —NO2 or halogen, R4 is substituted aryl, substituted heteroaryl or an aryl-N═N-aryl radical, wherein one or both of the aryl radicals in aryl-N═N-aryl is/are unsubstituted or substituted, or a radical heteroaryl-N═N-heteroaryl, wherein one or both of the heteroaryl radicals in heteroaryl-N═N-heteroaryl is/are unsubstituted or substituted, R5 is hydrogen, alkyl or unsubstituted or substituted aryl, R6 is hydrogen, alkyl or unsubstituted or substituted aryl, R7 is hydrogen, alkyl or unsubstituted or substituted aryl, M+ is a cation, n is a number 1, 2 or 3 and m is a number 1, 2 or 3, to a process for the preparation thereof and to the use thereof in the production of colored plastics or polymeric color particles, and as printing inks, printing dyes, coating compositions and wood stains
摘要翻译：本发明涉及可溶于有机溶剂的式（1）的偶氮染料，其中R 1是-CN，-COOR 5，-CONR 6 R 7或杂环R 2是未取代或取代的烷基，未取代或取代的芳基，-CF 3 - ， - COOR 5，-CONR 6 R 7或-COR 5，R 3，是氢，-SO 3 M，烷基，烷氧基，烷基羰基，-NO 2或卤素，R 4是取代的芳基，取代的杂芳基或芳基-NH-芳基，其中芳基-NH-芳基中的一个或两个芳基是未被取代或取代的，或者是杂芳基-NH-杂芳基，其中杂芳基-NN中的一个或两个杂芳基 - 杂芳基是未取代或取代的，R 5是氢，烷基或未取代或取代的芳基，R 6是氢，烷基或未取代或取代的芳基，R SUB > 7是氢，烷基或未取代的取代或取代的芳基，M + +是一种阳离子，n是数字1,2或3，m是数字1,2或3，其制备方法及其用途在生产有色塑料或聚合彩色颗粒时，以及作为印刷油墨，印刷染料，涂料组合物和木材污渍

4. 发明授权

US5302704A Azodyes containing a sulfoacetoacetic acid anilide coupling component 失效
标题翻译：含有磺乙酰乙酸苯胺偶联组分的偶氮染料
公开(公告)号：US5302704A
公开(公告)日：1994-04-12
申请号：US924140
申请日：1992-08-03
申请人： Jean-Marie Adam , Thomas Eichenberger
发明人： Jean-Marie Adam , Thomas Eichenberger
IPC分类号： C09B26/02 , C07C309/17 , C09B29/01 , C09B29/33 , C09B31/11 , C09B56/18 , D06P3/24 , D06P3/32 , D06P3/60 , C09B29/033 , C07C309/14 , D06P1/06
CPC分类号： D06P3/241 , C07C309/17 , C09B29/0011 , C09B29/332 , C09B31/115
摘要： Dyes of formula ##STR1## wherein D is the radical of a diazo component of the benzene or naphthalene series or of the heterocyclic series, R.sub.1 is hydrogen or C.sub.1 -C.sub.4 alkyl and R.sub.2 is phenyl or substituted phenyl, give dyeings of good fastness properties on nitrogen-containing or hydroxyl group containing fibre materials.
摘要翻译：式（1）的染料其中D是苯或萘系的重氮组分或杂环系列的基团，R 1是氢或C 1 -C 4烷基，R 2是苯基或取代的苯基，得到具有良好牢度的染色含氮或含羟基纤维材料的性质。

5. 发明申请

US20110294385A1 ORGANIC BLACK PIGMENTS AND THEIR PREPARATION 有权
标题翻译：有机黑色素及其制备
公开(公告)号：US20110294385A1
公开(公告)日：2011-12-01
申请号：US13144940
申请日：2009-12-28
申请人： Thomas Eichenberger , Thomas Ruch , Ralf Bauer , Christoph Krebs , Ursula Luterbacher , Marc Maurer
发明人： Thomas Eichenberger , Thomas Ruch , Ralf Bauer , Christoph Krebs , Ursula Luterbacher , Marc Maurer
IPC分类号： D03D15/00 , C09D11/02 , B32B5/16 , C07D493/04 , C08K5/3417 , B82Y30/00
CPC分类号： C09B57/00 , C07D405/04 , C07D493/04 , C08K5/0041 , C09B67/0034 , Y10T428/2982 , Y10T442/30
摘要： A process for preparing a black colorant, preferably a black pigment, characterized in that a compound of the Formula (I) is reacted with a compound of the Formula (II) in a molar ratio of 1:2, in the presence of a catalyst which in water at 25° C. has a pK≦4.5. For the definition of R1 to R7, refer to the description; preferably all are H. Likewise claimed are new crystal polymorphs obtainable by this process, and preferably single-phase mixed crystals. Also claimed are synergistic compositions. These compositions exhibit increased light stability in plastics stabilized with basic light stabilizers when they are pigmented with colorants of the invention rather than with known black pigments such as carbon black. The specification also relates, furthermore, to the use of the black colorants of the invention for coloring paints, printing inks and plastics in the mass, and to mulch film, instrument panels, woven fabrics, garden furniture items or elements for the construction industry that are pigmented with said colorants.
摘要翻译：一种制备黑色着色剂，优选黑色颜料的方法，其特征在于使式（I）化合物与摩尔比为1:2的式（II）化合物在催化剂存在下反应其在25℃的水中具有pK＆nlE; 4.5。关于R1〜R7的定义，请参考说明书; 优选全部为H.同样要求保护的是通过该方法可获得的新晶体多晶型物，优选单相混合晶体。还要求的是协同组合物。当用本发明的着色剂着色时，这些组合物在用碱性光稳定剂稳定的塑料中显示增强的光稳定性，而不是已知的黑色颜料如炭黑。此外，本说明书还涉及本发明的黑色着色剂用于在油漆中着色油漆，印刷油墨和塑料的用途，以及用于建筑行业的膜，仪表板，机织织物，花园家具或元件的覆盖用着色剂着色。

6. 发明申请

US20110186821A1 AZAPYRENES FOR ELECTRONIC APPLICATIONS 有权
标题翻译：用于电子应用的AZAPYRENES
公开(公告)号：US20110186821A1
公开(公告)日：2011-08-04
申请号：US13003614
申请日：2009-06-23
申请人： Thomas Schäfer , Thomas Eichenberger , Kristina Bardon , Andrea Ricci , Natalia Chebotareva
发明人： Thomas Schäfer , Thomas Eichenberger , Kristina Bardon , Andrea Ricci , Natalia Chebotareva
IPC分类号： H01L51/50 , C07D239/70 , C07D471/06 , C07D487/16 , C07D403/10 , C07D401/04 , C09K11/06 , H01B1/12
CPC分类号： C09K11/025 , C07D239/70 , C07D471/06 , C09K11/06 , C09K2211/1007 , C09K2211/1044 , C09K2211/1059 , H01L51/0054 , H01L51/006 , H01L51/0072 , H01L51/0085 , H01L51/5016 , H01L51/5048 , H05B33/14 , Y02E10/549 , Y02P70/521
摘要： The present invention relates to electronic devices, especially electroluminescent devices, comprising azapyrenes of formula (I), or formula (III), wherein Y1, Y2, Y3, Y4, X1, X2 and X3 are independently each other N, or CR4, with the proviso that at least one of the groups X1, X2 and X3 is a group CR4, R1 is hydrogen, F, —SiR100R101R102, or an organic substituent, R4 is hydrogen, F, —SiR100R101R102, or an organic substituent, or any of the substituents R1, R1′ and R4, which are adjacent to each other, together form an aromatic, or heteroaromatic ring, or ring system, which can optionally be substituted, m is an integer of 1 to 6, and R100, R101 and R102 are independently of each other a C1-C8alkyl group, a C6-C24aryl group, or a C7-C12aralkyl group, which may optionally be substituted, and Q is a linking group; with the proviso that in the compound of formula (III) at least one of the substituents R1, or R4 is a group Q; especially as host for phosphorescent emitters, electron transporting materials, or emitter materials. The hosts may function with phosphorescent materials to provide improved efficiency, stability, manufacturability, or spectral characteristics of electroluminescent devices.
摘要翻译：本发明涉及包含式（I）或式（III）的吡喃酮的电子器件，特别是电致发光器件，其中Y1，Y2，Y3，Y4，X1，X2和X3彼此独立地为N或CR4，与条件是基团X1，X2和X3中的至少一个是基团CR4，R1是氢，F，-SiR100R101R102或有机取代基，R4是氢，F，-SiR100R101R102或有机取代基，或任何彼此相邻的取代基R 1，R 1'和R 4一起形成可任选被取代的芳族或杂芳族环或环系，m是1至6的整数，且R 100，R 101和R 102 彼此独立地为C1-C8烷基，C6-C24芳基或可任意取代的C7-C12芳烷基，Q为连接基团; 条件是在式（III）的化合物中，至少一个取代基R 1或R 4为基团Q; 特别是作为磷光发射体，电子传输材料或发射体材料的主体。主机可以与磷光材料一起工作，以提供电致发光器件的改进的效率，稳定性，可制造性或光谱特性。

7. 发明授权

US07731791B2 Use of pyrimido[5,4-g]pteridines as shading component in color filter colorant compositions 失效
标题翻译：在滤色剂着色剂组合物中使用嘧啶并[5,4-g]蝶啶作为遮光组分
公开(公告)号：US07731791B2
公开(公告)日：2010-06-08
申请号：US11663823
申请日：2005-09-21
申请人： Takashi Deno , Thomas Eichenberger , Joachim Voigt
发明人： Takashi Deno , Thomas Eichenberger , Joachim Voigt
IPC分类号： C09B67/22 , C09B67/20 , G02F1/1335 , G02B5/22 , C08K5/00
CPC分类号： C08K5/0041 , C09B67/0033 , G02B5/223
摘要： The present invention relates to the field of color filters and LCDs. More specifically, the invention relates to a colorant composition for making color filters comprising pyrimido[5,4-g]pteridine derivatives of formula (I) wherein A1, A2, A3, and A4 are each independently of the others —NR1R2, wherein R1 and R2 are each independently of the others hydrogen, CrC8alkyl, —CO—C1-C8alkyl, —CO—Ce—Cuaryl, —COO—C1-C8alkyl, —COO—Ce—CMaryl, —CONH-d-Cβalkyl or —CONH—Ce-CMaryl, Or A1, A2, A3, and A4 are each independently of the others —OH, —SH, hydrogen, CrC8alkyl, CrC8alkoxy, or C6-C14aryl or —O—C6-C14aryl each unsubstituted or mono- or poly-substituted by halogen, nitro, cyano, —OR10, —SR10, —NR10R11, —CONR10R11, —COOR10, —SO2R10, —SO2NR10R11, —SO3R10, —NR11COR10 or by —NR11COOR10, wherein R10 and R11 are each independently of the others hydrogen, CrC8alkyl, C5-C12cycloalkyl or C2-C8-alkenyl; and to their use for color filter production and to color filters comprising said pyrimido[5,4-g]pteridine derivatives of formula (I).
摘要翻译：本发明涉及滤色器和LCD的领域。更具体地，本发明涉及一种用于制备包含式（I）的嘧啶并[5,4-g]蝶啶衍生物的滤色剂的着色剂组合物，其中A1，A2，A3和A4各自独立地为-NR1R2，其中R1 -CO-C 1 -C 8烷基，-CO-C 1 -C 6芳基，-COO-C 1 -C 8烷基，-COO-C 1 -C 10芳基，-CONH-d-C 1 -C 8烷基或 - CONH-C 1 -C 10芳基或者A 1，A 2，A 3和A 4各自独立地为-OH，-SH，氢，C 1 -C 8烷基，C 1 -C 8烷氧基或C 6 -C 14芳基或者-O-C 6 -C 14芳基，被卤素，硝基，氰基，-OR10，-SR10，-NR10R11，-CONR10R11，-COOR10，-SO2R10，-SO2NR10R11，-SO3R10，-NR11COR10或-NR11COOR10多取代，其中R10和R11各自独立地为其它氢，C 1 -C 8烷基，C 5 -C 12环烷基或C 2 -C 8 - 烯基; 以及它们用于滤色器生产的用途以及包含式（I）的所述嘧啶并[5,4-g]蝶啶衍生物的滤色片。

8. 发明申请

US20060053571A1 Azo dyes soluble in organic solvents 失效
标题翻译：偶氮染料可溶于有机溶剂
公开(公告)号：US20060053571A1
公开(公告)日：2006-03-16
申请号：US10537063
申请日：2003-11-26
申请人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hugin
发明人： Leonhard Feiler , Thomas Raimann , Thomas Eichenberger , Max Hugin
IPC分类号： D06P3/52
CPC分类号： C09B69/045 , C09B29/3617 , C09B31/14 , Y10S8/922
摘要： The present invention relates to azo dyes of formula (1) which are soluble in organic solvents, wherein R1 is —CN, —COOR5, —CONR6R7 or a heterocyclic ring, R2 is unsubstituted or substituted alkyl, unsubstituted or substituted aryl, —CF3, —COOR5, —CONR6R7 or —COR5, R3 is hydrogen, —SO3M, alkyl, alkoxy, alkylcarbonyl, —NO2 or halogen, R4 is substituted aryl, substituted heteroaryl or an aryl-N═N-aryl radical, wherein one or both of the aryl radicals in aryl-N═N-aryl is/are unsubstituted or substituted, or a radical heteroaryl-N═N-heteroaryl, wherein one or both of the heteroaryl radicals in heteroaryl-N═N-heteroaryl is/are unsubstituted or substituted, R5 is hydrogen, alkyl or unsubstituted or substituted aryl, R6 is hydrogen, alkyl or unsubstituted or substituted aryl, R7 is hydrogen, alkyl or unsubstituted or substituted aryl, M+ is a cation, n is a number 1, 2 or 3 and m is a number 1, 2 or 3, to a process for the preparation thereof and to the use thereof in the production of coloured plastics or polymeric colour particles, and as printing inks, printing dyes, coating compositions and wood stains.
摘要翻译：

9. 发明授权

US5785720A Process for coloring high molecular weight material with polycyclic compounds 失效
标题翻译：用多环化合物着色高分子量材料的方法
公开(公告)号：US5785720A
公开(公告)日：1998-07-28
申请号：US709050
申请日：1996-09-06
申请人： Thomas Eichenberger , Thomas Ruch
发明人： Thomas Eichenberger , Thomas Ruch
IPC分类号： C07D487/14 , C08K5/3442 , C08K5/3465 , C08L101/00 , C09B57/00 , C07D241/00 , C08K5/3462
CPC分类号： C07D487/14 , C09B57/00
摘要： The present invention relates to a process for bulk coloration of high molecular weight organic material, which comprises the use of a compound of the formula (I) ##STR1## in which Q is O or S, and X is C(R.sub.3) or N, R.sub.1, R.sub.2 and R.sub.3 independently of one another are hydrogen, halogen chosen from the group consisting of chlorine, bromine and fluorine, C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 alkoxy, hydroxyl, cyano, nitro, amino, morpholino, ##STR2## in which A.sub.1 and A.sub.2 independently of one another are unsubstituted or substituted C.sub.6 -C.sub.12 aryl or C.sub.3 -C.sub.12 heteroaryl, which contains, in the ring system, 1 to 3 hetero atoms chosen from the group consisting of N, O and S, and E.sub.1 is ##STR3## or R.sub.1 and R.sub.2 together, or R.sub.1 and R.sub.3 together, are a radical A.sub.3, which A.sub.3 is unsubstituted or substituted C.sub.4 -C.sub.8 alkenylene or C.sub.8 -C.sub.12 arylene. Individual novel compounds of the formula (I) are claimed themselves.
摘要翻译：本发明涉及高分子量有机材料的批量着色方法，其包括使用其中Q为O或S的式（I）化合物（I），X为C（R 3））或N，R 1，R 2和R 3彼此独立地是氢，选自氯，溴和氟的卤素，C 1 -C 6烷基，C 1 -C 6烷氧基，羟基，氰基，硝基，氨基，吗啉代，其中A1和A2彼此独立地是未取代的或取代的C6-C12芳基或C3-C12杂芳基，其在环系中含有1至3个选自N，O和S的杂原子，以及 E1是R 1和R 2，或者R 1和R 3一起是基团A 3，其中A 3是未取代的或取代的C 4 -C 8亚烯基或C 8 -C 12亚芳基。本发明还提出了单独的式（I）化合物。

10. 发明授权

US08697792B2 Migration-free coloured copolycondensates for colouring polymers 有权
标题翻译：用于着色聚合物的无迁移的着色共缩聚物
公开(公告)号：US08697792B2
公开(公告)日：2014-04-15
申请号：US13496530
申请日：2010-09-15
申请人： Thomas Ruch , Thomas Eichenberger , Peter Sutter , Christoph Krebs , Ursula Luterbacher
发明人： Thomas Ruch , Thomas Eichenberger , Peter Sutter , Christoph Krebs , Ursula Luterbacher
IPC分类号： D06G5/00 , C08K5/03 , C08K5/092 , C08G73/10 , C08G63/682 , C08G63/685 , C08G63/688
CPC分类号： C09B57/08 , C09B69/101 , C09B69/102 , C09B69/103 , C09B69/109 , D06P1/0012 , D06P1/0052 , D06P3/006
摘要： The invention relates to colored and/or fluorescent copolycondensates which are obtained by reaction of colorants substituted by at least two reactive groups which do not interfere with one another, with selected cyclic dicarboxylic acids (especially 1,4-cyclohexanedicarboxylic acid), aliphatic diols (especially ethylene glycol), cyclic diamines (especially isophoronediamine) and/or amino acids in particular amounts.
摘要翻译：本发明涉及有色和/或荧光共聚缩聚物，其是通过被不被彼此干扰的至少两个反应性基团取代的着色剂与选择的环状二羧酸（特别是1,4-环己烷二羧酸），脂族二醇（特别是乙二醇），环状二胺（特别是异佛尔酮二胺）和/或氨基酸。

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