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1. 发明申请

US20090286076A1 Material to be measured for stress analysis, coating liquid for forming coating film layer on the material to be measured, and stress-induced luminescent structure 审中-公开
标题翻译：要测量的材料用于应力分析，用于在待测材料上形成涂膜层的涂布液和应力诱导的发光结构
公开(公告)号：US20090286076A1
公开(公告)日：2009-11-19
申请号：US11989598
申请日：2006-08-02
申请人： Chao-Nan Xu , Yusuke Imai , Nao Terasaki , Yoshio Adachi , Hiroshi Yamada , Keiko Nishikubo
发明人： Chao-Nan Xu , Yusuke Imai , Nao Terasaki , Yoshio Adachi , Hiroshi Yamada , Keiko Nishikubo
IPC分类号： C09K11/08 , B32B27/00
CPC分类号： G01L1/247 , C09D5/22 , C09K11/02 , C09K11/7734 , G01L1/241 , G01M11/081 , Y10T428/269
摘要： In one embodiment of the present invention, on the surface of a material to be measured for stress analysis which has a stress-induced luminescent material layer formed thereon, a distortion energy is disclosed which is transmitted from a base material of a stress-induced luminescent material to the stress-induced luminescent material with high efficiency. The material to be measured for stress analysis has, on the surface thereof, a coating film layer, which emits light upon exposure to a change in distortion energy. The coating film layer is formed of a synthetic resin layer containing stress-induced luminescent particles, and the modulus of elasticity of a base material is not less than 1.0 GPa. The thickness of the coating film layer is preferably 1 μm to 500 μm.
摘要翻译：在本发明的一个实施例中，在其上形成有应力诱导的发光材料层的应力分析材料的表面上，公开了从应力诱导发光材料的基底材料传递的变形能量材料对应力致发光材料的高效率。用于应力分析的待测量材料在其表面上具有在暴露于变形能量变化时发光的涂膜层。涂膜层由含有应力诱发的发光粒子的合成树脂层形成，基材的弹性模量不小于1.0GPa。涂膜层的厚度优选为1〜500μm。

2. 发明申请

US20060124901A1 Method for preparing high brightness luminescent material and high brightness luminescent material 审中-公开
标题翻译：制备高亮度发光材料和高亮度发光材料的方法
公开(公告)号：US20060124901A1
公开(公告)日：2006-06-15
申请号：US10542999
申请日：2003-12-26
申请人： Chaonan Xu , Keiko Nishikubo , Shuxiu Zhang , Michio Obata , Hiroaki Tanno
发明人： Chaonan Xu , Keiko Nishikubo , Shuxiu Zhang , Michio Obata , Hiroaki Tanno
IPC分类号： C09K11/77
CPC分类号： C09K11/7734
摘要： A method for preparing fine particles of a high brightness luminescent material improved in crystallinity; and a high brightness luminescent material prepared by the method. In an embodiment, BaMgAl10O17:Eu (BAM) as a high brightness luminescent material is prepared by a method which comprises providing an aqueous solution containing an aluminum alcoholate and water-soluble compounds of barium, magnesium and europium, adding an acid to the aqueous solution to form an acidic solution, heating the acidic solution to ca.900° C. and conducting a calcination at the temperature for a short time, and subsequently, firing the calcined product at a temperature higher than that for the calcination, for example, 1400° C. or higher. The method allows the preparation of BAM which comprises spherical fine particles having a pure phase and being improved in crystallinity, and thus is reduced in the deterioration by heat or VUV.
摘要翻译：一种制备提高结晶度的高亮度发光材料的微粒的方法; 和通过该方法制备的高亮度发光材料。在一个实施方案中，通过包括提供含有醇铝和水的水溶液的方法制备作为高亮度发光材料的BaMgAl 10 O 17：Eu（BAM）的钡，镁和铕的可溶性化合物，向该水溶液中加入酸形成酸性溶液，将酸性溶液加热至约900℃，并在该温度下进行短时间煅烧，随后进行烧成煅烧产物的温度高于煅烧产物，例如1400℃或更高。该方法允许制备包含具有纯相的球形微粒并且结晶度提高的BAM，从而减少由热或VUV引起的劣化。

3. 发明申请

US20120269715A1 CARBON MICROPARTICLE HAVING LIGNIN AS RAW MATERIAL AND PREPARATION METHOD THEREFOR 有权
标题翻译：具有作为原料的木质素的碳微球及其制备方法
公开(公告)号：US20120269715A1
公开(公告)日：2012-10-25
申请号：US13536053
申请日：2012-06-28
申请人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
发明人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
IPC分类号： C01B31/02
CPC分类号： C01B31/02 , C01B32/05 , C01B32/348 , C01P2004/32 , C01P2004/61 , C01P2006/12 , Y10T428/2982
摘要： A method for preparing a carbon microparticle from an organic raw material having lignin as a main constituent, wherein an aqueous solution with 5% total concentration of lignin and sodium hydroxide (the proportion in mass is 1:0.5) is spray-dried to prepare a complex microparticle. This complex microparticle is heat-processed under nitrogen atmosphere at 600° C. for one hour and cooled. Thereafter, this is washed with water and further dried to prepare a hollow carbon microparticle such as those shown in FIG. 2(b). The prepared carbon microparticle is light-weight and has an equivalent specific surface area to commercially available activated charcoal.
摘要翻译：从具有木质素作为主要成分的有机原料制备碳微粒的方法，其中将木质素和氢氧化钠的总浓度为5％（质量比为1:0.5）的水溶液喷雾干燥以制备复合微粒。将该复合微粒在氮气气氛下在600℃下热处理1小时并冷却。然后，用水洗涤，进一步干燥，制备如图1所示的中空碳微粒。 2（b）。制备的碳微粒重量轻且具有与市售活性炭相当的比表面积。

4. 发明申请

US20100304141A1 CARBON MICROPARTICLE HAVING LIGNIN AS RAW MATERIAL AND PREPARATION METHOD THEREFOR 审中-公开
标题翻译：具有作为原料的木质素的碳微球及其制备方法
公开(公告)号：US20100304141A1
公开(公告)日：2010-12-02
申请号：US12745148
申请日：2008-11-18
申请人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
发明人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
IPC分类号： B32B5/00 , C01B31/02
CPC分类号： C01B32/348 , C01B32/05 , C01P2004/32 , C01P2004/61 , C01P2006/12 , Y10T428/2982
摘要： The present invention provides a method for preparing a carbon microparticle from an organic raw material having lignin as a main constituent, and a carbon microparticle obtained thereby.An aqueous solution with 5% total concentration of lignin and sodium hydroxide (the proportion in mass is 1:0.5) is spray-dried to prepare a complex microparticle. This is heat-processed under nitrogen atmosphere at 600° C. for one hour and let to cool. Thereafter, this is washed with water and further dried to prepare a hollow carbon microparticle such as those shown in FIG. 2 (b). The prepared carbon microparticle is light-weight and has an equivalent specific surface area to commercially available activated charcoal.
摘要翻译：本发明提供从具有木质素作为主要成分的有机原料制备碳微粒的方法和由此获得的碳微粒。将木质素和氢氧化钠的总浓度为5％（质量比为1:0.5）的水溶液喷雾干燥以制备复合微粒。将其在氮气气氛下在600℃下加热处理1小时并让其冷却。然后，用水洗涤，进一步干燥，制备如图1所示的中空碳微粒。 2（b）。制备的碳微粒重量轻且具有与市售活性炭相当的比表面积。

5. 发明申请

US20060091806A1 Process for producing luminant excitable with vacuum ultraviolet radiation, luminant excitable with vacuum ultraviolet radiation and luminous element including the same 审中-公开
标题翻译：用真空紫外线辐射激发的发光体的制造方法，用真空紫外线辐射激发的发光体和包含其的发光元件
公开(公告)号：US20060091806A1
公开(公告)日：2006-05-04
申请号：US10540827
申请日：2003-12-26
申请人： Chaonan Xu , Wensheng Shi , Keiko Nishikubo , Shuxiu Zhang , Michio Obata , Hiroaki Tanno
发明人： Chaonan Xu , Wensheng Shi , Keiko Nishikubo , Shuxiu Zhang , Michio Obata , Hiroaki Tanno
IPC分类号： H01J17/49
CPC分类号： C09K11/7734 , H01J1/63 , H01J2211/42
摘要： A plasma display panel having its thermal degradation and VUV deterioration reduced through enhancement of the crystallinity of luminant excitable with vacuum ultraviolet radiation to thereby attain an enhancement of luminous efficiency; and a process for producing the same. The plasma display panel comprises a pair of opposite arranged substrates and, interposed therebetween, a phosphor layer that is excited with vacuum ultraviolet radiation to thereby emit light, the phosphor layer containing spherical fine particles of a luminant excitable with vacuum ultraviolet radiation. The luminant is composed only of a matrix substance and an activator and is highly pure without having any impurity phase. Accordingly, the phosphor layer can be formed while maintaining the luminance of luminant excitable with vacuum ultraviolet radiation, so that the luminescence intensity of phosphor layer can be enhanced. Thus, there can be provided a plasma display of high luminance.
摘要翻译：通过提高可用真空紫外线辐射激发的发光体的结晶度从而降低其热劣化和VUV劣化的等离子体显示面板，从而提高发光效率; 及其制造方法。等离子体显示面板包括一对相对布置的基板，并且插入在其间具有由真空紫外线辐射激发从而发光的荧光体层，该荧光体层包含可用真空紫外线辐射激发的发光体的球形微粒。发光体仅由基质物质和活化剂组成，并且是高纯度的，没有任何杂质相。因此，可以在保持发光体的亮度同时用真空紫外线照射而形成荧光体层，从而能够提高荧光体层的发光强度。因此，可以提供高亮度的等离子体显示器。

6. 发明申请

US20050119132A1 Method and apparatus for preparing spherical crystalline fine particles 审中-公开
标题翻译：制备球状结晶微粒的方法和装置
公开(公告)号：US20050119132A1
公开(公告)日：2005-06-02
申请号：US10497149
申请日：2002-11-29
申请人： Chao-Nan Xu , Wengsheng Shi , Hiroshi Tateyama , Keiko Nishikubo
发明人： Chao-Nan Xu , Wengsheng Shi , Hiroshi Tateyama , Keiko Nishikubo
IPC分类号： B01J19/00 , B01J19/06 , C01B13/34 , C01F17/00 , C09K11/77 , F26B3/12 , F26B7/00 , H01B1/00
CPC分类号： B82Y30/00 , B01J19/06 , B01J2208/00734 , B01J2219/1946 , C01B13/34 , C01F17/0025 , C01P2002/50 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C09K11/7734 , F26B3/12 , F26B7/002
摘要： A spherical crystalline metal oxide particle is produced by introducing a metal ion-containing solution, which has been atomized, into an atmosphere that is kept at 1000° C. or more and under oxidizing condition, in order to concurrently dry and sinter the metal ion-containing solution. Moreover, As an apparatus for producing the particle, an apparatus is used, which is structured by connecting: (A) a heating apparatus for concurrently drying and sintering an atomized particulate, the heating apparatus (4) including multi channel atomizing apparatus (3) having a function of atomizing a metal ion-containing solution, and a function of sorting a size of the thus atomized particulate; and (B) an electrostatic particle collecting apparatus (5) for electrostatically collecting the particle that is thus produced by (A) and has a predetermined size. With this arrangement, it is possible to provide a method and an apparatus capable of obtaining a highly crystalline spherical particle of a metal oxide safely and easily.
摘要翻译：通过将已经雾化的含有金属离子的溶液引入保持在1000℃以上且在氧化条件下的气氛中来制造球状结晶金属氧化物颗粒，以同时干燥和烧结金属离子含有解决方案。另外，作为粒子的制造装置，使用以下装置：（A）同时干燥和烧结雾化粒子的加热装置，包括多通道雾化装置（3）的加热装置（4）具有使含有金属离子的溶液雾化的功能，以及对这样雾化的颗粒的尺寸进行分选的功能; 和（B）用于静电收集由（A）制成并具有预定尺寸的颗粒的静电颗粒收集装置（5）。通过这种布置，可以提供能够安全且容易地获得金属氧化物的高结晶球形颗粒的方法和装置。

7. 发明授权

US08986838B2 Hollow carbon microparticle and method for producing same 有权
标题翻译：中空碳微粒及其制造方法
公开(公告)号：US08986838B2
公开(公告)日：2015-03-24
申请号：US13145051
申请日：2009-12-11
申请人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
发明人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
IPC分类号： C01B31/02 , B32B5/16 , B82Y30/00 , B82Y40/00
CPC分类号： C01B31/02 , B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/15 , C01P2004/34 , C01P2004/61 , Y10T428/2984 , Y10T428/2991 , Y10T428/2993
摘要： Elastic and ultra-lightweight hollow carbon fine particles and a method for producing such hollow carbon fine particles are to be provided. In the method, fine droplets are formed from a mixed solution containing a water soluble organic substance and lithium carbonate; composite fine particles of the water soluble organic substance and the lithium carbonate are prepared by drying the fine droplets formed from the mixed solution; and the composite fine particles are decomposed at a temperature in a range of 500° C. to 900° C.
摘要翻译：要提供弹性和超轻质的中空碳细颗粒以及这种中空碳微细颗粒的制造方法。在该方法中，由含有水溶性有机物和碳酸锂的混合溶液形成细小的液滴，通过干燥由混合溶液形成的微小液滴制备水溶性有机物和碳酸锂的复合微粒; 复合微粒在500℃〜900℃的温度下分解。

8. 发明申请

US20120000766A1 METHOD FOR MANUFACTURING SCANDIUM ALUMINUM NITRIDE FILM 审中-公开
标题翻译：制造氮化铝薄膜的方法
公开(公告)号：US20120000766A1
公开(公告)日：2012-01-05
申请号：US13171806
申请日：2011-06-29
申请人： Akihiko Teshigahara , Kazuhiko Kano , Morito Akiyama , Tatsuo Tabaru , Keiko Nishikubo
发明人： Akihiko Teshigahara , Kazuhiko Kano , Morito Akiyama , Tatsuo Tabaru , Keiko Nishikubo
IPC分类号： C23C14/34
CPC分类号： C23C14/0641 , C23C14/0036 , C23C14/3414
摘要： A method for manufacturing a scandium aluminum nitride film includes: sputtering a scandium aluminum alloy target under atmosphere including nitrogen gas so that a thin film is deposited on a substrate. Since the scandium aluminum nitride film is manufactured with using one alloy target, a composition of the film is maintained even when the sputtering time is long. Further, the above method is capable of being performed by a mass production sputtering apparatus.
摘要翻译：制造氮化钪膜的方法包括：在包括氮气的气氛下溅射钪铝合金靶，使得在基板上沉积薄膜。由于使用一种合金靶来制造氮化钪膜，所以即使在溅射时间长的情况下也能够保持膜的组成。此外，上述方法能够通过大规模生产溅射装置进行。

9. 发明申请

US20110281113A1 HOLLOW CARBON MICROPARTICLE AND METHOD FOR PRODUCING SAME 有权
标题翻译：中空碳微球及其生产方法
公开(公告)号：US20110281113A1
公开(公告)日：2011-11-17
申请号：US13145051
申请日：2009-12-11
申请人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
发明人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
IPC分类号： B29B9/10 , B32B9/00
CPC分类号： C01B31/02 , B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/15 , C01P2004/34 , C01P2004/61 , Y10T428/2984 , Y10T428/2991 , Y10T428/2993
摘要： Elastic and ultra-lightweight hollow carbon fine particles and a method for producing such hollow carbon fine particles are to be provided. In the method, fine droplets are formed from a mixed solution containing a water soluble organic substance and lithium carbonate; composite fine particles of the water soluble organic substance and the lithium carbonate are prepared by drying the fine droplets formed from the mixed solution; and the composite fine particles are decomposed at a temperature in a range of 500° C. to 900° C.
摘要翻译：要提供弹性和超轻质的中空碳细颗粒以及这种中空碳微细颗粒的制造方法。在该方法中，由含有水溶性有机物和碳酸锂的混合溶液形成细小的液滴，通过干燥由混合溶液形成的微小液滴制备水溶性有机物和碳酸锂的复合微粒; 复合微粒在500℃〜900℃的温度下分解。

10. 发明授权

US09321649B2 Carbon microparticle having lignin as raw material and preparation method therefor 有权
标题翻译：具有木质素作为原料的碳微粒及其制备方法
公开(公告)号：US09321649B2
公开(公告)日：2016-04-26
申请号：US13536053
申请日：2012-06-28
申请人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
发明人： Katsumi Kamegawa , Tsuyoshi Sakaki , Kinya Sakanishi , Masaya Kodama , Keiko Nishikubo , Yoshio Adachi
IPC分类号： C01B31/02
CPC分类号： C01B31/02 , C01B32/05 , C01B32/348 , C01P2004/32 , C01P2004/61 , C01P2006/12 , Y10T428/2982
摘要： A method for preparing a carbon microparticle from an organic raw material having lignin as a main constituent, wherein an aqueous solution with 5% total concentration of lignin and sodium hydroxide (the proportion in mass is 1:0.5) is spray-dried to prepare a complex microparticle. This complex microparticle is heat-processed under nitrogen atmosphere at 600° C. for one hour and cooled. Thereafter, this is washed with water and further dried to prepare a hollow carbon microparticle such as those shown in FIG. 2 (b). The prepared carbon microparticle is light-weight and has an equivalent specific surface area to commercially available activated charcoal.
摘要翻译：从具有木质素作为主要成分的有机原料制备碳微粒的方法，其中将木质素和氢氧化钠的总浓度为5％（质量比为1:0.5）的水溶液喷雾干燥以制备复合微粒。将该复合微粒在氮气气氛下在600℃下热处理1小时并冷却。然后，用水洗涤，进一步干燥，制备如图1所示的中空碳微粒。 2（b）。制备的碳微粒重量轻且具有与市售活性炭相当的比表面积。

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