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1. 发明授权

US4946653A Process for the simultaneous classification and regulated, continuous discharge of particulate material from fluidized bed reactors 失效
标题翻译：从流化床反应器中同时分级和调节，连续排放颗粒物质的方法
公开(公告)号：US4946653A
公开(公告)日：1990-08-07
申请号：US462738
申请日：1983-02-01
申请人： Gerhard Stopp , Karl-Heinz Kreutzer , Horst Karkossa , Karl Mannes , Hans-Joachim Laakmann , Viktor Trescher
发明人： Gerhard Stopp , Karl-Heinz Kreutzer , Horst Karkossa , Karl Mannes , Hans-Joachim Laakmann , Viktor Trescher
IPC分类号： B01J2/16 , B01J4/00 , B01J8/00 , B01J8/24 , B07B4/08 , C07C37/68 , C07C39/235 , F26B3/08
CPC分类号： B01J2/16 , B01J8/003 , F26B3/08
摘要： Particulate material is discharged continuously from fluidized bed reactors by passing the material emerging at the lowest point of the fluidized bed through a zone which is narrower than the fluidized bed and in which a gas stream flows counter-current to the material, the pressure of the gas stream being above the pressure of the fluidized zone.
摘要翻译：颗粒材料通过使出现在流化床最低点处的材料通过比流化床更窄的区域并且其中气流逆流流向材料，从流化床反应器连续排出，气流高于流化区的压力。

2. 发明授权

US4447647A Process for the preparation of 2,4,6-trichloroaniline 失效
标题翻译：制备2,4,6-三氯苯胺的方法
公开(公告)号：US4447647A
公开(公告)日：1984-05-08
申请号：US453984
申请日：1982-12-28
申请人： Friedrich Werner , Karl Mannes , Viktor Trescher
发明人： Friedrich Werner , Karl Mannes , Viktor Trescher
IPC分类号： C07C209/74 , C07C67/00 , C07C209/00 , C07C211/52 , C07C85/24
CPC分类号： C07C209/74
摘要： 2,4,6-Trichloroaniline is prepared by reaction of aniline, which is optionally substituted by halogen, with a chlorinating agent in the presence of inert organic solvents and/or diluents at elevated temperatures.
摘要翻译：通过在惰性有机溶剂和/或稀释剂存在下在升高的温度下，将任选被卤素取代的苯胺与氯化剂反应来制备2,4,6-三氯苯胺。

3. 发明授权

US4341720A Process for the preparation of oxalyl chloride 失效
标题翻译：草酰氯的制备方法
公开(公告)号：US4341720A
公开(公告)日：1982-07-27
申请号：US247186
申请日：1981-03-24
申请人： Axel Vogel , Guido Steffan , Karl Mannes , Viktor Trescher
发明人： Axel Vogel , Guido Steffan , Karl Mannes , Viktor Trescher
IPC分类号： C07C55/36 , C07C51/00 , C07C51/60 , C07C67/00 , C07C57/00
CPC分类号： C07C51/60
摘要： In a process for the preparation of oxalyl chloride from an oxalic acid compound of the formula ##STR1## wherein R.sup.1 and R.sup.2 are identical or different and represent hydrogen or a lower alkyl radical,and phosphorus pentachloride in the presence of phosphorus oxychloride, the improvement wherein the reaction is carried out in the presence of an amino compound of the formula ##STR2## wherein R.sup.3 represents alkyl, aralkyl, aryl or an acyl group, optionally substituted by amino or carboxamido andR.sup.4 and R.sup.5 are identical or different and represent hydrogen or alkyl, aralkyl, or aryl, optionally substituted by amino or carboxamido, orR.sup.4 and R.sup.5 are linked in an optionally substituted carbocyclic ring with 5 to 7 ring members, which optionally contains nitrogen, sulphur and/or oxygen and is optionally substituted by alkyl, aralkyl, aryl and/or amino groups, andR.sup.3 represents hydrogen or alkyl, which can be linked with R.sup.4 to form a carbocyclic ring, aralkyl or aryl, optionally substituted by an amino or carboxamido group, or optionally forms a double bond in one of the radials R.sup.4 or R.sup.5,and the oxalyl chloride formed is distilled off during the reaction.
摘要翻译：在通式“IMAGE”的草酸化合物（其中R 1和R 2相同或不同并且代表氢或低级烷基）和五氯化磷在磷酰氯存在下制备草酰氯的方法中，该反应在下式的氨基化合物存在下进行：其中R 3表示烷基，芳烷基，芳基或酰基，任选被氨基或甲酰氨基取代，R 4和R 5相同或不同，表示氢或烷基，芳烷基或芳基，其任选被氨基或羧酰氨基取代，或R 4和R 5在任选取代的碳环中与5至7个环成员连接，所述环成员任选地含有氮，硫和/或氧并且任选地被烷基，芳烷基，芳基和/或氨基，并且R 3表示氢或烷基，其可以与R 4连接形成碳环，芳烷基或芳基，任选被上位体取代或者在一个径向R4或R5中任选形成双键，并且在反应期间蒸馏形成的草酰氯。

4. 发明授权

US4339396A Process for the preparation of naphthalenesulphonyl chloride 失效
标题翻译：萘磺酰氯的制备方法
公开(公告)号：US4339396A
公开(公告)日：1982-07-13
申请号：US163357
申请日：1980-06-26
申请人： Gunter Rauchschwalbe , Karl Mannes , Dietmar Mayer
发明人： Gunter Rauchschwalbe , Karl Mannes , Dietmar Mayer
IPC分类号： C07C309/86 , C07C67/00 , C07C301/00 , C07C303/12 , H04N11/06 , C07C143/30
CPC分类号： C07C309/00
摘要： In a process for the preparation of a naphthalenesulphonyl chloride by reacting an alkali metal salt or ammonium salt of a naphthalenesulphonic acid with thionyl chloride in the presence of a catalytically active substance the improvement wherein the reaction is carried out in the presence of an optionally substituted pyridine, tertiary aliphatic amine, secondary amidine and/or quaternary ammonium salt.
摘要翻译：在通过使萘磺酸的碱金属盐或铵盐与亚硫酰氯在催化活性物质的存在下反应制备萘磺酰氯的方法，其中反应在任选取代的吡啶存在下进行叔脂族胺，仲脒和/或季铵盐。

5. 发明授权

US4366102A Process for the preparation of chloroformic acid aryl esters 失效
标题翻译：氯甲酸芳酯的制备方法
公开(公告)号：US4366102A
公开(公告)日：1982-12-28
申请号：US261082
申请日：1981-05-06
申请人： Gunter Rauchschwalbe , Heinz U. Blank , Karl Mannes , Dietmar Mayer
发明人： Gunter Rauchschwalbe , Heinz U. Blank , Karl Mannes , Dietmar Mayer
IPC分类号： C07C69/96 , B01J27/00 , B01J31/00 , B01J31/24 , C07C68/02
CPC分类号： B01J31/0262 , B01J31/0267 , C07C68/02 , B01J2231/4288
摘要： In a process for the preparation of an aromatic chloroformic acid ester by contacting a phenol and phosgene, the improvement wherein the reaction is carried out in a homogeneous liquid phase at a temperature of 60.degree. to 180.degree. C. in the presence of organic phosphorus compound of the formulaR.sup.1 R.sup.2 R.sup.3 PR.sup.4.sub.n X.sub.nin whichR.sup.1, R.sup.2 and R.sup.3 independently of one another represent hydrogen, alkyl, alkenyl, aralkyl, aryl or halogen and two of the said radicals together with the phosphorus atom can form a 5-membered or 6-membered phosphorus-containing saturated or unsaturated heterocyclic radical,X represents OH, homopolar-bonded halogen or an inorganic or organic acid anion,R.sup.4 denotes hydrogen or alkyl or, if X denotes halogen, can also denote halogen and n denotes 0 or 1,and in which, furthermore,R.sup.4 and X together can represent oxygen or sulfur.
摘要翻译：在通过使苯酚和光气接触来制备芳族氯甲酸酯的方法中，其中反应在有机磷化合物存在下在60-180℃的温度下在均相液相中进行其中R 1，R 2和R 3彼此独立地表示氢，烷基，烯基，芳烷基，芳基或卤素，并且所述基团中的两个与磷原子一起形成式R 1 R 2 R 3 PR 4 n X n可以形成5元或6元磷 - 含有饱和或不饱和杂环基，X表示OH，单键键合的卤素或无机或有机酸阴离子，R4表示氢或烷基，或者如果X表示卤素，也可以表示卤素，n表示0或1，此外，R4和X可以一起代表氧或硫。

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