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1. 发明授权

US4720541A Process for improving the application properties of disazo pigments 失效
标题翻译：改善双偶氮颜料应用性能的方法
公开(公告)号：US4720541A
公开(公告)日：1988-01-19
申请号：US627497
申请日：1984-07-06
申请人： Wolfgang Rieper , Klaus Hunger
发明人： Wolfgang Rieper , Klaus Hunger
IPC分类号： C09B67/10 , C09B67/14 , C09B35/035 , C09D7/12 , D06P1/44
CPC分类号： C09B67/0017 , C09B67/0015
摘要： Process for improving the application properties of disazo pigments obtained by coupling bis-diazotized chlorine-substituted 4,4'-diaminobiphenyls with acetoacetylaminobenzenes, which includes adding sulfite ions to the pigment suspension obtained in the coupling and then heating for one half to two hours at 50.degree. to 100.degree. C. The process produces, above all in large scale industrial batches, a product of uniform quality and having acceptable fastness to solvents, overlacquering, migration and bleeding.
摘要翻译：通过将双重重氮化的氯取代的4,4'-二氨基联苯与乙酰乙酰氨基苯偶联而获得的双偶氮颜料的应用性能的改进方法，其包括将亚硫酸根离子加入到偶联中得到的颜料悬浮液中，然后加热半小时至两小时 50℃至100℃。该工艺首先在大规模工业批次中生产质量均匀且具有可接受的溶剂牢度，超标，迁移和渗出的产品。

2. 发明授权

US4665163A Diaryl pigments with improved heat stability obtained by coupling bis-diazotized diamines with acetoacetanilides 失效
标题翻译：通过将双重重氮化二胺与乙酰乙酰苯胺偶联获得的具有改善的热稳定性的二芳基颜料
公开(公告)号：US4665163A
公开(公告)日：1987-05-12
申请号：US507711
申请日：1983-06-23
申请人： Klaus Hunger , Heinrich Frolich , Hans-Joachim Lenz
发明人： Klaus Hunger , Heinrich Frolich , Hans-Joachim Lenz
IPC分类号： C09B35/033 , C09B35/10 , C09B41/00 , C09B35/035 , C09B67/20 , C09D11/02
CPC分类号： C09B35/105
摘要： Diaryl pigments having an excellent stability to heat are obtained by carrying out the coupling of bis-diazotized 3,3'-dichloro-4,4'-diaminobiphenyl with acetoacetanilides in the presence of an added quantity of acetoacetanilides which are monosubstituted or disubstituted in the 3-position or 4-position of the nucleus. As a result of their good heat stability, these pigments are particularly suitable for pigmenting plastics having processing temperatures above 200.degree. C.
摘要翻译：通过在添加量的乙酰乙酰苯胺的存在下进行双重重氮化的3,3'-二氯-4,4'-二氨基联苯与乙酰乙酰苯胺的偶合获得具有优异的耐热稳定性的二芳基颜料，所述乙酰乙酰替苯胺在核的3位或4位。由于其良好的热稳定性，这些颜料特别适用于加工温度高于200℃的着色塑料。

3. 发明授权

US4607096A Azo pigments obtained by diazotizing in a dipolar aprotic organic solvent 失效
标题翻译：通过在偶极非质子有机溶剂中重氮化获得的偶氮颜料
公开(公告)号：US4607096A
公开(公告)日：1986-08-19
申请号：US439270
申请日：1982-11-04
申请人： Josef Landler , Klaus Hunger , Erhard Worfel
发明人： Josef Landler , Klaus Hunger , Erhard Worfel
IPC分类号： C09B29/20 , C09B29/00 , C09B41/00 , C09B46/00 , C09B67/00 , C09B67/20
CPC分类号： C09B41/002 , C09B29/00
摘要： Azo pigments are obtained by diazotizing a diazotizable aromatic amine without solubilizing groups in anhydrous dipolar aprotic water-miscible solvents with the stoichiometric amount or a small excess of nitrosylsulfuric acid or nitrosyl chloride, coupling the diazonium compound so obtained with a coupling component and isolating the pigment obtained in usual manner. This process is carried out in homogeneous solution and yields azo pigments the advantageous properties of which cannot be achieved by other methods, for example, the excellent purity, grain softness, narrow range of particle size distribution, excellent dispersibility in plastic materials and color lacquers, high gloss and excellent opacity in color lacquers.
摘要翻译：偶氮颜料通过重氮化可重氮化的芳族胺而不增溶基团与化学计量量或少量过量亚硝酰基亚磺酰氯或亚硝酰氯的无水偶极非质子水溶性溶剂进行重氮化，将所得重氮化合物与偶联组分偶联并分离出颜料以通常的方式获得。该方法在均匀溶液中进行，产生偶氮颜料，其有利性质不能通过其它方法实现，例如，优异的纯度，颗粒柔软度，窄的粒度分布范围，在塑料材料和彩色漆中的优异分散性，高光泽和优异的不透明度在彩色漆。

4. 发明授权

US4555568A Monoazo compounds derived from 3-nitro-4-amino-benzoates and 5-(2'-hydroxy-3'-naphthoylamino)-benzimidazolones 失效
标题翻译：衍生自3-硝基-4-氨基 - 苯甲酸酯和5-（2'-羟基-3'-萘甲酰氨基） - 苯并咪唑酮的单偶氮化合物
公开(公告)号：US4555568A
公开(公告)日：1985-11-26
申请号：US162074
申请日：1980-06-23
申请人： Klaus Hunger
发明人： Klaus Hunger
IPC分类号： C09B29/20 , C09B29/01 , C09B29/15 , D06P1/44 , D06P3/24
CPC分类号： C09B29/20
摘要： When diazotizing lower alkyl esters of 3-nitro-4-aminobenzoic acid and coupling them onto 5-(2'-hydroxy-3'-naphthoylamino)-benzimidazolone-(2) which may be substituted in 6'-position by chlorine or bromine, in 1-position by methyl or ethyl and in the benzo-nucleus by chlorine, bromine, methyl, ethyl, methoxy or ethoxy, and such as further illustrated by a representative formula ##STR1## wherein R is alkyl of 1 to 4 carbon atoms, X is hydrogen, chlorine, bromine, methyl, ethyl, methoxy or ethoxy, Y is hydrogen, methyl or ethyl, and Z is hydrogen, chlorine or bromine. Colorants are obtained which are especially useful for pigmenting plastics, spinning masses, printing inks, varnishes and paints. The dyeings obtained therewith are fast to light, weathering, solvents and migration, especially fast to overvarnishing and bleeding.
摘要翻译：当重氮化3-硝基-4-氨基苯甲酸的低级烷基酯并将其偶联到5-（2'-羟基-3'-萘甲酰基氨基） - 苯并咪唑酮 - （2）时，其可以在6'位被氯或溴取代在甲基或乙基的1-位，在苯并 - 核中由氯，溴，甲基，乙基，甲氧基或乙氧基取代，并且如通过其代表性的式I进一步说明的，其中R是1至4个碳的烷基原子，X是氢，氯，溴，甲基，乙基，甲氧基或乙氧基，Y是氢，甲基或乙基，Z是氢，氯或溴。得到着色剂，其对于着色塑料，纺丝团，印刷油墨，清漆和油漆特别有用。由此获得的染色具有耐光，耐候性，溶剂和迁移性，特别是快速渗透和渗色。

5. 发明授权

US4302388A Monoazo compounds deriving from meta-amino-benzoic acid anilides and acetoacetyl amino-benzimidazolone 失效
标题翻译：衍生自间位氨基 - 苯甲酸苯胺和乙酰乙酰氨基 - 苯并咪唑酮的单偶氮化合物
公开(公告)号：US4302388A
公开(公告)日：1981-11-24
申请号：US86125
申请日：1979-10-18
申请人： Klaus Hunger , Manfred Pesenacker
发明人： Klaus Hunger , Manfred Pesenacker
IPC分类号： C09B29/01 , C09B29/32 , C09B29/33 , D06P1/44
CPC分类号： C09B29/338 , C09B29/0003
摘要： When diazotizing a benzanilide of the formula ##STR1## wherein R is chloro, methyl or methoxy and X is carbamoyl or acetamino, or, when R is chloro or methyl, X is also methyl or chloro, and coupling it onto 5-acetoacetylaminobenzimidazolone-(2), monoazo pigments are obtained which are useful for coloring plastics and lacquers. The pigments have a very good fastness to light, solvents, over-lacquering, bleeding and a high heat resistance.
摘要翻译：当式（Ⅰa）其中R是氯时，甲基或甲氧基，X是氨基甲酰基或乙酰氨基，或当R是氯或甲基时，X也是甲基或氯，并且将其偶联到5-乙酰乙酰氨基苯并咪唑酮（ 2），获得可用于着色塑料和漆的单偶氮颜料。颜料具有非常好的耐光牢度，溶剂，过漆，渗色和高耐热性。

6. 发明授权

US4056553A 3-Amino-4-carboalkoxy-benzoic acid 4'-phenoxy-anilides 失效
标题翻译： 3-氨基-4-羰基烷氧基 - 苯甲酸4 {40-苯氧基 - 苯胺
公开(公告)号：US4056553A
公开(公告)日：1977-11-01
申请号：US686008
申请日：1976-05-13
申请人： Friedrich Wilhelm Weingarten , Klaus Hunger
发明人： Friedrich Wilhelm Weingarten , Klaus Hunger
IPC分类号： C09B29/03 , C07C67/00 , C07C231/00 , C07C231/02 , C07C237/40 , C09B29/01 , C09B29/20 , C07C103/78
CPC分类号： C09B29/0003 , C09B29/20
摘要： 3-Amino-4-lower carboalkoxy-benzoic acid-4'-phenoxy-anilides which may be halogenated in the phenoxy nucleus are obtained by reacting the corresponding 4-carboalkoxy-benzoyl chlorides having in 3-position a group capable of yielding the amino group with a 4-amino-diphenyl ether which may be halogenated in the phenyl nucleus which is not substituted by the amino group, and setting free the amino group from the group capable of yielding it. The products are diazo components for azo pigments, especially of the 2-hydroxy-3-naphthoic acid arylide type.
摘要翻译：可以在苯氧基核中被卤化的3-氨基-4-低级烷酰氧基 - 苯甲酸-4'-苯氧基苯胺，通过使具有3位的相应的4-烷氧基 - 苯甲酰氯反应得到氨基与可以在未被氨基取代的苯基核中被卤化的4-氨基 - 二苯基醚组合，并且从能够产生该氨基的基团中释放出氨基。该产品是偶氮颜料的重氮组分，特别是2-羟基-3-萘甲酸芳基酯型。

7. 发明授权

US4056522A Azo compounds deriving from 3-amino-4-lower carboalkoxy-benzoic acid-4'-phenoxy anilides and 2-hydroxy-3-naphthoic acid-4'-benzoylamino anilides 失效
标题翻译：衍生自3-氨基-4-低级羧酸 - 苯甲酸 - 4'-苯氧基脲和2-羟基-3-萘基-4-硝基苯甲酰胺的AZO化合物
公开(公告)号：US4056522A
公开(公告)日：1977-11-01
申请号：US686031
申请日：1976-05-13
申请人： Klaus Hunger , Friedrich Wilhelm Weingarten
发明人： Klaus Hunger , Friedrich Wilhelm Weingarten
IPC分类号： C08K5/00 , C08K5/22 , C08L7/00 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L67/00 , C08L77/00 , C08L101/00 , C09B23/01 , C09B29/01 , C09B29/03 , C09B29/15 , C09B29/20
CPC分类号： C09B23/0008 , C09B29/0003 , C09B29/20
摘要： Diazotation of 3-amino-4-carboalkoxy-benzoic acid (4'-phenoxy)-anilides which may be halogenated in said phenoxy nucleus and coupling on 2-hydroxy-3-naphthoic acid-(4'-benzoylamino)-anilides which may be further substituted in said anilide nucleus by halogen, lower alkyl or lower alkoxy, yields azo compounds which are valuable pigments of clear shades and high fastness to migration, light and weather.

8. 发明授权

US4041036A Water-insoluble colorants, process for preparing them and their use 失效
标题翻译：水不溶性着色剂，其制备方法及其用途
公开(公告)号：US4041036A
公开(公告)日：1977-08-09
申请号：US676925
申请日：1976-04-14
申请人： Klaus Hunger
发明人： Klaus Hunger
IPC分类号： C07D491/04 , C07D491/052 , C08K5/35 , C09B57/00 , C07D491/22
CPC分类号： C07D491/04 , C08K5/35 , C09B57/00
摘要： The condensation of barbituric acid, thiobarbituric acid or imino-barbituric acid with 2-hydroxy-3-carboxy-1-naphthaldehydes or their arylamides in a solvent at 20.degree. to 180.degree. C yields colored compounds which are useful as pigments.
摘要翻译：巴比妥酸，硫代巴比妥酸或亚氨基巴比妥酸与2-羟基-3-羧基-1-萘醛或其芳基酰胺在20至180℃的溶剂中的缩合产生可用作颜料的有色化合物。

9. 发明授权

US4476052A Azo pigment having improved hiding power and a process for its preparation 失效
标题翻译：具有改善遮盖力的偶氮颜料及其制备方法
公开(公告)号：US4476052A
公开(公告)日：1984-10-09
申请号：US357287
申请日：1982-03-11
申请人： Klaus Hunger , Joachim Ribka , Friedrich Weingarten , Wolfgang Rieper
发明人： Klaus Hunger , Joachim Ribka , Friedrich Weingarten , Wolfgang Rieper
IPC分类号： C09D7/00 , C09B29/33 , C09B67/10 , C09B67/20 , C09D7/12 , C09B29/32 , C09D3/00 , C09D11/02
CPC分类号： C09B67/0015
摘要： Process for the aftertreatment of the azo pigment of the formula ##STR1## C.I. PIGMENT ORANGE 36 wherein the crude pigment obtained after coupling is heated to temperatures from 100.degree. to 150.degree. C. in dry or wet condition in a solvent which is water-immiscible or not indefinitely water-miscible and the pigment is isolated in known manner. The pigment aftertreated in this way shows substantially improved hiding power while the same pigment prepared in the usual way has poor hiding power and can not be used in stoving lacquers.
摘要翻译：后处理式（Ⅰ）的偶氮颜料的方法颜料橙36，其中将偶联后获得的粗颜料在干燥或潮湿条件下在100℃至150℃的温度下在与水不混溶的溶剂中或不是无限期地与水混溶的溶剂中加热，并以已知方式分离颜料。以这种方式处理的颜料显示出显着改善的遮盖力，而以通常方式制备的相同颜料具有差的遮盖力并且不能用于烘烤漆中。

10. 发明授权

US4182708A Process for the preparation of azo pigments by diazotizing in a dipolar aprotic organic solvent and azo pigments obtained therefrom 失效
标题翻译：通过在偶极非质子有机溶剂和由其获得的偶氮颜料中重氮化制备偶氮颜料的方法
公开(公告)号：US4182708A
公开(公告)日：1980-01-08
申请号：US761071
申请日：1977-01-21
申请人： Josef Landler , Klaus Hunger , Erhard Worfel
发明人： Josef Landler , Klaus Hunger , Erhard Worfel
IPC分类号： C09B29/00 , C09B41/00 , C09B29/20 , C09B29/32 , C09B29/36 , C09B29/38
CPC分类号： C09B41/00 , C09B29/00
摘要： Azo pigments are obtained by diazotizing a diazotizable aromatic amine without solubilizing groups in anhydrous dipolar aprotic water-miscible solvents with the stoichiometric amount or a small excess of nitrosylsulfuric acid or nitrosyl chloride, coupling the diazonium compound so obtained with a coupling component and isolating the pigment obtained in usual manner. This process is carried out in homogeneous solution and yields azo pigments the advantageous properties of which cannot be achieved by other methods, for example, the excellent purity, grain softness, narrow range of particle size distribution, excellent dispersibility in plastic materials and color lacquers, high gloss and excellent opacity in color lacquers.
摘要翻译：偶氮颜料通过重氮化可重氮化的芳族胺而不增溶基团与化学计量量或少量过量亚硝酰基亚磺酰氯或亚硝酰氯的无水偶极非质子水溶性溶剂进行重氮化，将所得重氮化合物与偶联组分偶合并分离出颜料以通常的方式获得。该方法在均匀溶液中进行，产生偶氮颜料，其有利性质不能通过其它方法实现，例如，优异的纯度，颗粒柔软度，窄的粒度分布范围，在塑料材料和彩色漆中的优异分散性，高光泽和优异的不透明度在彩色漆。

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