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1. 发明申请

WO2010048392A1 MULTI-LAYER MICROPOROUS MEMBRANES AND METHODS FOR MAKING AND USING SUCH MEMBRANES 审中-公开
标题翻译：多层微孔膜及其制造与使用方法
公开(公告)号：WO2010048392A1
公开(公告)日：2010-04-29
申请号：PCT/US2009/061667
申请日：2009-10-22
申请人： TONEN CHEMICAL CORPORATION , BRANT, Patrick , THURMAN, Derek, W. , ZHAO, Rui , KONO, Koichi , KOTARO, Takita
发明人： BRANT, Patrick , THURMAN, Derek, W. , ZHAO, Rui , KONO, Koichi , KOTARO, Takita
IPC分类号： B32B5/32 , B32B27/08 , B32B27/32 , B01D69/12 , B29C69/00 , H01M2/16
CPC分类号： B01D69/12 , B01D71/26 , B01D2323/225 , H01M2/166 , H01M2/1686
摘要： The invention relates to layered microporous membranes having blend regions located between interior layers or in some cases the blend regions are in surface contact with one another. The invention also relates to methods for making such a membrane and methods for using such a membrane, e.g., as a battery separator.
摘要翻译：本发明涉及具有位于内层之间的混合区域或在某些情况下共混区域彼此表面接触的层状微孔膜。本发明还涉及制造这种膜的方法以及使用这种膜的方法，例如电池隔膜。

2. 发明授权

US09492965B2 Method for producing multi-layer, microporous polyolefin membrane 有权
标题翻译：生产多层，微孔聚烯烃膜的方法
公开(公告)号：US09492965B2
公开(公告)日：2016-11-15
申请号：US12089676
申请日：2006-10-19
申请人： Kotaro Takita , Shintaro Kikuchi
发明人： Kotaro Takita , Shintaro Kikuchi
IPC分类号： B29C55/02 , B29C47/00 , B29C47/06 , B29C55/00 , B29C55/16 , B32B5/32 , B32B27/32 , B32B38/00 , H01M2/14 , H01M2/16 , B29K23/00 , B29K105/04 , B32B37/15 , B32B38/16
CPC分类号： B29C55/023 , B29C47/0021 , B29C47/06 , B29C55/005 , B29C55/16 , B29K2023/065 , B29K2023/0683 , B29K2023/12 , B29K2105/04 , B32B5/32 , B32B27/32 , B32B37/153 , B32B38/0032 , B32B2038/0028 , B32B2038/168 , B32B2305/026 , B32B2323/04 , B32B2323/10 , H01M2/145 , H01M2/1653 , H01M2/1686
摘要： A multi-layer, microporous polyolefin membrane comprising a polypropylene layer and a polyethylene resin layer and having well-balanced permeability, mechanical strength, heat shrinkage resistance, shutdown properties and meltdown properties can be obtained by (1) forming a sheet comprising a gel-like polypropylene layer containing a membrane-forming solvent or a polypropylene layer containing no membrane-forming solvent and a gel-like polyethylene resin layer containing a membrane-forming solvent, stretching the sheet at two-stage temperatures, and then removing the membrane-forming solvent, or (2) forming a gel-like polypropylene sheet containing a membrane-forming solvent or a polypropylene sheet containing no membrane-forming solvent, and a gel-like polyethylene resin sheet containing a membrane-forming solvent, stretching them at two-stage temperatures, removing the membrane-forming solvent, and then laminating the resultant microporous polypropylene membrane and the resultant microporous polyethylene membrane.
摘要翻译：包含聚丙烯层和聚乙烯树脂层并具有良好平衡的渗透性，机械强度，耐热收缩性，停止性能和熔化性能的多层微孔聚烯烃膜可以通过（1）形成包含凝胶 - 含有成膜溶剂的聚丙烯层或不含成膜溶剂的聚丙烯层和含有成膜溶剂的凝胶状聚乙烯树脂层，在两段温度下拉伸，然后除去膜形成溶剂，或（2）形成含有成膜溶剂或不含成膜溶剂的聚丙烯片的凝胶状聚丙烯片，以及含有成膜溶剂的凝胶状聚乙烯树脂片，阶段温度，去除成膜溶剂，然后层压得到的微孔聚丙烯膜和所得麦克风无孔聚乙烯膜。

3. 发明授权

US09287542B2 Multi-layer, microporous polyolefin membrane, its production method, battery separator, and battery 有权
标题翻译：多层，微孔聚烯烃膜，其生产方法，电池隔膜和电池
公开(公告)号：US09287542B2
公开(公告)日：2016-03-15
申请号：US13547850
申请日：2012-07-12
申请人： Kotaro Takita , Junko Takita , Shintaro Kikuchi
发明人： Kotaro Takita , Shintaro Kikuchi
IPC分类号： H01M2/16 , B29C55/06 , B29C55/12 , C08L23/06 , B29K23/00 , B29K105/00 , B29K105/04 , C08L23/10
CPC分类号： H01M2/1653 , B29C47/0021 , B29C47/8805 , B29C47/8845 , B29C47/90 , B29C47/906 , B29C55/065 , B29C55/12 , B29K2023/0683 , B29K2105/0061 , B29K2105/0088 , B29K2105/04 , C08L23/06 , C08L23/10 , C08L2205/02 , Y10T428/249978 , C08L2666/06
摘要： A multi-layer, microporous polyolefin membrane comprising first microporous layers constituting at least both surface layers, and at least one second microporous layer disposed between both surface layers, the first microporous layer comprising a first polyethylene resin containing 8% or more by mass of ultra-high-molecular-weight polyethylene having a weight-average molecular weight of 1×106 or more, the second microporous layer comprising a second polyethylene resin containing 7% or less by mass of the ultra-high-molecular-weight polyethylene, and having a structure in which a pore diameter distribution curve obtained by mercury intrusion porosimetry has at least two peaks, and the total thickness of the first microporous layers being 15-60% per 100% of the total thickness of the first and second microporous layers.
摘要翻译：一种多层微孔聚烯烃膜，其包括构成至少两个表面层的第一微孔层和设置在两个表面层之间的至少一个第二微孔层，所述第一微孔层包含含有8质量％或更多的超微结构的第一聚乙烯树脂重均分子量为1×10 6以上的高分子量聚乙烯，所述第二微孔层包含含有超过所述超高分子量聚乙烯7质量％以下的第二聚乙烯树脂，并且具有其中通过水银侵入孔隙率法获得的孔径分布曲线具有至少两个峰，并且第一微孔层的总厚度相对于第一和第二微孔层的总厚度的100％为15-60％。

4. 发明授权

US08778525B2 Multi-layer, microporous polyethylene membrane, battery separator formed thereby and battery 有权
标题翻译：多层，微孔聚乙烯膜，由此形成的电池隔板和电池
公开(公告)号：US08778525B2
公开(公告)日：2014-07-15
申请号：US12064350
申请日：2006-08-24
申请人： Shintaro Kikuchi , Kotaro Takita
发明人： Shintaro Kikuchi , Kotaro Takita
IPC分类号： H01M2/16
CPC分类号： H01M2/162 , B32B27/32 , H01M2/1653 , H01M10/0525 , H01M2200/10 , H01M2300/0025 , Y02E60/122 , Y02P70/54 , Y10T428/249978
摘要： A multi-layer, microporous polyethylene membrane comprising (a) a first microporous layer made of a polyethylene resin, and (b) a second microporous layer comprising a polyethylene resin, and a heat-resistant polymer having a melting point or a glass transition temperature of 170° C. or higher, the heat-resistant polymer being dispersed in the form of fine particles in the polyethylene resin, and the second microporous layer having pores containing fine particles of the heat-resistant polymer as nuclei from which the cleavage of polyethylene resin fibrils starts, the multi-layer microporous polyethylene membrane having well-balanced shutdown properties, meltdown properties, permeability, mechanical strength, heat shrinkage resistance and compression resistance.
摘要翻译：一种多层微孔聚乙烯膜，包括（a）由聚乙烯树脂制成的第一微孔层，和（b）包含聚乙烯树脂的第二微孔层和具有熔点或玻璃化转变温度的耐热聚合物为170℃以上，耐热性聚合物以聚乙烯树脂中的细颗粒的形式分散，第二微孔层具有含有耐热聚合物微粒的孔，作为核，其中聚乙烯树脂原纤维开始，多层微孔聚乙烯膜具有良好的平衡关闭性能，熔化性能，渗透性，机械强度，耐热收缩性和抗压缩性。

5. 发明申请

US20130034777A1 MICROPOROUS MEMBRANE, BATTERY SEPARATOR AND BATTERY 审中-公开
标题翻译：微波膜，电池分离器和电池
公开(公告)号：US20130034777A1
公开(公告)日：2013-02-07
申请号：US13633363
申请日：2012-10-02
申请人： Kotaro Takita , Kohtaro Kimishima , Norimitsu Kaimai
发明人： Kotaro Takita , Kohtaro Kimishima , Norimitsu Kaimai
IPC分类号： H01M2/16 , C08F110/02
CPC分类号： H01M2/1653 , B01D67/0083 , B01D71/26 , H01M2/145 , H01M10/0525 , H01M10/24 , H01M10/30 , H01M10/32 , H01M10/345
摘要： A method of manufacturing a microporous polymeric membrane including: heat-setting the microporous polymeric membrane in at least a first stage and a final stage, the first stage being upstream of the final stage and a temperature of the first stage being at least 15° C. cooler than a temperature of the final stage.
摘要翻译：一种制造微孔聚合物膜的方法，包括：在至少第一阶段和最终阶段中热固定微孔聚合物膜，第一阶段在最后阶段的上游，第一阶段的温度为至少15℃ 比最后阶段的温度更冷。

6. 发明申请

US20110236764A1 MICROPOROUS MEMBRANES AND METHODS FOR PRODUCING AND USING SUCH MEMBRANES 审中-公开
标题翻译：微孔膜和用于生产和使用这种膜的方法
公开(公告)号：US20110236764A1
公开(公告)日：2011-09-29
申请号：US13129670
申请日：2009-10-30
申请人： Kotaro Takita , Junko Takita , Yoichi Matsuda , Sadakatsu Suzuki
发明人： Kotaro Takita , Junko Takita , Yoichi Matsuda , Sadakatsu Suzuki
IPC分类号： H01M2/16 , C08J9/00 , C08F10/02
CPC分类号： H01M2/145 , B01D67/0027 , B01D71/26 , B01D2323/10 , B29C55/023 , B29K2023/06 , B29K2023/12 , B29K2105/256 , B29K2995/0097 , B29L2009/00 , B29L2031/3468 , B29L2031/755 , H01M2/1653 , H01M2/1686 , H01M10/052
摘要： The invention relates to microporous polymeric membranes suitable for use as battery separator film. The invention also relates to a method for producing such membranes, batteries containing such membranes as battery separators, methods for making such batteries, and methods for using such batteries.
摘要翻译：本发明涉及适合用作电池隔膜的微孔聚合物膜。本发明还涉及一种生产这种膜的方法，包含诸如电池隔板的膜的电池，制造这种电池的方法以及使用这种电池的方法。

7. 发明授权

US07988895B2 Production method of microporous polyethylene membrane and battery separator 有权
标题翻译：微孔聚乙烯膜和电池隔膜的生产方法
公开(公告)号：US07988895B2
公开(公告)日：2011-08-02
申请号：US12088037
申请日：2006-09-27
申请人： Kotaro Takita , Shintaro Kikuchi , Kotaro Kimishima
发明人： Kotaro Takita , Shintaro Kikuchi , Kotaro Kimishima
IPC分类号： B29C47/06
CPC分类号： H01M2/1653 , B01D67/002 , B01D69/12 , B01D71/26 , B01D2323/12 , B01D2325/22 , B01D2325/34 , B32B5/18 , B32B27/32 , H01G9/02 , H01M2/145 , H01M2/162 , H01M10/0565
摘要： A microporous polyethylene membrane having well-balanced permeability, mechanical properties, heat shrinkage resistance, compression resistance, electrolytic solution absorbability, shutdown properties and meltdown properties, with an average pore diameter changing in a thickness direction is produced by melt-blending a polyethylene resin and a membrane-forming solvent to prepare a solution A having a resin concentration of 25 to 50% by mass and a solution B having a resin concentration of 10 to 30% by mass, the resin concentration in the solution A being higher than that in the solution B, (a) simultaneously extruding the resin solutions A and B through a die, cooling the resultant extrudate to provide a gel-like sheet in which the resin solutions A and B are laminated, and removing the membrane-forming solvent from the gel-like sheet, or (b) extruding the resin solutions A and B through separate dies, removing the membrane-forming solvent from the resultant gel-like sheets A and B to form microporous polyethylene membranes A and B, and alternately laminating the microporous polyethylene membranes A and B, while easily controlling the average pore diameter distribution in the microporous polyethylene membrane in a thickness direction.
摘要翻译：通过将聚乙烯树脂和聚乙烯树脂熔融共混来制造平均孔径在厚度方向上变化的具有良好平衡的渗透性，机械性能，耐热收缩性，耐压缩性，电解溶液吸收性，停机性和熔融性的微孔聚乙烯膜，成膜溶剂以制备树脂浓度为25〜50质量％的溶液A和树脂浓度为10〜30质量％的溶液B，溶液A中的树脂浓度高于溶液B，（a）通过模具同时挤出树脂溶液A和B，冷却所得挤出物以提供其中层压有树脂溶液A和B的凝胶状片材，并从凝胶中除去成膜溶剂或（b）通过分开的模具挤出树脂溶液A和B，从得到的凝胶状片材A和B中除去成膜溶剂，形成微孔聚乙烯膜A和B，并且交替地层叠微孔聚乙烯膜A和B，同时容易地控制微孔聚乙烯膜在厚度方向上的平均孔径分布。

8. 发明授权

US07985497B2 Multi-layer, microporous polyethylene membrane, its production method, and battery separator 有权
标题翻译：多层，微孔聚乙烯膜，其制作方法和电池隔膜
公开(公告)号：US07985497B2
公开(公告)日：2011-07-26
申请号：US12088493
申请日：2006-09-27
申请人： Kotaro Takita , Shintaro Kikuchi
发明人： Kotaro Takita , Shintaro Kikuchi
IPC分类号： H01M2/16
CPC分类号： H01M2/1653 , B01D67/002 , B01D69/02 , B01D69/12 , B01D71/26 , B01D2323/08 , B01D2325/023 , B01D2325/22 , B01D2325/24 , B32B5/32 , B32B27/32 , H01G9/02 , H01M2/145 , H01M2/1686 , H01M10/0565 , H01M2300/0094 , Y10T428/249981
摘要： A multi-layer, microporous polyethylene membrane having at least two layers, which comprises (a) a microporous polyethylene resin layer A comprising high-density polyethylene A having 0.2 or more terminal vinyl groups per 10,000 carbon atoms when measured by infrared spectroscopy, and (b) a microporous polyethylene resin layer B comprising high-density polyethylene B having less than 0.2 terminal vinyl groups per 10,000 carbon atoms when measured by infrared spectroscopy, has well-balanced permeability, mechanical strength, heat shrinkage resistance, shutdown properties, meltdown properties and oxidation resistance.
摘要翻译：具有至少两层的多层微孔聚乙烯膜，其包含：（a）当通过红外光谱测定时，包含每10,000个碳原子具有0.2个或更多个末端乙烯基的高密度聚乙烯A的微孔聚乙烯树脂层A和（ b）当通过红外光谱法测量时，包含每10,000个碳原子具有小于0.2个末端乙烯基的高密度聚乙烯B的微孔聚乙烯树脂层B具有良好平衡的渗透性，机械强度，耐热收缩性，停机性能，熔化性能和耐氧化性。

9. 发明申请

US20110089602A1 Extruder And Process For Preparing A Mixture Of Polymer And Diluent 有权
标题翻译：用于制备聚合物和稀释剂混合物的挤出机和方法
公开(公告)号：US20110089602A1
公开(公告)日：2011-04-21
申请号：US12681695
申请日：2008-10-20
申请人： Tetsuro Nogata , Soichiro Yamaguchi , Norimitsu Kaimai , Kotaro Takita , Takita Junko
发明人： Tetsuro Nogata , Soichiro Yamaguchi , Norimitsu Kaimai , Kotaro Takita , Takita Junko
IPC分类号： B29C47/00 , B29C47/40
CPC分类号： B29C47/0825 , B29B7/482 , B29B7/60 , B29C47/0021 , B29C47/38 , B29C47/402 , B29C47/60
摘要： The invention relates to a twin screw extruder for preparing a polymeric solution. The extruder includes an elongated housing having an inlet end, an outlet end, an extruder shaft length L and a pair of interconnecting bores disposed within the housing, a pair of elongated extruder shafts, each having an axis of rotation, the pair of elongated extruder shafts disposed within the pair of interconnecting bores and drivable in at least one direction of rotation, a plurality of extruder screw segments positioned along the pair of elongated extruder shafts in a fixed angular relationship therewith, the plurality of extruder screw segments selected to form multiple extruder stages. The invention also relates to a process for extruding a mixture of polymer and diluent.
摘要翻译：本发明涉及一种用于制备聚合物溶液的双螺杆挤出机。挤出机包括细长壳体，其具有入口端，出口端，挤出机轴长度L和布置在壳体内的一对互连孔，每对具有旋转轴线的一对细长挤出机轴，该对细长挤出机设置在所述一对互连孔内并且可沿至少一个旋转方向驱动的轴;多个挤出机螺杆段，沿着所述一对细长挤出机轴以固定的角度关系定位，所述多个挤出机螺杆段被选择以形成多个挤出机阶段本发明还涉及挤出聚合物和稀释剂的混合物的方法。

10. 发明申请

US20100021808A1 MULTI-LAYER, MICROPOROUS POLYOLEFIN MEMBRANE, ITS PRODUCTION METHOD, BATTERY SEPARATOR, AND BATTERY 有权
标题翻译：多层，微孔聚烯烃薄膜，其生产方法，电池分离器和电池
公开(公告)号：US20100021808A1
公开(公告)日：2010-01-28
申请号：US12296242
申请日：2007-04-09
申请人： Kotaro Takita , Shintaro Kikuchi
发明人： Kotaro Takita , Shintaro Kikuchi
IPC分类号： H01M2/16 , B29C47/06 , B32B37/14 , B32B3/26
CPC分类号： H01M2/1653 , B29C47/0021 , B29C47/8805 , B29C47/8845 , B29C47/90 , B29C47/906 , B29C55/065 , B29C55/12 , B29K2023/0683 , B29K2105/0061 , B29K2105/0088 , B29K2105/04 , C08L23/06 , C08L23/10 , C08L2205/02 , Y10T428/249978 , C08L2666/06
摘要： A multi-layer, microporous polyolefin membrane comprising first microporous layers constituting at least both surface layers, and at least one second microporous layer disposed between both surface layers, the first microporous layer comprising a first polyethylene resin containing 8% or more by mass of ultra-high-molecular-weight polyethylene having a weight-average molecular weight of 1×106 or more, the second microporous layer comprising a second polyethylene resin containing 7% or less by mass of the ultra-high-molecular-weight polyethylene, and having a structure in which a pore diameter distribution curve obtained by mercury intrusion porosimetry has at least two peaks, and the total thickness of the first microporous layers being 15-60% per 100% of the total thickness of the first and second microporous layers.
摘要翻译：一种多层微孔聚烯烃膜，其包括构成至少两个表面层的第一微孔层和设置在两个表面层之间的至少一个第二微孔层，所述第一微孔层包含含有8质量％或更多的超微结构的第一聚乙烯树脂重均分子量为1×10 6以上的高分子量聚乙烯，第二微孔层包含含有7质量％以下的超高分子量聚乙烯的第二聚乙烯树脂，具有结构其中通过水银侵入孔隙率法获得的孔径分布曲线具有至少两个峰，并且第一微孔层的总厚度相对于第一和第二微孔层的总厚度的100％为15-60％。

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