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1. 发明授权

US08765902B2 Method for the production of polyamides in extruders 有权
标题翻译：在挤出机中生产聚酰胺的方法
公开(公告)号：US08765902B2
公开(公告)日：2014-07-01
申请号：US12665585
申请日：2008-06-11
申请人： Philippe Desbois , Michael Kopietz , Ralf Neuhaus , Hagen Stawitzki , Hans-Joachim Weis , Jochen Engelmann
发明人： Philippe Desbois , Michael Kopietz , Ralf Neuhaus , Hagen Stawitzki , Hans-Joachim Weis , Jochen Engelmann
IPC分类号： C08G69/28
CPC分类号： C08G69/265 , B29C47/822 , C08G69/30
摘要： In a process for preparing a polyamide based on dicarboxylic acids and diamines in an extruder, a solid mixture comprising a monomer mixture composed of 50 mol % of dicarboxylic acid mixture composed of from 60 to 88 % by weight of terephthalic acid and from 12 to 40% by weight of isophthalic acid, in which up to 20% by weight of the dicarboxylic acid mixture may also be replaced by other dicarboxylic acids, and 50 mol % of hexamethylenediamine which may be up to 20% by weight replaced by other C2-30-diamines, in a corotatory twin-screw extruder for a residence time of from 10 seconds to 30 minutes, is heated to a temperature in the range from 150 to 400° C. while removing steam and if appropriate diamines through venting orifices.
摘要翻译：在挤出机中制备基于二羧酸和二胺的聚酰胺的方法中，包含由50摩尔％的由对苯二甲酸的重量比为60-88％的二羧酸混合物和12-40的二羧酸混合物组成的单体混合物的固体混合物重量％的间苯二甲酸，其中高达20重量％的二羧酸混合物也可以被其它二羧酸代替，并且50摩尔％的六亚甲基二胺可以被其他C2-30重量代替 - 二胺在旋转双螺杆挤出机中停留时间为10秒至30分钟，加热至150-400℃的温度，同时除去蒸汽，如果合适的话，将其加热至通过排气孔。

2. 发明申请

US20120157594A1 COPOLYAMIDES 有权
标题翻译：共聚酰胺
公开(公告)号：US20120157594A1
公开(公告)日：2012-06-21
申请号：US13378980
申请日：2010-06-15
申请人： Christian Schmidt , Faissal-Ali El-Toufaili , Philippe Desbois , Racquel Fernandez Rodiles
发明人： Christian Schmidt , Faissal-Ali El-Toufaili , Philippe Desbois , Racquel Fernandez Rodiles
IPC分类号： C08K5/05
CPC分类号： C08G69/265 , C08G69/14 , C08G69/36 , C08L77/02 , C08L77/06 , C09D177/02 , C09D177/06
摘要： What are described are a solution comprising a terpolymer formed from the monomers of components A, B and C, the total amount of which adds up to 100% by weight,a) 5 to 60% by weight of lactams as component A,b) 5 to 60% by weight of equimolar amounts of adipic acid and one or more aliphatic diamines as component B,c) 10 to 70% by weight of equimolar amounts of adipic acid and 4,4′-diaminodicyclohexylmethane (dicycan) as component C,in an aromatics-free solvent system comprising50 to 100% by weight of C1-4-alkanol,0 to 50% by weight of water andnot more than 10% by weight of further aromatics-free solvents,where the total amount of the solvent system adds up to 100% by weight, and a terpolymer formed from the monomers of components A, B and C, the total amount of which adds up to 100% by weight,a) 15 to 40% by weight of lactams as component A,b) 20 to 45% by weight of equimolar amounts of adipic acid and one or more aliphatic diamines as component B,c) 25 to 60% by weight of equimolar amounts of adipic acid and 4,4′-diaminodicyclohexylmethane (dicycan) as component C,excluding terpolymers formed from 30 to 40% by weight of component A, 30 to 40% by weight of component B and 30 to 40% by weight of component C.
摘要翻译：描述的是包含由组分A，B和C的单体形成的三元共聚物的溶液，其总量加至100重量％，a）5至60重量％的作为组分A的内酰胺，b） 5至60重量％的等摩尔量的己二酸和一种或多种脂族二胺作为组分B，c）10至70重量％的等摩尔量的己二酸和作为组分C的4,4'-二氨基二环己基甲烷（二环己烷）在不含芳族化合物的溶剂体系中，其包含50至100重量％的C 1-4链烷醇，0至50重量％的水和不超过10重量％的其它不含芳族化合物的溶剂，其中溶剂系统加入到100重量％，和由组分A，B和C的单体形成的三元共聚物，其总量加至100重量％，a）15至40重量％的作为组分的内酰胺 A，b）20〜45重量％的等摩尔量的己二酸和一种或多种作为组分B的脂族二胺，c）25至60重量％的等摩尔量的己二酸和4,4'-二氨基二环己基甲烷（二环己烷）作为组分C，不包括由30至40重量％的组分A形成的三元共聚物，30至40重量％的组分B和30至40重量％的组分C.

3. 发明申请

US20120142887A1 CROSSLINKED POLYAMIDES 审中-公开
标题翻译：交联聚氨酯
公开(公告)号：US20120142887A1
公开(公告)日：2012-06-07
申请号：US13308707
申请日：2011-12-01
申请人： Philippe Desbois , Dietrich Scherzer , Andreas Wollny , Andreas Radtke
发明人： Philippe Desbois , Dietrich Scherzer , Andreas Wollny , Andreas Radtke
IPC分类号： C08G69/16
CPC分类号： C08G69/18
摘要： A process for crosslinking polyamides by reacting a compound of the general formula R1R2C═CR3—X in which R1, R2 and R3 are each independently hydrogen or an organic radical with a lactam A at a temperature of (−30) to 150° C., and then reacting with a lactam B, a catalyst and an activator at a temperature of 40 to 240° C.
摘要翻译：通过使通式为R 1 R 2 C = CR 3 -X的化合物（其中R 1，R 2和R 3各自独立地为氢或有机基团）与内酰胺A在（-30）至150℃的温度下反应来交联聚酰胺的方法。然后在40〜240℃的温度下与内酰胺B，催化剂和活化剂反应。

4. 发明申请

US20120022187A1 POLYAMIDE MOLDINGS COMPRISING MICROENCAPSULATED LATENT-HEAT-ACCUMULATOR MATERIAL 有权
标题翻译：包含微晶硅酸盐蓄热材料的聚酰胺模具
公开(公告)号：US20120022187A1
公开(公告)日：2012-01-26
申请号：US13184863
申请日：2011-07-18
申请人： Philippe DESBOIS , Tina Schröder-Grimonpont , Stephan Altmann , Marco Schmidt
发明人： Philippe DESBOIS , Tina Schröder-Grimonpont , Stephan Altmann , Marco Schmidt
IPC分类号： C08L1/00
CPC分类号： C08L1/00 , C08G69/18 , C08G69/24 , C08K5/01 , C08L33/06 , C08L77/02
摘要： The present invention relates to polyamide moldings obtainable via anionic polymerization of a lactam comprising microcapsules with a capsule core made of latent-heat-accumulator material and a polymer as capsule wall, to a process for producing the same, and also to the use of the same in motor-vehicle construction, as battery housing, as housing for small electronic devices, and for heat-retention systems for foods.
摘要翻译：本发明涉及通过由包含由潜热蓄热材料制成的胶囊芯的微胶囊和具有胶囊壁的聚合物的内酰胺的阴离子聚合得到的聚酰胺成型品，其制造方法，以及使用机动车辆结构相同，电池外壳，小型电子设备的外壳以及食品的保温系统。

5. 发明申请

US20120004353A1 HEAT AGING RESISTANT POLYAMIDES 有权
标题翻译：耐热耐久性聚氨酯
公开(公告)号：US20120004353A1
公开(公告)日：2012-01-05
申请号：US13139768
申请日：2009-12-10
申请人： Manoranjan Prusty , Philippe Desbois , Matthias Scheibitz , Martin Baumert
发明人： Manoranjan Prusty , Philippe Desbois , Matthias Scheibitz , Martin Baumert
IPC分类号： C08L77/06 , C08K13/02 , C08L79/02 , C08K3/08
CPC分类号： C08L77/06 , C08K2003/0856 , C08L77/00 , C08L77/02 , C08L79/02 , C08L2205/02 , C08L2205/03 , C08L2666/20 , C08K3/08 , C08K7/14
摘要： Thermoplastic molding compositions comprising A) from 10 to 99.94% by weight of a polyamide, B) from 0.05 to 5% by weight of a polyethyleneimine homo- or copolymer, C) from 0.01 to 20% by weight of iron powder, and D) from 0 to 70% by weight of further additives, where the total of the percentages by weight of A) to D) is 100%.
摘要翻译：热塑性成型组合物，其包含A）10至99.94重量％的聚酰胺，B）0.05至5重量％的聚乙烯亚胺均聚物或共聚物，C）0.01至20重量％的铁粉，以及D） 0至70重量％的其它添加剂，其中A）至D）的重量百分比的总和为100％。

6. 发明授权

US07288612B2 Initiator composition and method for anionic polymerisation 失效
标题翻译：用于阴离子聚合的引发剂组合物和方法
公开(公告)号：US07288612B2
公开(公告)日：2007-10-30
申请号：US10512444
申请日：2003-04-15
申请人： Philippe Desbois , Christian Schade , Alain Deffieux , Stephane Menoret , Jürgen Demeter
发明人： Philippe Desbois , Christian Schade , Alain Deffieux , Stephane Menoret , Jürgen Demeter
IPC分类号： C08F4/48 , C08F12/08 , C08F36/02
CPC分类号： C08F297/04 , C07F5/062 , C08F4/54 , C08F36/04 , C08L53/02 , C08F4/52 , C08F4/48 , C08L2666/02
摘要： The invention relates to an initiator composition for anionic polymerization, comprising at least one alkali metal hydride selected from LiH, NaH, and KH, and at least one organylaluminum compound, and to a process for the anionic polymerization of styrene monomers or of diene monomers using the initiator composition.
摘要翻译：本发明涉及用于阴离子聚合的引发剂组合物，其包含至少一种选自LiH，NaH和KH的碱金属氢化物和至少一种有机铝化合物，以及使用苯乙烯单体或二烯单体进行阴离子聚合的方法，该方法使用引发剂组合物。

7. 发明申请

US20060160971A1 Method for anionic polymerisation of $g(a)-methylstyrene 失效
标题翻译： $ g（a） - 甲基苯乙烯的阴离子聚合方法
公开(公告)号：US20060160971A1
公开(公告)日：2006-07-20
申请号：US10545945
申请日：2004-01-28
申请人： Philippe Desbois , Michael Ishaque , Christian Schade , Alain Deffieux , Stephane Carlotti
发明人： Philippe Desbois , Michael Ishaque , Christian Schade , Alain Deffieux , Stephane Carlotti
IPC分类号： C08F4/46
CPC分类号： C08F4/56 , C08F4/463 , C08F4/52 , C08F112/12 , C08F212/08 , C08F297/04 , C08L9/06 , C08L25/10 , C08L53/02 , C08L2666/24
摘要： Process for preparing homopolymers of α-methylstyrene, or copolymers of α-methylstyrene and comonomers, by anionic polymerization in the presence of an initiator composition, which comprises using an initiator composition in which potassium hydride and at least one organylaluminum compound are present.
摘要翻译：在引发剂组合物的存在下通过阴离子聚合制备α-甲基苯乙烯的均聚物或α-甲基苯乙烯和共聚单体的共聚物的方法，其包括使用其中存在氢化钾和至少一种有机铝化合物的引发剂组合物。

8. 发明授权

US06951901B2 Method for continuous anionic polymerization of impact-resistant polystyrene 失效
标题翻译：耐冲击聚苯乙烯连续阴离子聚合方法
公开(公告)号：US06951901B2
公开(公告)日：2005-10-04
申请号：US10492620
申请日：2002-10-18
申请人： Hermann Gausepohl , Jürgen Demeter , Philippe Desbois , Christian Schade
发明人： Hermann Gausepohl , Jürgen Demeter , Philippe Desbois , Christian Schade
IPC分类号： C08F2/44 , C08F4/00 , C08F279/02 , C08F287/00 , C08F279/00
CPC分类号： C08F287/00 , C08F279/02
摘要： A process for preparing impact-resistant molding compositions by anionic polymerization of vinylaromatic monomers in the presence of a rubber, in a continuous-flow reactor cascade composed of at least two reactors, where the vinylaromatic monomers are fed in substreams to the reactors of the reactor cascade, and an anionic initiator and a rubber are fed at least to the first reactor, and where the reactor cascade is composed of back-mixing reactors.
摘要翻译：一种在由至少两个反应器组成的连续流动反应器级联中，在橡胶存在下通过阴离子聚合乙烯基芳族单体制备耐冲击成型组合物的方法，其中乙烯基芳族单体以子流加入反应器的反应器级联，并且阴离子引发剂和橡胶至少进料到第一反应器，并且其中反应器级联由反混合反应器组成。

9. 发明授权

US06350834B1 Method for retarded anionic polymerization 失效
标题翻译：延迟阴离子聚合法
公开(公告)号：US06350834B1
公开(公告)日：2002-02-26
申请号：US09622210
申请日：2000-08-14
申请人： Christian Schade , Wolfgang Fischer , Hermann Gausepohl , Konrad Knoll , Volker Warzelhan , Michel Fontanille , Alain Deffieux , Philippe Desbois
发明人： Christian Schade , Wolfgang Fischer , Hermann Gausepohl , Konrad Knoll , Volker Warzelhan , Michel Fontanille , Alain Deffieux , Philippe Desbois
IPC分类号： C08F452
CPC分类号： C08F12/04 , C08F236/10 , C08F4/46 , C08F4/54 , C08F4/12 , C08F4/52
摘要： In a process for the homopolymerization of vinylaromatic monomers or the copolymerization of vinylaromatic monomers and dienes in the presence of at least one alkali metal compound and at least one compound of an element of group 3a of the Periodic Table of the elements, the compounds contain, based on the sum of molar equivalents of alkali metal and elements of group 3a, in each case a) from 0.1 to 3.9 molar equivalents of oxygen, sulfur, nitrogen or phosphorus and b) from 0.1 to 3.9 molar equivalents of an organyl ligand.
摘要翻译：在至少一种碱金属化合物和元素周期表第3a族元素的至少一种化合物的存在下，在乙烯基芳族单体的均聚或乙烯基芳族单体和二烯的共聚合的方法中，基于碱金属和第3a族元素的摩尔当量的总和，在每种情况下）a 0.1至3.9摩尔当量的氧，硫，氮或磷和b）0.1至3.9摩尔当量的有机配体。

10. 发明授权

US10538624B2 Process for producing monomer compositions and use of these for producing a polyamide molding 有权
公开(公告)号：US10538624B2
公开(公告)日：2020-01-21
申请号：US13268228
申请日：2011-10-07
申请人： Dietrich Scherzer , Philippe Desbois , Volker Warzelhan , Andreas Wollny , Andreas Radtke , Axel Wilms , Martin Klatt
发明人： Dietrich Scherzer , Philippe Desbois , Volker Warzelhan , Andreas Wollny , Andreas Radtke , Axel Wilms , Martin Klatt
IPC分类号： C08G69/14 , C08G69/18 , C08G69/16 , C08G69/20
摘要： A process for producing an activated monomer composition comprising at least one lactam and/or lactone, one catalyst, and one activator permits storage of the resultant monomer composition, since this is stable with respect to polymerization. Said monomer composition is used inter alia in producing a polyamide molding via ring-opening, anionic polymerization.

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