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1. 发明授权

US10047452B2 Film formation device and film formation method for forming metal film 有权
公开(公告)号：US10047452B2
公开(公告)日：2018-08-14
申请号：US14371036
申请日：2013-02-21
申请人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
发明人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
IPC分类号： C25B9/00 , C25D17/00 , C25D3/00 , C25D5/02 , C25D5/08 , C25D17/12 , C25D17/14 , C25D21/14 , C25D5/34 , C25D3/38
摘要： Provided are a film formation device and a film formation method for forming a metal film, with which metal films with a desired thickness can be continuously formed on surfaces of a plurality of substrates. A film formation device 1A includes at least a positive electrode 11, a negative electrode 12, a solid electrolyte membrane 13 arranged on a surface of the positive electrode 12, between. the positive electrode and a substrate to serve as the negative electrode, and a power supply unit E adapted to apply a voltage across the positive electrode 11 and the substrate B. A voltage is applied across the positive electrode 11 and the substrate B to deposit metal on a surface of the substrate from metal ions contained in the solid electrolyte membrane 13, whereby a metal film F made of metal is formed, The positive electrode 11 is made of a porous body that allows a solution L containing metal ions to pass therethrough and supplies the metal ions to the solid electrolyte membrane 13.

2. 发明授权

US09957634B2 Film formation device and film formation method for forming metal film 有权
公开(公告)号：US09957634B2
公开(公告)日：2018-05-01
申请号：US14371036
申请日：2013-02-21
申请人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
发明人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
IPC分类号： C25B9/00 , C25D17/00 , C25D3/00 , C25D17/12 , C25D5/08 , C25D21/14 , C25D5/02 , C25D5/34 , C25D17/14 , C25D3/38
摘要： Provided are a film formation device and a film formation method for forming a metal film, with which metal films with a desired thickness can be continuously formed on surfaces of a plurality of substrates. A film formation device 1A includes at least a positive electrode 11, a negative electrode 12, a solid electrolyte membrane 13 arranged on a surface of the positive electrode 12, between. the positive electrode and a substrate to serve as the negative electrode, and a power supply unit E adapted to apply a voltage across the positive electrode 11 and the substrate B. A voltage is applied across the positive electrode 11 and the substrate B to deposit metal on a surface of the substrate from metal ions contained in the solid electrolyte membrane 13, whereby a metal film F made of metal is formed, The positive electrode 11 is made of a porous body that allows a solution L containing metal ions to pass therethrough and supplies the metal ions to the solid electrolyte membrane 13.

3. 发明授权

US08052858B2 Pretreatment method for electroless plating material and method for producing member having plated coating 有权
标题翻译：化学镀材料的预处理方法及具有镀覆层的构件的制造方法
公开(公告)号：US08052858B2
公开(公告)日：2011-11-08
申请号：US10530516
申请日：2003-10-09
申请人： Motoki Hiraoka , Takeshi Bessho , Sigeru Sibata
发明人： Motoki Hiraoka , Takeshi Bessho , Sigeru Sibata
IPC分类号： B05D3/02 , C25D5/56 , C25D5/34 , C23C28/02 , C23C18/18 , C23C18/22 , C23C18/26
CPC分类号： C23C18/1653 , C23C18/2006 , C23C18/204
摘要： A resin material is brought into contact with a first solution containing ozone, and at the same time, ultraviolet rays are irradiated. The activation due to the treatment with ozone water and the activation due to the treatment with ultraviolet rays are synergistically operated to enable the formation of a plated coating having excellent adhesive strength by a short treatment. In addition, even by a long treatment, the adhesive strength can be restrained from lowering. Consequently, a plated coating having excellent adhesion can be formed without roughening the surface of the resin material by a short pretreatment.
摘要翻译：使树脂材料与含有臭氧的第一溶液接触，同时照射紫外线。由臭氧水处理引起的活化和紫外线处理引起的活化协同作用，能够通过短时间处理形成具有优异粘合强度的镀覆层。此外，即使通过长时间处理，也可以抑制粘合强度的降低。因此，可以通过短预处理而不使树脂材料的表面粗糙化来形成具有优异粘附性的镀覆涂层。

4. 发明申请

US20070110973A1 Resin substrate having a resin-metal composite layer and method for manufacturing thereof 有权
标题翻译：具有树脂金属复合层的树脂基板及其制造方法
公开(公告)号：US20070110973A1
公开(公告)日：2007-05-17
申请号：US10565215
申请日：2004-07-22
申请人： Motoki Hiraoka , Fumitaka Yoshinaga , Setsuto Daiza , Takeshi Bessho
发明人： Motoki Hiraoka , Fumitaka Yoshinaga , Setsuto Daiza , Takeshi Bessho
IPC分类号： B05D3/10 , B05D1/36 , B32B27/04 , B32B5/16
CPC分类号： H05K3/38 , C23C18/08 , C23C18/2033 , C23C18/2086 , C23C18/31 , H05K3/181 , H05K2201/2063 , H05K2203/1152 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31678
摘要： A resin-metal composite layer is formed by modifying a surface of a resin substrate to a modified layer, contacting the modified layer with a metal compound solution, and adsorbing at least either metal colloids or ions are adsorbed to the polar group, so that metal particles are dispersed into the modified layer. Because of the fineness of the metal particles in the resin-metal composite layer, high transparent can be achieved. The resin-metal composite layer functions as a transparent conductive layer and the like.
摘要翻译：通过将树脂基板的表面改性为改性层，使改性层与金属化合物溶液接触而吸附至少一种金属胶体或离子而形成树脂 - 金属复合层，从而金属颗粒分散在改性层中。由于树脂 - 金属复合层中的金属颗粒的细度，可以实现高透明度。树脂 - 金属复合层用作透明导电层等。

5. 发明授权

US09514870B2 Rare earth magnet and method for producing the same 有权
标题翻译：稀土磁铁及其制造方法
公开(公告)号：US09514870B2
公开(公告)日：2016-12-06
申请号：US13978788
申请日：2012-02-13
申请人： Yuji Kaneko , Hisaaki Takao , Yukio Takada , Motoki Hiraoka , Keiu Kanada
发明人： Yuji Kaneko , Hisaaki Takao , Yukio Takada , Motoki Hiraoka , Keiu Kanada
IPC分类号： C23C10/28 , C23C10/06 , H01F1/08 , H01F41/02 , C22C38/00 , C22C38/10 , C22C38/16 , C22C1/00 , B22F3/10 , H01F41/00 , B22F3/24 , C22C1/02 , H01F1/057
CPC分类号： H01F1/086 , B22F3/1007 , B22F3/24 , B22F2003/241 , B22F2203/11 , B22F2207/01 , C22C1/00 , C22C1/02 , C22C38/002 , C22C38/005 , C22C38/10 , C22C38/16 , C22C2202/02 , H01F1/0577 , H01F41/005 , H01F41/0266 , H01F41/0293
摘要： A rare earth magnet production method of the present invention includes a placing step of placing a magnet material including a compact or a sintered body of powder particles having a rare earth magnet alloy, and a diffusing material containing a diffusing element to improve coercivity, in a vicinity of each other; and a diffusing step of diffusing the diffusing element into an inside of the magnet material by exposing the magnet material heated to vapor of the diffusing element evaporated from the diffusing material heated; and wherein the diffusing step is a step of heating the diffusing material independently of the magnet material to diffusing material temperature which is different from heating temperature of the magnet material called magnet material temperature.
摘要翻译：本发明的稀土类磁体制造方法包括：放置步骤，放置包括具有稀土类磁体合金的粉末颗粒的致密体或烧结体的磁体材料和包含扩散元件的扩散材料以提高矫顽力，相邻; 以及扩散步骤，通过使被加热的扩散材料蒸发的扩散元件被加热至蒸汽的磁体材料暴露而将漫射元件扩散到磁体材料的内部; 并且其中所述漫射步骤是独立于所述磁体材料加热所述漫射材料以扩散材料温度的步骤，所述扩散材料温度不同于称为磁体材料温度的所述磁体材料的加热温度。

6. 发明申请

US20130335180A1 RARE EARTH MAGNET AND PROCESS FOR PRODUCING SAME 有权
标题翻译：稀土磁铁及其生产方法
公开(公告)号：US20130335180A1
公开(公告)日：2013-12-19
申请号：US14000537
申请日：2012-03-08
申请人： Yuji Kaneko , Yukio Takada , Motoki Hiraoka , Keiu Kanada
发明人： Yuji Kaneko , Yukio Takada , Motoki Hiraoka , Keiu Kanada
IPC分类号： H01F7/02 , H01F41/02
CPC分类号： H01F7/02 , B22F3/24 , B22F2003/241 , B22F2003/248 , C23C10/28 , H01F1/0577 , H01F41/0293
摘要： A process for producing a rare earth magnet comprises: an adhesion step of causing a diffusion element capable of diffusing inwardly to adhere to the surface part of a magnet material comprising a compact or sintered body of rare earth alloy particles; and an evaporation step of heating the magnet material in vacuum to evaporate at least a portion of the diffusion element having been retained on or in the surface part of the magnet material.
摘要翻译：稀土类磁体的制造方法包括：使能够向内扩散的扩散元件附着在包含稀土类合金粒子的致密体或烧结体的磁体材料的表面部分的粘合工序; 以及蒸发步骤，在真空中加热所述磁体材料，以蒸发所述扩散元件的至少一部分已被保留在所述磁体材料的表面部分或其表面部分中。

7. 发明申请

US20130315775A1 RARE EARTH MAGNET AND METHOD FOR PRODUCING THE SAME 有权
标题翻译：稀土磁铁及其制造方法
公开(公告)号：US20130315775A1
公开(公告)日：2013-11-28
申请号：US13978788
申请日：2012-02-13
申请人： Yuji Kaneko , Hisaaki Takao , Yukio Takada , Motoki Hiraoka , Keiu Kanada
发明人： Yuji Kaneko , Hisaaki Takao , Yukio Takada , Motoki Hiraoka , Keiu Kanada
IPC分类号： H01F1/08 , H01F41/02 , H01F41/00
CPC分类号： H01F1/086 , B22F3/1007 , B22F3/24 , B22F2003/241 , B22F2203/11 , B22F2207/01 , C22C1/00 , C22C1/02 , C22C38/002 , C22C38/005 , C22C38/10 , C22C38/16 , C22C2202/02 , H01F1/0577 , H01F41/005 , H01F41/0266 , H01F41/0293
摘要： A rare earth magnet production method of the present invention includes a placing step of placing a magnet material including a compact or a sintered body of powder particles having a rare earth magnet alloy, and a diffusing material containing a diffusing element to improve coercivity, in a vicinity of each other; and a diffusing step of diffusing the diffusing element into an inside of the magnet material by exposing the magnet material heated to vapor of the diffusing element evaporated from the diffusing material heated; and wherein the diffusing step is a step of heating the diffusing material independently of the magnet material to diffusing material temperature which is different from heating temperature of the magnet material called magnet material temperature.
摘要翻译：本发明的稀土类磁体制造方法包括：放置步骤，放置包括具有稀土类磁体合金的粉末颗粒的致密体或烧结体的磁体材料和包含扩散元件的扩散材料以提高矫顽力，相邻; 以及扩散步骤，通过使被加热的扩散材料蒸发的扩散元件被加热至蒸汽的磁体材料暴露而将漫射元件扩散到磁体材料的内部; 并且其中所述漫射步骤是独立于所述磁体材料加热所述漫射材料以扩散材料温度的步骤，所述扩散材料温度不同于称为磁体材料温度的所述磁体材料的加热温度。

8. 发明申请

US20130195710A1 METHOD FOR MANUFACTURING RARE-EARTH MAGNET 有权
标题翻译：制造稀土磁铁的方法
公开(公告)号：US20130195710A1
公开(公告)日：2013-08-01
申请号：US13750576
申请日：2013-01-25
申请人： Kazuaki HAGA , Noritaka MIYAMOTO , Tetsuya SHOJI , Noritsugu SAKUMA , Shinya OMURA , Motoki HIRAOKA
发明人： Kazuaki HAGA , Noritaka MIYAMOTO , Tetsuya SHOJI , Noritsugu SAKUMA , Shinya OMURA , Motoki HIRAOKA
IPC分类号： H01F41/00
CPC分类号： H01F41/005 , B22F3/14 , B22F3/26 , B22F2009/048 , C22C28/00 , C22C30/00 , C22C38/00 , H01F41/0293
摘要： Provided is a manufacturing method of a rare-earth magnet capable of penetrant-diffusing a modifier alloy to increase a coercive force (especially a coercive force under a high-temperature atmosphere) at a temperature lower than the conventional method for manufacturing a rare-earth magnet without using heavy rare-earth metals such as Dy and Tb, and accordingly capable of manufacturing a high coercivity rare-earth magnet at the lowest cost possible. A method for manufacturing a rare-earth magnet includes the steps of: first step of pressing-forming powder as a rare-earth magnet material to form a compact S, the powder including a RE-Fe—B main phase MP (RE: at least one type of Nd and Pr) and a RE-X alloy (X: metal element) grain boundary phase surrounding the main phase; and second step of bringing a modifier alloy M into contact with the compact S or a rare-earth magnet precursor C obtained by hot deformation processing of the compact S, followed by heat treatment to penetrant-diffuse melt of the modifier alloy M into the compact S or the rare-earth magnet precursor C to manufacture the rare-earth magnet RM, the modifier alloy including a RE-Y (Y: metal element and not including a heavy rare-earth element) alloy having a eutectic or a RE-rich hyper eutectic composition.
摘要翻译：本发明提供一种稀土类磁铁的制造方法，该稀土类磁体能够在比传统稀土制造方法低的温度下，使改性剂合金渗透扩散以提高矫顽力（特别是高温环境下的矫顽力）磁体，而不使用重稀土金属如Dy和Tb，因此能够以最低成本制造高矫顽力稀土类磁体。一种稀土类磁铁的制造方法，其特征在于，包括以下步骤：作为稀土类磁铁材料的压制成形粉末的第一工序，形成小型S，所述粉末含有RE-Fe-B主相MP（RE：at 至少一种Nd和Pr）和围绕主相的RE-X合金（X：金属元素）晶界; 将改性合金M与压制体S的热变形加工得到的压粉体S或稀土类磁体前体C接触，然后对改性合金M的渗透扩散熔体进行热处理， S或稀土磁体前体C制造稀土磁体RM，改性合金包括具有共晶或富RE的Y-Y（Y：金属元素，不包括重稀土元素）合金超共晶组成。

9. 发明授权

US09257227B2 Method for manufacturing rare-earth magnet 有权
标题翻译：制造稀土磁铁的方法
公开(公告)号：US09257227B2
公开(公告)日：2016-02-09
申请号：US13750576
申请日：2013-01-25
申请人： Kazuaki Haga , Noritaka Miyamoto , Tetsuya Shoji , Noritsugu Sakuma , Shinya Omura , Motoki Hiraoka
发明人： Kazuaki Haga , Noritaka Miyamoto , Tetsuya Shoji , Noritsugu Sakuma , Shinya Omura , Motoki Hiraoka
IPC分类号： H01F41/00 , H01F41/02
CPC分类号： H01F41/005 , B22F3/14 , B22F3/26 , B22F2009/048 , C22C28/00 , C22C30/00 , C22C38/00 , H01F41/0293
摘要： Provided is a manufacturing method of a rare-earth magnet with high coercive force, including a first step of pressing-forming powder as a rare-earth magnet material to form a compact S, the powder including a RE-Fe—B main phase MP (RE: at least one type of Nd and Pr) and a RE-X alloy (X: metal element) grain boundary phase surrounding the main phase; and second step of bringing a modifier alloy M into contact with the compact S or a rare-earth magnet precursor C obtained by hot deformation processing of the compact S, followed by heat treatment to penetrant diffuse melt of the modifier alloy M into the compact S or the rare-earth magnet precursor C to manufacture the rare-earth magnet RM, the modifier alloy including a RE-Y (Y: metal element and not including a heavy rare-earth element) alloy having a eutectic or a RE-rich hyper-eutectic composition.
摘要翻译：提供一种具有高矫顽力的稀土类磁体的制造方法，包括：作为稀土类磁铁材料的压制成形粉末的第一工序，形成小型S，该粉末包括RE-Fe-B主相MP （RE：至少一种Nd和Pr）和围绕主相的RE-X合金（X：金属元素）晶界; 将改性剂合金M与压制体S的热变形加工得到的压块S或稀土类磁体前体C接触，然后进行热处理，将改性合金M的扩散熔融渗透到压块S中或稀土磁体前体C制造稀土磁体RM，改性合金包括具有共晶或富含RE的超高分子量的RE-Y（Y：金属元素，不包括重稀土元素）合金共晶组成。

10. 发明申请

US20150014178A1 FILM FORMATION DEVICE AND FILM FORMATION METHOD FOR FORMING METAL FILM 审中-公开
标题翻译：薄膜形成装置和薄膜形成方法形成金属薄膜
公开(公告)号：US20150014178A1
公开(公告)日：2015-01-15
申请号：US14371036
申请日：2013-02-21
申请人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
发明人： Motoki Hiraoka , Hiroshi Yanagimoto , Yuki Sato , Takayasu Yoshioka
IPC分类号： C25D17/00 , C25D21/14
CPC分类号： C25D17/00 , C25D3/00 , C25D3/38 , C25D5/02 , C25D5/022 , C25D5/08 , C25D5/34 , C25D17/005 , C25D17/12 , C25D17/14 , C25D21/14
摘要： Provided are a film formation device and a film formation method for forming a metal film, with which metal films with a desired thickness can be continuously formed on surfaces of a plurality of substrates. A film formation device 1A includes at least a positive electrode 11, a negative electrode 12, a solid electrolyte membrane 13 arranged on a surface of the positive electrode 12, between. the positive electrode and a substrate to serve as the negative electrode, and a power supply unit E adapted to apply a voltage across the positive electrode 11 and the substrate B. A voltage is applied across the positive electrode 11 and the substrate B to deposit metal on a surface of the substrate from metal ions contained in the solid electrolyte membrane 13, whereby a metal film F made of metal is formed, The positive electrode 11 is made of a porous body that allows a solution L containing metal ions to pass therethrough and supplies the metal ions to the solid electrolyte membrane 13.
摘要翻译：提供一种用于形成金属膜的成膜装置和成膜方法，可以在多个基板的表面上连续地形成具有所需厚度的金属膜。成膜装置1A至少包括正极11，负极12，布置在正极12的表面上的固体电解质膜13。正电极和用作负极的衬底，以及适于在正电极11和衬底B两端施加电压的电源单元E.跨正电极11和衬底B施加电压以沉积金属在固体电解质膜13中的金属离子的表面上形成由金属制成的金属膜F.正极11由允许含有金属离子的溶液L通过的多孔体构成，将金属离子供给固体电解质膜13。

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