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    • 3. 发明授权
    • Process for manufacturing sintered polybenzimidazole article
    • 制造烧结聚苯并咪唑制品的方法
    • US5770142A
    • 1998-06-23
    • US874860
    • 1997-06-13
    • Yoshisato SasakiMinoru Kurisaki
    • Yoshisato SasakiMinoru Kurisaki
    • B29C43/02B29C43/52B29C67/04B29K79/00C08G73/18C08G33/02B27J5/00C08J5/00
    • C08G73/18
    • Provided is a process for manufacturing sintered polybenzimidazole (PBI) articles at high yields, said articles having neither voids nor porous, low-strength parts resulting from oxidative deterioration. To produce said sintered PBI articles from a particulate PBI resin, said PBI resin is compacted in a closed mold, the mold is heated up to a predetermined temperature of from 350.degree. to 600.degree. C. without applying any external pressure thereto, then, after having heated up to said predetermined temperature, the mold is pressed to have a predetermined external pressure of from 140 to 1400 kg/cm2 at said predetermined temperature whereby the resin is sintered for from 60 to 350 minutes under that conditions, and finally the sintered PBI article is cooled and taken out of the mold.
    • 提供了以高产率制造聚苯并咪唑烧结体(PBI)制品的方法,所述制品既没有空隙,也没有由氧化劣化导致的多孔低强度部件。 为了从颗粒PBI树脂制备所述烧结的PBI制品,所述PBI树脂在闭合的模具中压实,将模具加热至350-600℃的预定温度,而不施加任何外部压力,然后在 在所述预定温度下加热到所述预定温度,在所述预定温度下将模具压制成具有140至1400kg / cm 2的预定外部压力,由此在该条件下将树脂烧结60至350分钟,最后将烧结的PBI 制品被冷却并从模具中取出。