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1. 发明授权

US07157068B2 Varied morphology carbon nanotubes and method for their manufacture 有权
标题翻译：不同形态的碳纳米管及其制造方法
公开(公告)号：US07157068B2
公开(公告)日：2007-01-02
申请号：US10151382
申请日：2002-05-20
申请人： Wenzhi Li , Jian Guo Wen , Zhi Feng Ren
发明人： Wenzhi Li , Jian Guo Wen , Zhi Feng Ren
IPC分类号： D01F9/12
CPC分类号： B01J37/036 , B01J23/745 , B01J23/75 , B82Y30/00 , B82Y40/00 , C01B32/162 , D01F9/127 , Y10S977/843
摘要： The present invention describes the preparation of carbon nanotubes of varied morphology, catalyst materials for their synthesis. The present invention also describes reactor apparatus and methods of optimizing and controlling process parameters for the manufacture carbon nanotubes with pre-determined morphologies in relatively high purity and in high yields. In particular, the present invention provides methods for the preparation of non-aligned carbon nanotubes with controllable morphologies, catalyst materials and methods for their manufacture.
摘要翻译：本发明描述了不同形态的碳纳米管的制备，用于它们的合成的催化剂材料。本发明还描述了反应器装置和优化和控制具有相对高纯度和高收率的具有预定形态的制造碳纳米管的工艺参数的方法。特别地，本发明提供了制备具有可控形态的非对准碳纳米管的方法，催化剂材料及其制造方法。

2. 发明授权

US5872079A Superconductor and precursor therefor, their preparation and use of superconductor 失效
标题翻译：超导体及其前体，其超导体的制备和使用
公开(公告)号：US5872079A
公开(公告)日：1999-02-16
申请号：US762211
申请日：1996-12-06
申请人： Masaru Nakamura , Yasuji Yamada , Jian-Guo Wen , Yuh Shiohara , Shoji Tanaka
发明人： Masaru Nakamura , Yasuji Yamada , Jian-Guo Wen , Yuh Shiohara , Shoji Tanaka
IPC分类号： C04B35/45 , C01G1/00 , C01G3/00 , H01B12/02 , H01B13/00 , H01L39/12 , H01L39/24 , H01B12/00 , C04B35/50 , C04B35/622
CPC分类号： H01L39/126 , Y10S505/78 , Y10S505/819
摘要： A superconductor comprising a compound of the formula (II):R.sub.1+x Ba.sub.2-x Cu.sub.3 O.sub.7-y1 (II)wherein not less than 40% of a crystal of the superconductor shows phase separation, and at (temperature, magnetic field) of (77�K!, O�T!) and (77�K!, 4�T!), a critical current density is not less than 10,000 A/cm.sup.2, which is obtained by heating a precursor which is a solid solution of the formula (I):R.sub.1+x Ba.sub.2-x Cu.sub.3 O.sub.7-y (I)wherein not more than 10% of a crystal of the solid solution shows phase separation, so that phase separation is formed in the crystals at a phase separation temperature, and introducing oxygen; and a superconductor comprising a compound of the formula (II):R.sub.1+x Ba.sub.2-x Cu.sub.3 O.sub.7-y1 (II)wherein not more than 10% of a crystal of the superconductor shows phase separation, and in a magnetic field of not less than 1�T! at a constant temperature of 77�K!, a critical current density is less than 10,000 A/cm.sup.2, which is obtained by introducing oxygen into the precursor (I) at a temperature less than the lower limit of the phase separation temperature. According to the method of the present invention, a superconductor having a high Jc or having different properties with respect to Jc, which is unobtainable by the conventional production method, can be obtained using the conventional materials.
摘要翻译：包含式（II）化合物的超导体：R1 + xBa2-xCu3O7-y1（II）其中不低于40％的超导体的晶体显示相分离，并且在（77℃）的（温度， K]，O [T]）和（77 [K]，4 [T]），临界电流密度不小于10,000A / cm 2，这是通过加热作为式 I）：R1 + xBa2-xCu3O7-y（I）其中不超过10％的固溶体晶体显示相分离，从而在相分离温度下在晶体中形成相分离并引入氧; 以及包含式（II）的化合物的超导体：R1 + xBa2-xCu3O7-y1（II）其中不超过10％的超导体的晶体显示相分离，并且在不小于1 [ T]在77 [K]的恒定温度下，临界电流密度小于10,000A / cm 2，其通过在低于相分离温度的下限的温度下将氧引入前体（I）而获得。根据本发明的方法，可以使用常规材料获得具有高Jc或具有相对于Jc的不同性能的超导体，其通过常规制备方法是不可获得的。

3. 发明授权

US06541789B1 High temperature superconductor Josephson junction element and manufacturing method for the same 失效
标题翻译：高温超导体约瑟夫逊结元件及其制造方法相同
公开(公告)号：US06541789B1
公开(公告)日：2003-04-01
申请号：US09385710
申请日：1999-08-30
申请人： Tetsuro Sato , Jian-Guo Wen , Naoki Koshizuka , Shoji Tanaka
发明人： Tetsuro Sato , Jian-Guo Wen , Naoki Koshizuka , Shoji Tanaka
IPC分类号： H01L3922
CPC分类号： H01L39/2496 , H01L39/225
摘要： In a method of manufacturing a Josephson junction, a first superconductive layer is formed on a substrate. An insulating film is formed on the first superconductive layer. The insulating film is etched to have an inclination portion. The first superconductive layer is etched using the etched insulating film as a mask, to have an inclination portion. A barrier layer is formed on a surface of the inclination portion of the first superconductive layer. A second superconductive layer is formed on the barrier layer and the inclination portion of the insulating layer.
摘要翻译：在制造约瑟夫逊结的方法中，在基板上形成第一超导层。绝缘膜形成在第一超导层上。绝缘膜被蚀刻以具有倾斜部分。使用蚀刻绝缘膜作为掩模蚀刻第一超导层，以具有倾斜部分。在第一超导层的倾斜部分的表面上形成阻挡层。在隔离层和绝缘层的倾斜部分上形成第二超导层。

4. 发明授权

US6011981A Oxide superconductor multilayered film and oxide superconductor josephson device 失效
标题翻译：氧化物超导体多层膜和氧化物超导体约瑟夫森装置
公开(公告)号：US6011981A
公开(公告)日：2000-01-04
申请号：US814172
申请日：1997-03-10
申请人： Gustavo Alvarez , Furen Wang , Jian-Guo Wen , Naoki Koshizuka , Youichi Enomoto , Tadashi Utagawa , Shoji Tanaka
发明人： Gustavo Alvarez , Furen Wang , Jian-Guo Wen , Naoki Koshizuka , Youichi Enomoto , Tadashi Utagawa , Shoji Tanaka
IPC分类号： H01L39/12 , H01L39/22
CPC分类号： H01L39/128 , H01L39/225 , Y10S505/702
摘要： An oxide superconducting multilayered thin film structure having a laminated layer structure of oxide superconductor thin film layers and non-superconductor thin film layers constituted by a combination of material groups for making strain free interfaces among both thin film layers. For example, an oxide superconductor multilayered film constituted by a laminated layer structure where thin films of an oxide superconductor represented by the chemical formula of M'Ba.sub.2 Cu.sub.3 O.sub.7-.delta. (M'; a rare earth element of Nd, Sm, Eu or the like or an alloy of these, .delta.; oxygen depletion amount) and thin films of an oxide represented by the chemical formula of M*Ba.sub.2 Cu.sub.3 O.sub.7-.delta. (M*; an element of Pr, Sc or the like or an alloy of these, .delta.; oxygen depletion amount) are alternately stacked. The oxide thin films are thin films fabricated by a pulsed laser deposition process or a sputtering process. A Josephson device can be provided by using the multilayered film.
摘要翻译：一种氧化物超导多层薄膜结构，其具有由氧化物超导体薄膜层和非超导体薄膜层组成的层叠层结构，所述非超导薄膜层由两个薄膜层之间形成无应力界面的材料组合组成。例如，由M'Ba2Cu3O7-δ（M'，Nd，Sm，Eu等的稀土元素表示的氧化物超导体的薄膜的层叠层结构构成的氧化物超导体多层膜，这些的合金，δ;氧耗尽量）和由化学式M * Ba2Cu3O7-δ（M *; Pr，Sc等元素或它们的合金，δ;氧气）表示的氧化物薄膜耗尽量）交替堆叠。氧化物薄膜是通过脉冲激光沉积工艺或溅射工艺制造的薄膜。可以通过使用多层膜来提供约瑟夫森装置。

5. 发明授权

US5883051A High Tc superconducting Josephson junction element 失效
标题翻译：高Tc超导约瑟夫逊结元件
公开(公告)号：US5883051A
公开(公告)日：1999-03-16
申请号：US735117
申请日：1996-10-22
申请人： Yoshihiro Ishimaru , Jian-Guo Wen , Kunihiko Hayashi , Youichi Enomoto , Naoki Koshizuka , Shoji Tanaka
发明人： Yoshihiro Ishimaru , Jian-Guo Wen , Kunihiko Hayashi , Youichi Enomoto , Naoki Koshizuka , Shoji Tanaka
IPC分类号： H01L39/22 , H01L39/24
CPC分类号： H01L39/225 , Y10S428/93 , Y10S505/702
摘要： A superconducting Josephson junction element including a first, a-axis oriented, superconductive metal oxide crystal grain having a first area of a {001} plane, and a second, c-axis oriented, superconductive metal oxide crystal grain having a second area of a {110} plane, wherein the first and second crystal grains are in contact with each other at the first and second areas to form a grain boundary therebetween.
摘要翻译：一种超导约瑟夫逊结元件，其包括具有第一面积{001}面的第一，a轴取向的超导金属氧化物晶粒和第二c轴取向的超导金属氧化物晶粒，其具有第二面积 {110}面，其中第一和第二晶粒在第一和第二区域彼此接触以在它们之间形成晶界。

6. 发明授权

US07442414B2 Methods for producing reinforced carbon nanotubes 失效
标题翻译：生产增强碳纳米管的方法
公开(公告)号：US07442414B2
公开(公告)日：2008-10-28
申请号：US10987257
申请日：2004-11-12
申请人： Zhifen Ren , Jian Guo Wen , Jing Y. Lao , Wenzhi Li
发明人： Zhifen Ren , Jian Guo Wen , Jing Y. Lao , Wenzhi Li
IPC分类号： C23C16/22
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/168 , C01B2202/06 , C04B35/62847 , C04B35/6286 , C04B35/62863 , C04B35/62892 , C04B35/62897 , C04B2235/5268 , C04B2235/5288 , D01F9/12 , D01F11/12 , Y10S977/752 , Y10T428/25 , Y10T428/2913 , Y10T428/2918 , Y10T428/292 , Y10T428/2975 , Y10T428/2982 , Y10T428/30
摘要： Methods for producing reinforced carbon nanotubes having a plurality of microparticulate carbide or oxide materials formed substantially on the surface of such reinforced carbon nanotubes composite materials are disclosed. In particular, the present invention provides reinforced carbon nanotubes (CNTs) having a plurality of boron carbide nanolumps formed substantially on a surface of the reinforced CNTs that provide a reinforcing effect on CNTs, enabling their use as effective reinforcing fillers for matrix materials to give high-strength composites. The present invention also provides methods for producing such carbide reinforced CNTs.
摘要翻译：公开了生产具有多个基本上形成在这种增强碳纳米管复合材料的表面上的微粒碳化物或氧化物材料的增强碳纳米管的方法。特别地，本发明提供了增强的碳纳米管（CNT），其具有基本上形成在增强CNT的表面上的多个碳化硼碳纳米管，其对CNT提供了增强作用，使得它们可用作基质材料的有效的增强填料以提供高强度复合材料。本发明还提供了生产这种碳化物增强CNT的方法。

7. 发明申请

US20080118426A1 Varied morphology carbon nanotubes 审中-公开
标题翻译：不同形态的碳纳米管
公开(公告)号：US20080118426A1
公开(公告)日：2008-05-22
申请号：US11544329
申请日：2006-10-09
申请人： Wenzhi Li , Jian Guo Wen , Zhifeng Ren
发明人： Wenzhi Li , Jian Guo Wen , Zhifeng Ren
IPC分类号： D01F9/12
CPC分类号： B01J37/036 , B01J23/745 , B01J23/75 , B82Y30/00 , B82Y40/00 , C01B32/162 , D01F9/127 , Y10S977/843
摘要： The present invention describes the preparation of carbon nanotubes of varied morphology, catalyst materials for their synthesis. The present invention also describes reactor apparatus and methods of optimizing and controlling process parameters for the manufacture carbon nanotubes with pre-determined morphologies in relatively high purity and in high yields. In particular, the present invention provides methods for the preparation of non-aligned carbon nanotubes with controllable morphologies, catalyst materials and methods for their manufacture.
摘要翻译：本发明描述了不同形态的碳纳米管的制备，用于它们的合成的催化剂材料。本发明还描述了反应器装置和优化和控制具有相对高纯度和高收率的具有预定形态的制造碳纳米管的工艺参数的方法。特别地，本发明提供了制备具有可控形态的非对准碳纳米管的方法，催化剂材料及其制造方法。

8. 发明授权

US06911260B2 Reinforced carbon nanotubes 失效
标题翻译：增强碳纳米管
公开(公告)号：US06911260B2
公开(公告)日：2005-06-28
申请号：US10339849
申请日：2003-01-10
申请人： Zhifen Ren , Jian Guo Wen , Jing Y. Lao , Wenzhi Li
发明人： Zhifen Ren , Jian Guo Wen , Jing Y. Lao , Wenzhi Li
IPC分类号： D01F9/12 , D01F11/12 , B32B9/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/168 , C01B2202/06 , C04B35/62847 , C04B35/6286 , C04B35/62863 , C04B35/62892 , C04B35/62897 , C04B2235/5268 , C04B2235/5288 , D01F9/12 , D01F11/12 , Y10S977/752 , Y10T428/25 , Y10T428/2913 , Y10T428/2918 , Y10T428/292 , Y10T428/2975 , Y10T428/2982 , Y10T428/30
摘要： The present invention relates generally to reinforced carbon nanotubes, and more particularly to reinforced carbon nanotubes having a plurality of microparticulate carbide or oxide materials formed substantially on the surface of such reinforced carbon nanotubes composite materials. In particular, the present invention provides reinforced carbon nanotubes (CNTs) having a plurality of boron carbide nanolumps formed substantially on a surface of the reinforced CNTs that provide a reinforcing effect on CNTs, enabling their use as effective reinforcing fillers for matrix materials to give high-strength composites. The present invention also provides methods for producing such carbide reinforced CNTs.
摘要翻译：本发明一般涉及增强碳纳米管，更具体地说涉及具有多个基本上在这种增强碳纳米管复合材料的表面上形成的微粒碳化物或氧化物材料的增强碳纳米管。特别地，本发明提供了增强的碳纳米管（CNT），其具有基本上形成在增强CNT的表面上的多个碳化硼碳纳米管，其对CNT提供了增强作用，使得它们可用作基质材料的有效的增强填料以提供高强度复合材料。本发明还提供了生产这种碳化物增强CNT的方法。

9. 发明授权

US06207067B1 Method for fabricating oxide superconducting device 失效
标题翻译：氧化物超导器件的制造方法
公开(公告)号：US06207067B1
公开(公告)日：2001-03-27
申请号：US09161697
申请日：1998-09-29
申请人： Naoki Yutani , Katsumi Suzuki , Youichi Enomoto , Jian-Guo Wen
发明人： Naoki Yutani , Katsumi Suzuki , Youichi Enomoto , Jian-Guo Wen
IPC分类号： C23F100
CPC分类号： H01L39/2496 , Y10S505/728
摘要： A method for fabricating an oxide superconducting device includes the steps of: forming a V-shaped groove on a substrate by a converging ion beam and forming a barrier with reduced superconductivity on the oxide superconducting thin-film on the groove to form a Josephson Junction, wherein the irradiation ion amount of the converging ion beam is varied according to the position of the beam within the groove in such a manner that an inclination angle of the inclined portion of the substrate is fixed. An oxide superconducting device (a Josephson Junction device) having a high degree of flexibility in arrangement and with high reproducibility, and having a high degree of uniformity is provided.
摘要翻译：一种制造氧化物超导器件的方法包括以下步骤：通过会聚离子束在衬底上形成V形槽，并在沟槽上的氧化物超导薄膜上形成具有降低的超导性的阻挡层以形成约瑟夫逊结，其中会聚离子束的照射离子量根据所述槽内的所述光束的位置以固定所述基板的倾斜部分的倾斜角度的方式而变化。提供了具有高度的布置灵活性和高重现性并且具有高均匀度的氧化物超导装置（约瑟夫逊结装置）。

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