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1. 发明公开

EP0900300A1 A METHOD FOR THE DELIGNIFICATION OF FIBROUS MATERIAL AND USE OF A CATALYST 失效
标题翻译：纤维材料的木质和使用催化剂的过程
公开(公告)号：EP0900300A1
公开(公告)日：1999-03-10
申请号：EP97923942.0
申请日：1997-05-20
申请人： Patt, Rudolf
发明人： PATT, Rudolf , MIELISCH, Hans-Jürgen , ODERMATT, Jürgen , WIEGHARDT, K. , WEYERMÜLLER, Thomas
IPC分类号： B01J31 , D21C9
CPC分类号： B01J31/182 , B01J31/2239 , B01J2531/0216 , B01J2531/0258 , B01J2531/72 , B01J2531/842 , D21C9/1036 , D21C9/163
摘要： The invention refers to a method to delignify fibrous material comprising an aqueous suspension of fibers which has a consistency between 5 % - 40 %, with a peroxy compound that is used in amounts between 0.5 % - 10 % based on bone dry fibrous material, and with a metal complex of the general formula (1): [LnMnmXp]zYq wherein Mn stands for manganese or iron, which can be present in oxidation state II, III, IV or V or in mixtures of these states; n and m are the integers 1-4; X is a coordinating ligand; p is an integer from 0 to 12; z is the charge of the complex and can be positive, neutral or negative; Y is a counter-ion or -molecule which depends on the charge of the complex; q is equal to z divided by the charge of Y; and L is a ligand and is represented by a macrocyclic organic molecule with general formula (2) wherein R?1, R2, R3 and R4¿ can be either zero, H, alkyl, aryl or otherwise optionally substituted; D and D' are either N, NR, PR O, or S, wherein R can be substituted by H or alkyl or aryl or otherwise optionally substituted; t and t' are whole integers from 2 to 3, s is an integer between 2 and 4, u is an integer from 1 to 20, and v is 0 or 1; this metal complex is used at an amount of 0.0001 % - 0.1 % based on bone dry fibrous material, wherein the fibers are delignified at an initial pH-level between 7.5 and 13.5, at a reaction temperature between 20 °C and 130 °C, and with a reaction time between 15 and 360 minutes. Further, the invention relates to the use of a metal complex.

2. 发明申请

WO2004104293A1 VERFAHREN ZUM DELIGNIFIZIEREN LIGNOCELLULOSISCHER ROHSTOFFE 审中-公开
标题翻译：方法脱木素木质纤维商品
公开(公告)号：WO2004104293A1
公开(公告)日：2004-12-02
申请号：PCT/EP2004/005411
申请日：2004-05-19
申请人： VOITH PAPER FIBER SYSTEMS GMBH & CO. KG , PATT, Rudolf , ROSE, Björn , KORDSACHIA, Othar , GEHR, Volker , SCHUBERT, Hans-Ludwig
发明人： PATT, Rudolf , ROSE, Björn , KORDSACHIA, Othar , GEHR, Volker , SCHUBERT, Hans-Ludwig
IPC分类号： D21C3/06
CPC分类号： D21C3/06
摘要： Die Erfindung betrifft ein Verfahren zum Delignifizieren lignocellulosischer Rohstoffe, durch Einsatz von Sulfiten in Gegenwart einer alkalischen Komponente, insbesondere Natriumhydroxid oder Natriumcarbonat oder einer Mischung davon, in wässriger Lösung unter Anwendung von erhöhter Temperatur und erhöhtem Druck, gekennzeichnet dadurch, dass zu Beginn eines Aufschlusses die wässrigen Sulfit-Lösung eingesetzt und die Temperatur bis auf die maximale Reaktionstemperatur gesteigert wird, wobei die alkalische Komponente erst nach Beginn des Aufschlusses zugesetzt wird.
摘要翻译：本发明涉及一种方法，用于与升高的温度和压力的应用，其特征在于，在膨胀时，开始时脱木质素的木质纤维素原料，通过在碱成分的存在下使用亚硫酸盐，特别是氢氧化钠或碳酸钠或它们的混合物，在水溶液用亚硫酸钠水溶液，并且将温度升高到最大反应温度升高，其中所述碱性组分仅在制浆过程开始后加入。

3. 发明申请

WO1997044520A1 A METHOD FOR THE DELIGNIFICATION OF FIBROUS MATERIAL AND USE OF A CATALYST 审中-公开
标题翻译：纤维材料的分级方法和催化剂的使用
公开(公告)号：WO1997044520A1
公开(公告)日：1997-11-27
申请号：PCT/EP1997002557
申请日：1997-05-20
申请人： PATT, Rudolf , MIELISCH, Hans-Jürgen , ODERMATT, Jürgen , WIEGHARDT, K. , WEYERMÜLLER, Thomas
IPC分类号： D21C09/10
CPC分类号： B01J31/182 , B01J31/2239 , B01J2531/0216 , B01J2531/0258 , B01J2531/72 , B01J2531/842 , D21C9/1036 , D21C9/163
摘要： The invention refers to a method to delignify fibrous material comprising an aqueous suspension of fibers which has a consistency between 5 % - 40 %, with a peroxy compound that is used in amounts between 0.5 % - 10 % based on bone dry fibrous material, and with a metal complex of the general formula (1): [LnMnmXp] Yq wherein Mn stands for manganese or iron, which can be present in oxidation state II, III, IV or V or in mixtures of these states; n and m are the integers 1-4; X is a coordinating ligand; p is an integer from 0 to 12; z is the charge of the complex and can be positive, neutral or negative; Y is a counter-ion or -molecule which depends on the charge of the complex; q is equal to z divided by the charge of Y; and L is a ligand and is represented by a macrocyclic organic molecule with general formula (2) wherein R , R , R and R can be either zero, H, alkyl, aryl or otherwise optionally substituted; D and D' are either N, NR, PR O, or S, wherein R can be substituted by H or alkyl or aryl or otherwise optionally substituted; t and t' are whole integers from 2 to 3, s is an integer between 2 and 4, u is an integer from 1 to 20, and v is 0 or 1; this metal complex is used at an amount of 0.0001 % - 0.1 % based on bone dry fibrous material, wherein the fibers are delignified at an initial pH-level between 7.5 and 13.5, at a reaction temperature between 20 DEG C and 130 DEG C, and with a reaction time between 15 and 360 minutes. Further, the invention relates to the use of a metal complex.
摘要翻译：本发明涉及一种脱木质纤维材料的方法，该纤维材料包含一种具有5％-40％的稠度的纤维的水性悬浮液与基于骨干纤维材料的用量为0.5％-10％的过氧化合物，以及与通式（1）的金属络合物：[LnMnmXp] Yq其中Mn代表锰或铁，其可以以氧化态II，III，IV或V存在或以这些状态的混合物存在; n和m是整数1-4; X是配位配体; p是0至12的整数; z是络合物的电荷，可以是正的，中性的或负的; Y是取决于复合物的电荷的抗衡离子或分子; q等于z除以Y的电荷; 并且L是配体，并且由通式（2）的大环有机分子表示，其中R 1，R 2，R 3和R 4可以是0，H，烷基，芳基或否则任选取代; D和D'是N，NR，PR O或S，其中R可以被H或烷基或芳基取代或以其它方式取代; t和t'是2至3的整数，s是2和4之间的整数，u是1至20的整数，v是0或1; 该金属络合物的使用量相对于骨干纤维材料为0.0001〜0.1％，其中纤维在初始pH值为7.5〜13.5之间，在20℃〜130℃的反应温度下脱木质素，反应时间在15到360分钟之间。此外，本发明涉及金属络合物的用途。

4. 发明申请

WO1994020670A1 PROCESS FOR PRODUCING CHEMOMECHANICAL AND/OR CHEMOTHERMOMECHANICAL WOOD PRODUCTS 审中-公开
标题翻译：制造CHEMO机械和/或化学 - 热 - 机械木质材料
公开(公告)号：WO1994020670A1
公开(公告)日：1994-09-15
申请号：PCT/EP1994000627
申请日：1994-03-03
申请人： STORA FELDMÜHLE AG , PATT, Rudolf , NEUMANN, Jens
发明人： STORA FELDMÜHLE AG
IPC分类号： D21C01/04
CPC分类号： D21C1/04 , D21B1/16 , D21C3/06
摘要： A process is disclosed for producing chemomechanical and/or chemothermomechanical wood products from lignocellulosic raw materials, such as wood chips. The raw materials are impregnated with a SO2-containing solution and then subjected to a sulfonating reaction in a gaseous or vapour phase at a pH value equal to 2 or less. When the sulfonating reaction is finished, the raw materials or wood chips are defibrated in a defibrating unit known per se and are crushed down to a preselected fineness degree. The wood product thus obtained is characterized by remarkable solidity and by requiring a reduced specific crushing energy.

5. 发明申请

WO1991005102A1 PROCESS FOR MANUFACTURING CHEMO-MECHANICAL AND/OR CHEMO-THERMO-MECHANICAL WOOD PULPS 审中-公开
标题翻译：制造机械和/或机械 - 机械木浆的方法
公开(公告)号：WO1991005102A1
公开(公告)日：1991-04-18
申请号：PCT/EP1990001622
申请日：1990-09-25
申请人： FELDMÜHLE AKTIENGESELLSCHAFT , PATT, Rudolf , RACHOR, Georg
发明人： FELDMÜHLE AKTIENGESELLSCHAFT
IPC分类号： D21C01/04
CPC分类号： D21C1/04 , D21B1/16 , D21C3/20
摘要： In a process for manufacturing chemo-mechanical and/or chemo-thermo-mechanical wood pulps, raw materials containing lignocellulose, such as wood shavings, wood chips, pre-ground wood or sawdust, are first impregnated with an aqueous alcoholic SO2 solution and then heated to a temperature between 50 and 170 °C for a period of 1 to 300 minutes. The wood shavings are then ground to the desired degree of fineness in a defibrinating device which is known per se. The process makes it possible to achieve up to 50 % reduction in grinding energy in comparison with known chemo-thermo-mechanical processes.

6. 发明申请

WO2011127999A1 VERFAHREN ZUM HERSTELLEN VON FASERSTOFF AUS HOLZ 审中-公开
标题翻译：方法木材生产的纸浆
公开(公告)号：WO2011127999A1
公开(公告)日：2011-10-20
申请号：PCT/EP2010/064780
申请日：2010-10-05
申请人： VOITH PATENT GMBH , PAASCH, Volker , PATT, Rudolf , KORDSACHIA, Othar
发明人： PAASCH, Volker , PATT, Rudolf , KORDSACHIA, Othar
IPC分类号： D21C3/06
CPC分类号： D21C3/06
摘要： Die Erfindung betrifft ein Verfahren zum Herstellen von Faserstoff und einen Faserstoff aus Holz mit einem Ligningehalt von mindestens 15 % für Nadelholz und von mindestens 12 % für Laubholz, jeweils bezogen auf die otro Fasermasse, mit den Schritten - Herstellen einer Chemikalienlösung mit einem pH-Wert zwischen pH 1,5 und pH 5,0, wobei zum Einstellen des pH-Wertes SO 2 -Gas in Wasser gelöst wird, und wobei Oxide, Hydroxide oder Salze von Natrium, Kalzium oder Magnesium, alternativ auch Ammonium, Methanol und/oder Ethanol als Base zugegeben werden - Mischen der Chemikalienlösung mit Holz in einem vorgegebenen Flottenverhältnis - Erwärmen der Chemikalienlösung und des Holzes auf eine Temperatur über Raumtemperatur und anschließend - entweder (1. Alternative) Entfernen frei fließender Chemikalienlösung und Aufschließen des Holzes in der Dampfphase - oder (2. Alternative) Aufschließen des Holzes in flüssiger Phase und Separieren der frei fließenden Chemikalienlösung und des Holzes.
摘要翻译：本发明涉及一种用于生产纸浆和带的至少15％为软木的木质素含量和至少12％为硬木由木材制成的纤维材料，各自基于包括以下步骤纤维的烘箱干燥质量 - 制备具有pH值的化学溶液 pH为1.5和pH 5.0，将其溶解到调整SO2气体的pH值在水，并且其中间的氧化物，氢氧化物或钠，钙或镁，或者铵，甲醇和/或乙醇作为盐碱被添加 - 化学溶液的加热和木高于室温的温度，然后温度 - - 化学品与木材中的预定液比溶液混合或者（备选1）除去自由流动的化学溶液和在气相中消化木材 - 或（2 替代）消化在自由流动的药液和去的液相和分离的木小号木材。

7. 发明申请

WO2008098601A3 FAS BLEACHING 审中-公开
标题翻译： FAS BLEACH
公开(公告)号：WO2008098601A3
公开(公告)日：2008-10-09
申请号：PCT/EP2007010166
申请日：2007-11-23
申请人： VOITH PATENT GMBH , SCHUBERT HANS-LUDWIG , AALTO ESA-MATT , PATT RUDOLF , KORDSACHIA OTHAR
发明人： SCHUBERT HANS-LUDWIG , AALTO ESA-MATT , PATT RUDOLF , KORDSACHIA OTHAR
IPC分类号： D21C9/10
CPC分类号： D21C9/1084 , D21C3/06 , D21C9/147
摘要： The invention relates to lignin-preserving bleaching of lignocellulosic primary fibres produced by the action of sulfites, by means of formamidine sulfinic acid (FAS). The invention also relates to a bleached primary fibrous material consisting of lignocellulosic material produced by the action of sulfites. Primary fibrous material consisting of coniferous wood has a lignin content of at least 15 % in relation to other fibrous materials and a breaking length of at least 7 km at 20°SR, and primary fibrous material consisting of deciduous wood has a lignin content of at least 15% in relation to other fibrous materials and a breaking length of at least 6 km at 30°SR.
摘要翻译：本发明涉及亚硫酸盐，甲脒与磺酸（FAS）的木质纤维素纤维主要的作用下产生的ligninerhaltendes的漂白。本发明还涉及使用亚硫酸盐产生的漂白初级纤维织物，木质纤维素材料，其中，从基于针木材主纸浆具有至少15％的烘箱干燥纤维的木质素含量和在20°SR的至少7公里韧度，并且其中从所述主纸浆硬木基于烘干纸浆，并在30°SR具有至少6公里的韧度为至少15％的木质素含量。

8. 发明申请

WO03002813A3 METHOD FOR DELIGNIFYING LIGNOCELLULOSIC RAW MATERIALS 审中-公开
标题翻译：方法脱木素木质纤维商品
公开(公告)号：WO03002813A3
公开(公告)日：2003-03-20
申请号：PCT/EP0207238
申请日：2002-07-01
申请人： VOITH PAPER FIBER SYSTEMS GMBH , PATT RUDOLF , KORDSACHIA OTHAR , ROSE BJOERN
发明人： PATT RUDOLF , KORDSACHIA OTHAR , ROSE BJOERN
IPC分类号： D21C3/02 , D21C3/06
CPC分类号： D21C3/06
摘要： The invention relates to a method for delignifying lignocellulosic raw materials by using sulfites in the presence of an alkaline component, especially sodium hydroxide or sodium carbonate or a mixture thereof in an aqueous solution at a high temperature and high pressure. The invention is characterized in that a first partial fragment of the alkaline component is added when the aqueous solution starts to decompose and in that at least a second partial fragment of the alkaline component is added only when delignification begins.
摘要翻译：本发明涉及一种方法，用于与升高的温度和压力的应用，其特征在于，在膨胀时，开始时脱木质素的木质纤维素原料，通过在碱成分的存在下使用亚硫酸盐，特别是氢氧化钠或碳酸钠或它们的混合物，在水溶液碱成分的第一部分量的水溶液加入，并且至少所述碱性组分的第二子集的水溶液在最早添加在脱木素开始。

9. 发明申请

WO1997039179A1 METHOD FOR BLEACHING OF LIGNOCELLULOSIC FIBERS 审中-公开
标题翻译：漂白纤维素纤维的方法
公开(公告)号：WO1997039179A1
公开(公告)日：1997-10-23
申请号：PCT/EP1997001865
申请日：1997-04-14
申请人： JASCHINSKI, Thomas , PATT, Rudolf
IPC分类号： D21C09/10
CPC分类号： D21C9/1036 , D21C9/163
摘要： The invention relates to a method for the bleaching of lignocellulosic fibers wherein lignocellulosic fibers are treated with at least one oxidizing bleaching chemical in aqueous solution. The invention also relates to the application of additives for bleaching lignocellulosic fibers and to the application of an aqueous solution containing at least one additive for bleaching lignocellulosic fibers. In the context of this paper, the term "lignocellulosic fibers" includes all sorts and types of pulp like e.g. chemical and mechanical pulp, dissolving pulp or pulp prepared from waste paper but also natural fibers like cotton or flax fibers. The method for bleaching of lignocellulosic fibers according to the invention is characterized in that lignocellulosic fibers are treated with at least one oxidizing bleaching agent in aqueous solution in the presence of at least one additive which activates delignification and/or bleaching, the additive being selected among the phenanthrolines and/or polypyridyles. The method is applicable to all known oxidizing bleaching agents like oxygen, ozone and/or peroxo-chemicals or mixtures thereof especially for peroxo-chemicals which comprise hydrogen peroxide, sodium peroxide, perborates, performic acid, peracetic acid or caroic acid and/or salts thereof.
摘要翻译：本发明涉及一种用于漂白木质纤维素纤维的方法，其中木质纤维素纤维用水溶液中的至少一种氧化漂白化学品处理。本发明还涉及用于漂白木质纤维素纤维的添加剂的应用，以及含有至少一种用于漂白木质纤维素纤维的添加剂的水溶液的应用。在本文的上下文中，术语“木质纤维素纤维”包括各种类型的纸浆，例如，化学和机械纸浆，溶解纸浆或废纸制备的纸浆，但也包括天然纤维如棉花或亚麻纤维。根据本发明的木质纤维素纤维的漂白方法的特征在于，在存在至少一种激活脱木质素和/或漂白的添加剂的情况下，用至少一种氧化漂白剂在水溶液中处理木质纤维素纤维，添加剂选自菲咯啉和/或聚吡啶基。该方法适用于所有已知的氧化漂白剂，例如氧气，臭氧和/或过氧化学物质或其混合物，特别是对于过氧化物，其包含过氧化氢，过氧化钠，过硼酸盐，甲酸，过乙酸或胡萝卜酸和/或盐它们。

10. 发明申请

WO2008098601A2 FAS BLEICHE 审中-公开
标题翻译： FAS BLEACH
公开(公告)号：WO2008098601A2
公开(公告)日：2008-08-21
申请号：PCT/EP2007/010166
申请日：2007-11-23
申请人： VOITH PATENT GMBH , SCHUBERT, Hans-Ludwig , AALTO, Esa-Matt , PATT, Rudolf , KORDSACHIA, Othar
发明人： SCHUBERT, Hans-Ludwig , AALTO, Esa-Matt , PATT, Rudolf , KORDSACHIA, Othar
IPC分类号： D21C9/10
CPC分类号： D21C9/1084 , D21C3/06 , D21C9/147
摘要： Die Erfindung betrifft ligninerhaltendes Bleichen von unter Einwirkung von Sulfiten hergestellten, lignocellulosischen Primärfasern mit Formamidin-Sulfonsäure (FAS). Die Erfindung betrifft weiter einen gebleichter Primärfaserstoff aus unter Einsatz von Sulfiten hergestelltem, lignocellulosischem Material, wobei Primärfaserstoff aus Nadel- holz einen Ligningehalt von mindestens 15 % bezogen auf otro Faserstoff und eine Reißlänge von mindestens 7 km bei 20 °SR aufweist, und wobei Primärfaserstoff aus Laubholz einen Ligningehalt von mindestens 15 % bezogen auf otro Faserstoff und eine Reißlänge von mindestens 6 km bei 30 °SR aufweist.
摘要翻译：
本发明涉及亚硫酸盐，木素纤维素的Prim＆AUML的作用下产生的ligninerhaltendes漂白; rfasern与甲脒磺酸BEAR酸（FAS）。本发明还涉及一种漂白的Prim＆AUML; rfaserstoff使用亚硫酸盐产生，木质纤维素材料，的Prim＆AUML所述; rfaserstoff针叶木具有至少15％的木质素含量基于烘箱干燥的纸浆和丽ROAD L＆AUML;至少7公里长度在20 °SR，并且其中的Prim＆AUML; rfaserstoff硬木基于烘干纸浆和丽ROAD L＆AUML的至少15％的木质素含量;在30℃的至少6公里长度SR具有

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