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1. 发明申请

WO2008039312A3 BOOTSTRAP SYNTHESIS OF BORANES 审中-公开
标题翻译： BORTSTRAP合成硼
公开(公告)号：WO2008039312A3
公开(公告)日：2008-05-08
申请号：PCT/US2007020028
申请日：2007-09-13
申请人： LOS ALAMOS NAT SECURITY LLC , THORN DAVID L , TUMAS WILLIAM
发明人： THORN DAVID L , TUMAS WILLIAM
IPC分类号： C01B35/14
CPC分类号： C07F5/006 , C01B3/0015 , C01B6/13 , Y02E60/328
摘要： Metal hydride materials react with BZ 3 compounds in the presence of ligand to form BH 3 -L compounds. A compound of the formula HBZ 2 is prepared from a compound of the formula BZ 3 by reacting a first amount of a compound of the formula HBZ 2 with a metal hydride material "MH" and a compound "L" to form a material of the formula BH 3 -L, and then reacting the BH 3 -L thus formed with a compound of the formula BZ 3 to form HBZ 2 in a second amount greater than the first amount of HBZ 2 . Z is selected from alkoxy, aryloxy, amido, arylamido, doubly substituted alkoxy, doubly substituted aryloxy, doubly substituted amido, doubly substituted arylamido, alkoxy-amido, and aryloxy-arylamido. When Z is bidentate, then HBZ 2 has a ring structure. "L" is selected from ethers, aromatic ethers, amines, aromatic amines, heterocyclic nitrogen compounds, sulfides, aromatic sulfides, and heterocyclic sulfur compounds. "L" becomes a ligand in the BH 3 -L material.
摘要翻译：金属氢化物材料在配体存在下与BZ 3化合物反应形成BH 3 SUB化合物。式HBZ SUB 2的化合物由式BZ SUB 3的化合物通过使第一量的式HBZ SUB 2的化合物与金属氢化物材料“MH”和化合物“L”反应以形成式BH _{3 -L的材料，然后如此反应BH <3> -L> 以比第一量的HBZ 2 / HB更大的第二量形成式BZ 3的化合物以形成HBZ 2。 Z选自烷氧基，芳氧基，酰氨基，芳基酰胺基，双取代的烷氧基，双取代的芳氧基，双取代的酰胺基，双取代的芳基酰胺基，烷氧基 - 酰胺基和芳氧基 - 芳基酰胺基。当Z是双齿时，则HBZ _{2 具有环状结构。 “L”选自醚，芳族醚，胺，芳族胺，杂环氮化合物，硫化物，芳族硫化物和杂环硫化合物。 “L”成为BH <3> SUB-L材料中的配体。}}

2. 发明申请

WO2007092602A3 COMPOSITION AND METHOD FOR STORING AND RELEASING HYDROGEN 审中-公开
标题翻译：用于储存和释放氢的组合物和方法
公开(公告)号：WO2007092602A3
公开(公告)日：2008-02-21
申请号：PCT/US2007003513
申请日：2007-02-08
申请人： LOS ALAMOS NAT SECURITY LLC , THORN DAVID L , TUMAS WILLIAM , OTT KEVIN C , BURRELL ANTHONY K
发明人： THORN DAVID L , TUMAS WILLIAM , OTT KEVIN C , BURRELL ANTHONY K
IPC分类号： B01J31/00
CPC分类号： C01B3/323 , B01J23/06 , B01J23/40 , B01J23/70 , B01J23/80 , C01B3/065 , C01B2203/0233 , C01B2203/0838 , C01B2203/0872 , C01B2203/1047 , C01B2203/1052 , C01B2203/1058 , C01B2203/1064 , C01B2203/107 , C01B2203/1076 , C01B2203/1223 , Y02E60/324 , Y02E60/362 , Y02E60/364 , Y02P20/52
摘要： A chemical system for storing and releasing hydrogen utilizes an endothermic reaction that releases hydrogen coupled to an exothermic reaction to drive the process thermodynamically, or an exothermic reaction that releases hydrogen coupled to an endothermic reaction.
摘要翻译：用于储存和释放氢的化学体系利用释放与放热反应耦合的氢以吸引热力学的热吸收反应，或放出与吸热反应耦合的氢的放热反应。

3. 发明申请

WO2008143780A1 METAL AMINOBORANES 审中-公开
标题翻译：金属氨基酸
公开(公告)号：WO2008143780A1
公开(公告)日：2008-11-27
申请号：PCT/US2008/005834
申请日：2008-05-07
申请人： LOS ALAMOS NATIONAL SECURITY, LLC , BURRELL, Anthony, K. , DAVIS, Benjamin, J. , THORN, David, L. , GORDON, John, C. , BAKER, R., Thomas , SEMELSBERGER, Troy, Allen , TUMAS, William , DIYABALANAGE, Himashinie, Vichalya Kaviraj , SHRESTHA, Roshan, P.
发明人： BURRELL, Anthony, K. , DAVIS, Benjamin, J. , THORN, David, L. , GORDON, John, C. , BAKER, R., Thomas , SEMELSBERGER, Troy, Allen , TUMAS, William , DIYABALANAGE, Himashinie, Vichalya Kaviraj , SHRESTHA, Roshan, P.
IPC分类号： C01B6/00 , C01B3/02 , H01M8/00
CPC分类号： H01M8/0606 , C01B3/0026 , C01B3/0031 , C01B6/19 , Y02E60/327
摘要： Metal aminoboranes of the formula M(NH 2 BH 3 ) n have been synthesized. Metal aminoboranes are hydrogen storage materials. Metal aminoboranes are also precursors for synthesizing other metal aminoboranes. Metal aminoboranes can be dehydrogenated to form hydrogen and a reaction product. The reaction product can react with hydrogen to form a hydrogen storage material. Metal aminoboranes can be included in a kit.
摘要翻译：已经合成了式M（NH 2 BH 3）n的金属氨基硼烷。金属氨基硼烷是储氢材料。金属氨基硼烷也是合成其它金属氨基硼烷的前体。金属氨基硼烷可以脱氢形成氢气和反应产物。反应产物可与氢反应形成储氢材料。金属氨基硼烷可以包含在试剂盒中。

4. 发明申请

WO2009067146A1 COATING FOR LEAK DETECTION AND METHOD 审中-公开
标题翻译：用于泄漏检测和方法的涂层
公开(公告)号：WO2009067146A1
公开(公告)日：2009-05-28
申请号：PCT/US2008/012546
申请日：2008-11-07
申请人： LOS ALAMOS NATIONAL SECURITY, LLC , THORN, David, L. , JONIETZ, Karl, K. , BONCELLA, James, M.
发明人： THORN, David, L. , JONIETZ, Karl, K. , BONCELLA, James, M.
IPC分类号： G01N31/22
CPC分类号： C08F136/22 , C08F136/20 , G01M3/12 , G01N31/22 , Y10T442/689
摘要： A coating is used to detect a fluid leak.
摘要翻译：使用涂层来检测流体泄漏。

5. 发明申请

WO2008039312A2 BOOTSTRAP SYNTHESIS OF BORANES 审中-公开
标题翻译： BOOTSTRAP合成硼烷
公开(公告)号：WO2008039312A2
公开(公告)日：2008-04-03
申请号：PCT/US2007/020028
申请日：2007-09-13
申请人： LOS ALAMOS NATIONAL SECURITY, LLC , THORN, David, L. , TUMAS, William
发明人： THORN, David, L. , TUMAS, William
IPC分类号： C07F5/04
CPC分类号： C07F5/006 , C01B3/0015 , C01B6/13 , Y02E60/328
摘要： Metal hydride materials react with BZ 3 compounds in the presence of ligand to form BH 3 -L compounds. A compound of the formula HBZ 2 is prepared from a compound of the formula BZ 3 by reacting a first amount of a compound of the formula HBZ 2 with a metal hydride material "MH" and a compound "L" to form a material of the formula BH 3 -L, and then reacting the BH 3 -L thus formed with a compound of the formula BZ 3 to form HBZ 2 in a second amount greater than the first amount of HBZ 2 . Z is selected from alkoxy, aryloxy, amido, arylamido, doubly substituted alkoxy, doubly substituted aryloxy, doubly substituted amido, doubly substituted arylamido, alkoxy-amido, and aryloxy-arylamido. When Z is bidentate, then HBZ 2 has a ring structure. "L" is selected from ethers, aromatic ethers, amines, aromatic amines, heterocyclic nitrogen compounds, sulfides, aromatic sulfides, and heterocyclic sulfur compounds. "L" becomes a ligand in the BH 3 -L material.
摘要翻译：在配体存在下，金属氢化物与BZ 3 N 3化合物反应形成BH 3 -L-L化合物。由式BZ 3 3的化合物通过使第一量的式为HBZ 2的化合物/ SUB 与金属氢化物材料“MH”和化合物“L”形成式BH 3 -L的材料，然后使BH 3 -L 3 -L 由式BZ 3 3的化合物形成，以形成大于第一量的HBZ 2 N 2的第二量的HBZ 2 N 2。 Z选自烷氧基，芳氧基，酰胺基，芳基酰氨基，双取代的烷氧基，双取代的芳氧基，双取代的酰氨基，双取代的芳基酰氨基，烷氧基 - 酰氨基和芳氧基 - 芳基酰氨基。当Z为双齿时，则HBZ 2具有环结构。 “L”选自醚，芳香醚，胺，芳胺，杂环氮化合物，硫化物，芳族硫化物和杂环硫化合物。 “L”成为BH 3 -L材料中的配体。

6. 发明申请

WO2007092601A3 ENERGY EFFICIENT SYNTHESIS OF BORANES 审中-公开
标题翻译：能量有效地合成硼
公开(公告)号：WO2007092601A3
公开(公告)日：2007-11-22
申请号：PCT/US2007003511
申请日：2007-02-08
申请人： LOS ALAMOS NAT SECURITY LLC , THORN DAVID L , TUMAS WILLIAM , SCHWARZ DANIEL E , BURRELL ANTHONY K
发明人： THORN DAVID L , TUMAS WILLIAM , SCHWARZ DANIEL E , BURRELL ANTHONY K
IPC分类号： C08F4/44 , C08F4/00 , C08F4/14
CPC分类号： C01B6/15 , C01B6/19 , C01B35/061
摘要： The reaction of halo-boron compounds (B-X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B-H compounds, compounds having one or more B-H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si-H) react with B-X compounds to form B-H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface- bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn-H bond) to form boranes and halostannanes (tin compounds having a Sn-X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCI 3 , the B-H compound is B 2 H 6 , and where the reducing potential is provided electrochemically or by the thermolysis of formate.
摘要翻译：卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。表面结合的卤代硅烷通过电化学转化回表面结合的硅烷。卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。当卤代硼化合物是BCI 3 N时，BH化合物是B 2 H 6 N，并且其中还原电位是电化学或由甲酸盐的热解。

7. 发明申请

WO2007092602A2 COMPOSITION AND METHOD FOR STORING AND RELEASING HYDROGEN 审中-公开
标题翻译：用于储存和释放氢的组合物和方法
公开(公告)号：WO2007092602A2
公开(公告)日：2007-08-16
申请号：PCT/US2007/003513
申请日：2007-02-08
申请人： LOS ALAMOS NATIONAL SECURITY, LLC , THORN, David, L. , TUMAS, William , OTT, Kevin, C. , BURRELL, Anthony, K.
发明人： THORN, David, L. , TUMAS, William , OTT, Kevin, C. , BURRELL, Anthony, K.
CPC分类号： C01B3/323 , B01J23/06 , B01J23/40 , B01J23/70 , B01J23/80 , C01B3/065 , C01B2203/0233 , C01B2203/0838 , C01B2203/0872 , C01B2203/1047 , C01B2203/1052 , C01B2203/1058 , C01B2203/1064 , C01B2203/107 , C01B2203/1076 , C01B2203/1223 , Y02E60/324 , Y02E60/362 , Y02E60/364 , Y02P20/52
摘要： A chemical system for storing and releasing hydrogen utilizes an endothermic reaction that releases hydrogen coupled to an exothermic reaction to drive the process thermodynamically, or an exothermic reaction that releases hydrogen coupled to an endothermic reaction.
摘要翻译：用于储存和释放氢的化学体系利用释放与放热反应耦合的氢以吸引热力学的热吸收反应，或放出与吸热反应耦合的氢的放热反应。

8. 发明申请

WO2007092601A2 ENERGY EFFICIENT SYNTHESIS OF BORANES 审中-公开
标题翻译：硼能的高能效合成
公开(公告)号：WO2007092601A2
公开(公告)日：2007-08-16
申请号：PCT/US2007/003511
申请日：2007-02-08
申请人： LOS ALAMOS NATIONAL SECURITY, LLC , THORN, David, L. , TUMAS, William , SCHWARZ, Daniel E. , BURRELL, Anthony, K.
发明人： THORN, David, L. , TUMAS, William , SCHWARZ, Daniel E. , BURRELL, Anthony, K.
CPC分类号： C01B6/15 , C01B6/19 , C01B35/061
摘要： The reaction of halo-boron compounds (B-X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B-H compounds, compounds having one or more B-H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si-H) react with B-X compounds to form B-H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface- bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn-H bond) to form boranes and halostannanes (tin compounds having a Sn-X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCI 3 , the B-H compound is B 2 H 6 , and where the reducing potential is provided electrochemically or by the thermolysis of formate.
摘要翻译：卤硼化合物（B-X化合物，具有一个或多个硼卤键的化合物）与硅烷的反应提供了硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。无机氢化物如表面键合的硅烷氢化物（Si-H）与B-X化合物反应形成B-H化合物和表面结合的卤代硅烷。表面键合的卤代硅烷电化学转化为表面结合的硅烷。卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代锡烷（具有Sn-X键的锡化合物）。卤代锡烷通过电化学方式或通过Sn-甲酸盐化合物的热分解转化为锡烷。当卤硼化合物为BCl 3 3时，BH化合物为B 2 H 6，并且其中还原电位通过电化学或通过甲酸的热分解。

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