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1. 发明授权

US09108188B2 Selective hydrogenation catalyst and methods of making and using same 有权
标题翻译：选择性氢化催化剂及其制备和使用方法
公开(公告)号：US09108188B2
公开(公告)日：2015-08-18
申请号：US13414544
申请日：2012-03-07
申请人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Stephen L. Kelly
发明人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Stephen L. Kelly
IPC分类号： B01J21/04 , B01J21/06 , B01J21/08 , B01J23/00 , B01J23/38 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/755 , B01J27/10 , B01J27/128 , B01J27/13 , C01B13/00 , C01B33/12 , C01F7/02 , C01G23/047 , B01J23/50 , B01J37/18 , B01J37/24 , B01J35/10 , B01J37/00 , C07C7/167 , C07C5/08 , C07C5/09
CPC分类号： B01J23/50 , B01J21/04 , B01J23/005 , B01J23/44 , B01J27/125 , B01J35/0006 , B01J35/08 , B01J35/1009 , B01J35/1014 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/1066 , B01J35/1071 , B01J35/1076 , B01J35/109 , B01J37/0009 , B01J37/0018 , B01J37/0221 , B01J37/08 , B01J37/082 , B01J37/18 , B01J37/24 , C07C5/03 , C07C5/08 , C07C5/09 , C07C7/167 , C07C2521/04 , C07C2527/13 , Y02P20/52 , C07C11/04 , C07C11/06
摘要： A composition comprising an extruded inorganic support comprising an oxide of a metal or metalloid, and at least one catalytically active metal, wherein the extruded inorganic support has pores, a total pore volume, and a pore size distribution, wherein the pore size distribution displays at least two peaks of pore diameters, each peak having a maximum, wherein a first peak has a first maximum of pore diameters of equal to or greater than about 120 nm and a second peak has a second maximum of pore diameters of less than about 120 nm, and wherein greater than or equal to about 5% of a total pore volume of the extruded inorganic support is contained within the first peak of pore diameters.
摘要翻译：一种组合物，其包含包含金属或准金属的氧化物的挤出无机载体和至少一种催化活性金属，其中所述挤出的无机载体具有孔，总孔体积和孔径分布，其中孔径分布显示在孔径的至少两个峰值，每个峰值具有最大值，其中第一峰值具有等于或大于约120nm的孔径的第一最大值，并且第二峰值具有小于约120nm的孔径的第二最大值，并且其中挤出的无机载体的总孔体积的大于或等于约5％包含在孔直径的第一峰内。

2. 发明授权

US08119203B2 Method of treating a surface to protect the same 有权
标题翻译：处理表面以保护其表面的方法
公开(公告)号：US08119203B2
公开(公告)日：2012-02-21
申请号：US11420904
申请日：2006-05-30
申请人： Robert L. Hise , Geoffrey E. Scanlon , Joseph Bergmeister, III , Daniel B. Knorr
发明人： Robert L. Hise , Geoffrey E. Scanlon , Joseph Bergmeister, III , Daniel B. Knorr
IPC分类号： C10G35/00 , B05D3/00 , B05D3/02
CPC分类号： C10G35/04 , C10G75/00 , C23C4/18 , C23C26/00 , C23C28/021 , C23C28/023
摘要： A method of treating a substrate by applying a layer of at least one metal to the substrate to form an applied metal layer on the substrate and followed by curing of the applied metal layer at sub-atmospheric pressure to form a metal protective layer. A method of treating a substrate by applying a layer of at least one metal to a substrate of an unassembled component of a reactor system to form an applied metal layer on the substrate of the unassembled component and curing the applied metal layer on the substrate of the unassembled component to form a metal protective layer. A method of treating a substrate by applying a layer of at least one metal to the substrate to form an applied metal layer, curing the applied metal layer at a first temperature and pressure for a first period of time, and curing the applied metal layer at a second temperature and pressure for a second period of time, wherein the curing forms a metal protective layer.
摘要翻译：一种通过将至少一种金属层施加到衬底上以在衬底上形成施加的金属层并随后在亚大气压下固化所施加的金属层以形成金属保护层来处理衬底的方法。一种通过将至少一种金属层施加到反应器系统的未组装组分的衬底上来处理衬底的方法，以在未组装的组件的衬底上形成施加的金属层，并将所施加的金属层固化在所述衬底上未组装的组分形成金属保护层。一种通过将至少一种金属层施加到基板上以形成施加的金属层来处理基板的方法，在第一温度和压力下固化所施加的金属层一段时间，并且将施加的金属层固化在第二温度和压力持续第二时间段，其中所述固化形成金属保护层。

3. 发明授权

US07417007B2 Selective hydrogenation catalyst and methods of making and using same 有权
标题翻译：选择性氢化催化剂及其制备和使用方法
公开(公告)号：US07417007B2
公开(公告)日：2008-08-26
申请号：US11458937
申请日：2006-07-20
申请人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
发明人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
IPC分类号： B01J27/02 , B01J27/045 , B01J27/10
CPC分类号： B01J27/13 , B01J21/04 , B01J23/44 , B01J23/50 , B01J27/125 , B01J35/1009 , B01J37/0205 , B01J37/0207 , B01J37/24 , C10G45/40 , C10G2300/70
摘要： A method for producing a selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon formed by the method comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A method of selectively hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting the highly unsaturated hydrocarbon with a selective hydrogenation catalyst composition produced by contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition.
摘要翻译：一种制备用于将高度不饱和烃氢化成不饱和烃的选择性氢化催化剂的方法，包括使无机催化剂载体与含氯化合物接触以形成氯化催化剂载体并向氯化催化剂载体中加入钯以形成负载钯组成。一种用于将高度不饱和烃氢化成不饱和烃的选择性氢化催化剂，该方法包括使无机催化剂载体与含氯化合物接触以形成氯化催化剂载体，并向氯化催化剂载体中加入钯以形成负载钯组成。包括将高度不饱和烃选择性氢化为不饱和烃的方法，包括使高度不饱和烃与选择性氢化催化剂组合物接触，所述选择性氢化催化剂组合物通过使无机催化剂载体与含氯化合物接触而形成氯化催化剂载体并向氯化物中加入钯催化剂载体以形成负载型钯组合物。

4. 发明申请

US20130237729A1 Selective Hydrogenation Catalyst and Methods of Making and Using Same 有权
公开(公告)号：US20130237729A1
公开(公告)日：2013-09-12
申请号：US13414544
申请日：2012-03-07
申请人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Stephen L. Kelly
发明人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Stephen L. Kelly
IPC分类号： C07C5/05 , B01J21/08 , B01J21/06 , B01J21/04 , B01J21/02 , B01J27/08 , B01J23/00 , B01J27/10 , B01J37/24 , C01B33/12 , C01G23/047 , C01F7/02 , C01B13/00 , B32B7/02 , B01J35/10
CPC分类号： B01J23/50 , B01J21/04 , B01J23/005 , B01J23/44 , B01J27/125 , B01J35/0006 , B01J35/08 , B01J35/1009 , B01J35/1014 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/1066 , B01J35/1071 , B01J35/1076 , B01J35/109 , B01J37/0009 , B01J37/0018 , B01J37/0221 , B01J37/08 , B01J37/082 , B01J37/18 , B01J37/24 , C07C5/03 , C07C5/08 , C07C5/09 , C07C7/167 , C07C2521/04 , C07C2527/13 , Y02P20/52 , C07C11/04 , C07C11/06
摘要： A composition comprising an extruded inorganic support comprising an oxide of a metal or metalloid, and at least one catalytically active metal, wherein the extruded inorganic support has pores, a total pore volume, and a pore size distribution, wherein the pore size distribution displays at least two peaks of pore diameters, each peak having a maximum, wherein a first peak has a first maximum of pore diameters of equal to or greater than about 120 nm and a second peak has a second maximum of pore diameters of less than about 120 nm, and wherein greater than or equal to about 5% of a total pore volume of the extruded inorganic support is contained within the first peak of pore diameters.

5. 发明申请

US20130014780A1 Methods of Removing a Protective Layer 有权
标题翻译：去除保护层的方法
公开(公告)号：US20130014780A1
公开(公告)日：2013-01-17
申请号：US13180163
申请日：2011-07-11
申请人： Dennis L. HOLTERMANN , Tin-Tack Peter CHEUNG , Christopher D. BLESSING , Lawrence E. HUFF , Joseph BERGMEISTER, III , Robert L. HISE , Geoffrey E. SCANLON , David W. Dockter
发明人： Dennis L. HOLTERMANN , Tin-Tack Peter CHEUNG , Christopher D. BLESSING , Lawrence E. HUFF , Joseph BERGMEISTER, III , Robert L. HISE , Geoffrey E. SCANLON , David W. Dockter
IPC分类号： C23G1/00 , C23G1/02
CPC分类号： C23G5/024 , C10G35/065 , C10G35/09 , C23F1/12 , C23F1/44 , C23G1/02
摘要： A method of removing a metal protective layer from a surface of a reactor component comprising treating the metal protective layer with one or more chemical removal agents to remove at least a portion of the metal protective layer from the reactor component. A method of removing a metal protective layer from a surface of a reactor component comprising treating the metal protective layer to remove the metal protective layer from the reactor component, and determining a thickness of the reactor component following treatment.
摘要翻译：从反应器组件的表面去除金属保护层的方法，包括用一种或多种化学去除剂处理金属保护层以从反应器组分中去除金属保护层的至少一部分。从反应器组件的表面除去金属保护层的方法，包括处理金属保护层以从反应器组分除去金属保护层，以及确定处理后反应器部件的厚度。

6. 发明申请

US20080300436A1 Selective hydrogenation catalyst and methods of making and using same 有权
公开(公告)号：US20080300436A1
公开(公告)日：2008-12-04
申请号：US12191899
申请日：2008-08-14
申请人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
发明人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
IPC分类号： C07C5/08
CPC分类号： B01J27/13 , B01J21/04 , B01J23/44 , B01J23/50 , B01J27/125 , B01J35/1009 , B01J37/0205 , B01J37/0207 , B01J37/24 , C10G45/40 , C10G2300/70
摘要： A method for producing a selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon formed by the method comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A method of selectively hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting the highly unsaturated hydrocarbon with a selective hydrogenation catalyst composition produced by contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition.

7. 发明授权

US08729326B2 Selective hydrogenation catalyst and methods of making and using same 有权
标题翻译：选择性氢化催化剂及其制备和使用方法
公开(公告)号：US08729326B2
公开(公告)日：2014-05-20
申请号：US12191899
申请日：2008-08-14
申请人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
发明人： Tin-Tack Peter Cheung , Joseph Bergmeister, III , Zongxuan Hong
IPC分类号： C07C7/163 , B01J27/13
CPC分类号： B01J27/13 , B01J21/04 , B01J23/44 , B01J23/50 , B01J27/125 , B01J35/1009 , B01J37/0205 , B01J37/0207 , B01J37/24 , C10G45/40 , C10G2300/70
摘要： A method for producing a selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A selective hydrogenation catalyst for hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon formed by the method comprising contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition. A method of selectively hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon comprising contacting the highly unsaturated hydrocarbon with a selective hydrogenation catalyst composition produced by contacting an inorganic catalyst support with a chlorine-containing compound to form a chlorided catalyst support and adding palladium to the chlorided catalyst support to form a supported-palladium composition.
摘要翻译：一种制备用于将高度不饱和烃氢化成不饱和烃的选择性氢化催化剂的方法，包括使无机催化剂载体与含氯化合物接触以形成氯化催化剂载体并向氯化催化剂载体中加入钯以形成负载钯组成。一种用于将高度不饱和烃氢化成不饱和烃的选择性氢化催化剂，该方法包括使无机催化剂载体与含氯化合物接触以形成氯化催化剂载体，并向氯化催化剂载体中加入钯以形成负载钯组成。包括将高度不饱和烃选择性氢化为不饱和烃的方法，包括使高度不饱和烃与选择性氢化催化剂组合物接触，所述选择性氢化催化剂组合物通过使无机催化剂载体与含氯化合物接触而形成氯化催化剂载体并向氯化物中加入钯催化剂载体以形成负载钯组合物。

8. 发明授权

US08535448B2 Methods of removing a protective layer 有权
标题翻译：去除保护层的方法
公开(公告)号：US08535448B2
公开(公告)日：2013-09-17
申请号：US13180163
申请日：2011-07-11
申请人： Dennis L. Holtermann , Tin-Tack Peter Cheung , Christopher D. Blessing , Lawrence E. Huff , Joseph Bergmeister, III , Robert L. Hise , Geoffrey E. Scanlon , David W. Dockter
发明人： Dennis L. Holtermann , Tin-Tack Peter Cheung , Christopher D. Blessing , Lawrence E. Huff , Joseph Bergmeister, III , Robert L. Hise , Geoffrey E. Scanlon , David W. Dockter
IPC分类号： B08B9/00 , C23G1/02 , C23G1/00
CPC分类号： C23G5/024 , C10G35/065 , C10G35/09 , C23F1/12 , C23F1/44 , C23G1/02
摘要： A method of removing a metal protective layer from a surface of a reactor component comprising treating the metal protective layer with one or more chemical removal agents to remove at least a portion of the metal protective layer from the reactor component. A method of removing a metal protective layer from a surface of a reactor component comprising treating the metal protective layer to remove the metal protective layer from the reactor component, and determining a thickness of the reactor component following treatment.
摘要翻译：从反应器组件的表面去除金属保护层的方法，包括用一种或多种化学去除剂处理金属保护层以从反应器组分中去除金属保护层的至少一部分。从反应器组件的表面除去金属保护层的方法，包括处理金属保护层以从反应器组分除去金属保护层，以及确定处理后反应器部件的厚度。

9. 发明授权

US07199076B2 Methods of making and using a selective hydrogenation catalyst 有权
标题翻译：制备和使用选择性氢化催化剂的方法
公开(公告)号：US07199076B2
公开(公告)日：2007-04-03
申请号：US10741800
申请日：2003-12-19
申请人： Joseph Bergmeister, III , Tin-Tack Peter Cheung
发明人： Joseph Bergmeister, III , Tin-Tack Peter Cheung
IPC分类号： B01J27/06 , B01J27/128 , B01J27/13 , B01J27/138
CPC分类号： C07C5/05 , C07C5/09 , C07C2523/66
摘要： In an embodiment, a method of hydrogenating a highly unsaturated hydrocarbon to an unsaturated hydrocarbon includes contacting the highly unsaturated hydrocarbon with a catalyst in the presence of hydrogen. The catalyst comprises palladium and an inorganic support having a surface area of from about 4.5 to about 20 m2/g, or alternatively 5 to 14.5 m2/g. The inorganic support may comprise α-alumina treated with a fluoride source. The palladium may be primarily disposed near the surface of the support. In addition, the catalyst may comprise silver distributed throughout the support. In another embodiment, a method of making the foregoing selective hydrogenation catalyst includes contacting a fluorine-containing compound with an inorganic support, heating the support, and adding palladium to the inorganic support. After adding palladium to the support, the support can then be heated again, followed by adding silver to and then heating the support once again.
摘要翻译：在一个实施方案中，将高度不饱和烃氢化成不饱和烃的方法包括在氢的存在下使高度不饱和烃与催化剂接触。催化剂包括钯和无机载体，其表面积为约4.5至约20m 2 / g，或者5至14.5m 2 / g。无机载体可以包括用氟化物源处理的α-氧化铝。钯可以主要设置在支撑体的表面附近。此外，催化剂可以包含分布在整个载体上的银。在另一个实施方案中，制备上述选择性氢化催化剂的方法包括使含氟化合物与无机载体接触，加热载体，并向无机载体中加入钯。向载体中加入钯后，再次加热载体，然后再加入银，然后再次加热载体。

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