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1. 发明授权

US08597731B2 Method for applying a diamond layer onto a graphite substrate 有权
标题翻译：在金刚石基底上涂布金刚石层的方法
公开(公告)号：US08597731B2
公开(公告)日：2013-12-03
申请号：US12338107
申请日：2008-12-18
申请人： Matthias Fryda , Thorsten Matthee , Shane Mulcahy
发明人： Matthias Fryda , Thorsten Matthee , Shane Mulcahy
IPC分类号： C23C16/44
CPC分类号： C23C16/0218 , C04B41/009 , C04B41/52 , C04B41/89 , C23C16/0236 , C23C16/27 , C30B25/02 , C30B25/18 , C30B29/04 , C04B41/5346 , C04B41/4539 , C04B41/5002 , C04B41/4531 , C04B35/522
摘要： A diamond layer can be applied stably onto a graphite substrate in a CVD process when the graphite substrate is subjected to the following pretreatment steps before the CVD process: fine cleaning of the surface in a vacuum at a temperature >500° C., preferably >800° C., in an etching gas atmosphere, mechanical removal of loose particles, seeding of the substrate surface with very small diamond particles and at least one degassing treatment in a vacuum to remove adsorbed hydrocarbons and adsorbed air at a temperature T>500° C., preferably T>700° C.
摘要翻译：在CVD工艺之前对石墨基板进行以下预处理步骤时，可以在CVD工艺中将金刚石层稳定地应用于石墨基板上：在温度> 500℃的真空中对表面进行精细清洗，优选> 800℃，在蚀刻气体气氛中，机械去除松散颗粒，用非常小的金刚石颗粒接种基材表面，并在真空中进行至少一次脱气处理以在温度T> 500°C下除去吸附的烃和吸附的空气 C.，优选T> 700℃

2. 发明授权

US08366945B2 Diamond electrode and process for producing it 有权
标题翻译：金刚石电极及其生产工艺
公开(公告)号：US08366945B2
公开(公告)日：2013-02-05
申请号：US12337770
申请日：2008-12-18
申请人： Matthias Fryda , Thorsten Matthee
发明人： Matthias Fryda , Thorsten Matthee
IPC分类号： H01B13/00 , B44C1/22
CPC分类号： C25B11/0447 , C02F2001/46138 , Y10T428/24355
摘要： Diamond electrodes with improved adhesion of the diamond layer to the electrode are produced by sandblasting a surface of the electrode body, and then non-oxidatively etching the roughened (sandblasted) surface so as to remove at least 5 μm of material from under the roughened surface. By removing at least 5 μm of material, the sand particulates in the surface of the electrode body are eliminated, and damage in the form of cracks in the electrode body which result from sandblasting is reduced or eliminated, and further, a surface metal oxide coating is not created. All of these contribute to preparing a surface where spalling of the diamond layer is less likely to occur. Concentrated phosphoric acid is an exemplary non-oxidative etchant used in the process.
摘要翻译：金刚石层与电极的附着力提高的金刚石电极是通过对电极体的表面进行喷砂，然后非氧化蚀刻粗糙（喷砂）表面，从而从粗糙表面下面除去至少5微米的材料。通过除去至少5微米的材料，消除了电极体表面的砂粒，减少或消除了由喷砂造成的电极体中的裂纹形式的损伤，此外，表面金属氧化物涂层没有创建所有这些都有助于制备难以发生金刚石层剥落的表面。浓磷酸是本方法中使用的示例性非氧化蚀刻剂。

3. 发明申请

US20090162549A1 Method for Applying a Diamond Layer Onto a Graphite Substrate 有权
标题翻译：将金刚石层应用于石墨基材的方法
公开(公告)号：US20090162549A1
公开(公告)日：2009-06-25
申请号：US12338107
申请日：2008-12-18
申请人： Matthias Fryda , Thorsten Matthee , Shane Mulcahy
发明人： Matthias Fryda , Thorsten Matthee , Shane Mulcahy
IPC分类号： C23C16/44
CPC分类号： C23C16/0218 , C04B41/009 , C04B41/52 , C04B41/89 , C23C16/0236 , C23C16/27 , C30B25/02 , C30B25/18 , C30B29/04 , C04B41/5346 , C04B41/4539 , C04B41/5002 , C04B41/4531 , C04B35/522
摘要： A diamond layer can be applied stably onto a graphite substrate in a CVD process when the graphite substrate is subjected to the following pretreatment steps before the CVD process: fine cleaning of the surface in a vacuum at a temperature >500° C., preferably >800° C., in an etching gas atmosphere, mechanical removal of loose particles, seeding of the substrate surface with very small diamond particles and at least one degassing treatment in a vacuum to remove adsorbed hydrocarbons and adsorbed air at a temperature T>500° C., preferably T>700° C.
摘要翻译：在CVD工艺之前对石墨基板进行以下预处理步骤时，可以在CVD工艺中将金刚石层稳定地应用于石墨基板上：在温度> 500℃的真空中对表面进行精细清洗，优选> 800℃，在蚀刻气体气氛中，机械去除松散颗粒，用非常小的金刚石颗粒接种基材表面，并在真空中进行至少一次脱气处理以在温度T> 500°C下除去吸附的烃和吸附的空气 C.，优选T> 700℃

4. 发明授权

US06558380B2 Instrument for surgical purposes and method of cleaning same 失效
标题翻译：手术用仪器及清洗方法
公开(公告)号：US06558380B2
公开(公告)日：2003-05-06
申请号：US09732862
申请日：2000-12-08
申请人： Christian Lingenfelder , Stephan Ertl , Stefan Strobel , Rudolf Rösch , Siegfried Förster , Matthias Fryda , Lothar Schäfer , Inga Tröster , Dennie Herrmann
发明人： Christian Lingenfelder , Stephan Ertl , Stefan Strobel , Rudolf Rösch , Siegfried Förster , Matthias Fryda , Lothar Schäfer , Inga Tröster , Dennie Herrmann
IPC分类号： A61B1818
CPC分类号： A61B18/1442 , A61B2018/1462 , A61B2090/0813
摘要： An instrument for surgical purposes, especially for coagulation, is proposed. This instrument has at least one arm, the tips of the arms having electrical contact regions which can be electrically connected to a control unit for touching a tissue for the purpose of coagulation. The contact regions are formed from doped diamond to produce the electrical conductivity.
摘要翻译：提出了一种用于外科手术，特别是用于凝血的仪器。该仪器具有至少一个臂，臂的尖端具有电接触区域，该电接触区域可以电连接到用于接触组织以用于凝结的控制单元。接触区由掺杂的金刚石形成以产生导电性。

5. 发明授权

US06855242B1 Electrochemical production of peroxopyrosulphuric acid using diamond coated electrodes 有权
标题翻译：使用金刚石涂层电极电化学生产过氧化吡咯硫酸
公开(公告)号：US06855242B1
公开(公告)日：2005-02-15
申请号：US10110010
申请日：2000-10-04
申请人： Christos Comninellis , Pierre A. Michaud , Werner Hänni , Andre Perret , Matthias Fryda
发明人： Christos Comninellis , Pierre A. Michaud , Werner Hänni , Andre Perret , Matthias Fryda
IPC分类号： C25B11/02 , C25B1/28 , C25B1/30 , C25B11/04 , C25B11/06
CPC分类号： C25B1/285
摘要： A process for the electrochemical production of peroxo-disulfuric acid and peroxo-disulfates is provided. In the process, an anode having a partially pre-polarized electrode which has been provided with a doped diamond layer is used.
摘要翻译：提供过氧二硫酸和过氧二硫酸盐的电化学生产方法。在该过程中，使用具有已经设置有掺杂金刚石层的部分预极化电极的阳极。

6. 发明授权

US06850598B1 X-ray anode and process for its manufacture 失效
标题翻译： X射线阳极及其制造方法
公开(公告)号：US06850598B1
公开(公告)日：2005-02-01
申请号：US10030133
申请日：2000-07-24
申请人： Matthias Fryda , Lothar Schafer , Thorston Matthee
发明人： Matthias Fryda , Lothar Schafer , Thorston Matthee
IPC分类号： G21K5/00 , G21K5/08 , G21K7/00 , H01J9/14 , H01J35/08 , H01J35/10 , H01J35/18 , H01J35/24
CPC分类号： H01J35/18 , H01J35/10 , H01J2235/186
摘要： The invention relates to an x-ray anode and a process for its manufacture. The x-ray anode is characterized in that the anode material is embodied as a layer on a diamond window. The x-ray anode is preferably used with x-ray units which require as selective as possible x-radiation production to achieve as high as possible radiation intensity. Use in x-ray microscopes in which a high radiation intensity guarantees the highest resolutions is particularly preferred.
摘要翻译：本发明涉及一种X射线阳极及其制造方法。 x射线阳极的特征在于阳极材料被实施为钻石窗上的层。 x射线阳极优选与需要尽可能选择性的x射线产生的X射线单元一起使用以实现尽可能高的辐射强度。在其中高辐射强度保证最高分辨率的X射线显微镜中使用是特别优选的。

7. 发明申请

US20090169815A1 Diamond electrode and process for producing it 有权
标题翻译：金刚石电极及其生产工艺
公开(公告)号：US20090169815A1
公开(公告)日：2009-07-02
申请号：US12337770
申请日：2008-12-18
申请人： Matthias Fryda , Thorsten Matthee
发明人： Matthias Fryda , Thorsten Matthee
IPC分类号： H01B13/00 , B32B5/00
CPC分类号： C25B11/0447 , C02F2001/46138 , Y10T428/24355
摘要： A process for producing a diamond electrode, comprising the following process steps roughening the surface of the electrode body by sand blasting, etching the roughened surface, and building up the diamond layer on the electrode body, results in improved adhesion of the diamond layer to the electrode body by virtue of non-oxidative etching of the electrode body being performed in such a way that more than 5 μm of the material of the electrode body under the roughened surface is removed.
摘要翻译：一种用于制造金刚石电极的方法，包括以下工艺步骤：通过喷砂，使粗糙化表面腐蚀电极体的表面，以及在电极体上建立金刚石层，从而改善金刚石层与通过非电氧化蚀刻电极体的方式，使电极体的粗糙表面下方的5μm以上的材料被去除。

8. 发明申请

US20080156642A1 System for the Disinfection of Low-Conductivity Liquids 审中-公开
标题翻译：低电导率液体消毒系统
公开(公告)号：US20080156642A1
公开(公告)日：2008-07-03
申请号：US11817655
申请日：2006-03-01
申请人： Matthias Fryda , Thorsten Matthee
发明人： Matthias Fryda , Thorsten Matthee
IPC分类号： C02F1/467
CPC分类号： A61L2/03 , C02F1/281 , C02F1/32 , C02F1/4672 , C02F2201/4613 , C02F2201/46195
摘要： A system for the disinfecting of low-conductivity liquids, in particular water, is provided. The system includes an electrochemical cell in which electrodes are arranged such that the liquid flushes or flows around them, and in which oxidizing agents are produced from the liquid by applying a current. A mixing unit is mounted downstream of the electrochemical cell in the flow direction, in which mixing unit the oxidizing agents are intermixed with the liquid.
摘要翻译：提供了用于消除低电导率液体，特别是水的系统。该系统包括电化学电池，其中电极布置成使得液体在其周围闪烁或流动，并且其中通过施加电流从液体产生氧化剂。混合单元沿流动方向安装在电化学电池的下游，其中混合单元将氧化剂与液体混合。

9. 发明申请

US20070095655A1 Electrode assembly for the electrochemical treatment of liquids with a low conductivity 失效
标题翻译：电极组件，用于电导率低的液体电化学处理
公开(公告)号：US20070095655A1
公开(公告)日：2007-05-03
申请号：US10599267
申请日：2005-03-24
申请人： Manuela Stadelmann , Manfred Blaschke , Maja Wuensche , Helmut Petzer , Alexander Kraft , Thorsten Matthee , Matthias Fryda
发明人： Manuela Stadelmann , Manfred Blaschke , Maja Wuensche , Helmut Petzer , Alexander Kraft , Thorsten Matthee , Matthias Fryda
IPC分类号： C25B9/00
CPC分类号： C02F1/46109 , C02F1/4672 , C02F2001/46138 , C02F2103/04 , C02F2201/46195 , C25B9/18 , C25B9/203
摘要： The invention relates to an electrode assembly for the electrochemical treatment of liquids with a low conductivity. Said assembly comprises electrodes (1, 2), between which a polymer solid electrolyte (3) is situated. The electrodes are pressed against one another by means of a compression device (9, 10; 91) and are configured in such a way that the assembly can be traversed by the liquid To produce said assembly simply and to ensure that it is flexible and easy to use, the compression device (9, 10; 91) is supported on the electrodes (1, 2).
摘要翻译：本发明涉及一种用于电化学处理低导电性液体的电极组件。所述组件包括电极（1,2），其间位于聚合物固体电解质（3）之间。电极通过压缩装置（9,10; 91）彼此压靠，并且被构造成使得组件能够被液体穿过。为了简单地产生所述组件并确保其柔性和容易为了使用，压缩装置（9,10; 91）被支撑在电极（1,2）上。

10. 发明申请

US20050139487A1 Method for the oxidative treatment of components comprised of or containing elementary silicon and/or substantially inorganic silicon compounds 审中-公开
标题翻译：用于氧化处理包含或含有基本硅和/或基本无机硅化合物的组分的方法
公开(公告)号：US20050139487A1
公开(公告)日：2005-06-30
申请号：US10512765
申请日：2003-05-02
申请人： Gerfried Zwicker , Matthias Fryda , Thorsten Matthee
发明人： Gerfried Zwicker , Matthias Fryda , Thorsten Matthee
IPC分类号： A61L2/18 , C02F1/461 , C25B1/28 , C25B1/30
CPC分类号： C25B1/30 , C25B1/285
摘要： In a method for the treatment of an object made of silicon or an inorganic, optionally organically modified, silicon compound, an oxidizing agent is prepared by electrolysis of an aqueous solution in an electrolysis device. The anode of the electrolysis device is a silicon electrode. The anode has an overvoltage for oxygen so that upon electrolysis of water the formation of hydrogen peroxide is preferred over that of oxygen. The aqueous solution used in electrolysis contains at least one reactive component or a constituent that is converted by electrolysis of the solution into a reactive component. The object to be treated is contacted with the freshly prepared oxidizing agent. The oxidizing agent is circulated and returned into the electrolysis device to be regenerated.
摘要翻译：在用于处理由硅或无机，任选有机改性的硅化合物制成的物体的方法中，通过在电解装置中电解水溶液来制备氧化剂。电解装置的阳极是硅电极。阳极具有氧的过电压，因此在电解水时，过氧化氢的形成优于氧气。用于电解的水溶液含有至少一种反应性组分或通过溶液电解转化成反应性组分的组分。将待处理的物体与新制备的氧化剂接触。氧化剂循环并返回到电解装置中以再生。

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