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    • 1. 发明授权
    • Method for transferring a thin layer by proton exchange
    • 通过质子交换传输薄层的方法
    • US08693835B2
    • 2014-04-08
    • US12937945
    • 2009-04-10
    • Aurélie TauzinJean-Sébastien Moulet
    • Aurélie TauzinJean-Sébastien Moulet
    • G02B6/10
    • C30B31/04C30B33/02H01L21/76254
    • A method for transferring a thin layer from a lithium-based first substrate includes proton exchange between the first substrate and a first electrolyte, which is an acid, through a free face of the first substrate so as to replace lithium ions of the first substrate by protons, in a proportion between 10% and 80%, over a first depth e1. A reverse proton exchange between the first substrate and a second electrolyte, through the free face is carried out so as to replace substantially all the protons with lithium ions over a second depth e2 smaller than the first depth e1, and so as to leave an intermediate layer between the depths e1 and e2, in which intermediate layer protons incorporated during the proton exchange step remain. The depth e2 defines a thin layer between the free face and the intermediate layer. A heat treatment is carried out under conditions suitable for embrittling the intermediate layer and the thin film is separated from the first substrate at the intermediate layer.
    • 用于从锂基第一衬底转移薄层的方法包括通过第一衬底的自由面在第一衬底和作为酸的第一电解质之间的质子交换,以便通过第一衬底的自由面来代替第一衬底的锂离子,以便代替第一衬底的锂离子 质子比例在第一深度e1之间以10%至80%的比例。 通过自由面进行第一衬底和第二电解质之间的反向质子交换,以便在小于第一深度e1的第二深度e2上用锂离子代替基本上所有的质子,并且留下中间体 深度e1和e2之间的层,其中保留在质子交换步骤期间并入的中间层质子。 深度e2限定了自由面和中间层之间的薄层。 在适于脆化中间层的条件下进行热处理,并且在中间层与第一基板分离薄膜。
    • 2. 发明申请
    • METHOD FOR TRANSFERRING A THIN LAYER BY PROTON EXCHANGE
    • 通过PROTON EXCHANGE传输薄层的方法
    • US20110030889A1
    • 2011-02-10
    • US12937945
    • 2009-04-10
    • Aurélie TauzinJean-Sébastien Moulet
    • Aurélie TauzinJean-Sébastien Moulet
    • B32B38/10
    • C30B31/04C30B33/02H01L21/76254
    • A method for transferring a thin layer from a lithium-based first substrate includes proton exchange between the first substrate and a first electrolyte, which is an acid, through a free face of the first substrate so as to replace lithium ions of the first substrate by protons, in a proportion between 10% and 80%, over a first depth e1. A reverse proton exchange between the first substrate and a second electrolyte, through the free face is carried out so as to replace substantially all the protons with lithium ions over a second depth e2 smaller than the first depth e1, and so as to leave an intermediate layer between the depths e1 and e2, in which intermediate layer protons incorporated during the proton exchange step remain. The depth e2 defines a thin layer between the free face and the intermediate layer. A heat treatment is carried out under conditions suitable for embrittling the intermediate layer and the thin film is separated from the first substrate at the intermediate layer.
    • 用于从锂基第一衬底转移薄层的方法包括通过第一衬底的自由面在第一衬底和作为酸的第一电解质之间的质子交换,以便通过第一衬底的自由面来代替第一衬底的锂离子,以便代替第一衬底的锂离子 质子比例在第一深度e1之间以10%至80%的比例。 通过自由面进行第一衬底和第二电解质之间的反向质子交换,以便在小于第一深度e1的第二深度e2上用锂离子代替基本上所有的质子,并且留下中间体 深度e1和e2之间的层,其中保留在质子交换步骤期间并入的中间层质子。 深度e2限定了自由面和中间层之间的薄层。 在适于脆化中间层的条件下进行热处理,并且在中间层与第一基板分离薄膜。