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    • 4. 发明授权
    • Molded products for molding compositions containing thermalsetting
(meth)acrylate liquid resins
    • 含有热固性(甲基)丙烯酸酯液体树脂的成型组合物的成型产品
    • US5364903A
    • 1994-11-15
    • US930975
    • 1992-08-14
    • Yuji TakayamaHirotaka WadaIwao Komiya
    • Yuji TakayamaHirotaka WadaIwao Komiya
    • C08F220/36C08G18/81C08K3/22C08F220/26
    • C08G18/8116C08F220/36
    • Thermosetting (meth)acrylate molding liquid resin consisting of a specified type of unsaturated oligourethane and alkyl (meth)acrylate within a specified range of ratio. Such a specified type of unsaturated oligourethane may be obtained by reaction between 2-isocyanatoalkyl (meth)acrylate and polyhydric alcohol or by reacting 2-isocyanatoalkyl (meth)acrylate with polyhydric alcohol at molar ratio of functional groups NCO/OH between 1.1 and 1.6 to form a urethane compound and reacting hydroxyalkyl (meth)acrylate with a residual portion of 2-isocyanatoalkyl (meth)acrylate at molar ratio of functional groups OH/NCO between 1.0 and 1.5. This invention also includes molding compositions containing such liquid resin and a specified type of inorganic filler and/or a certain type of thermoplastic high molecular compound as well as molded objects obtained by curing such compositions in a mold.
    • 由指定类型的不饱和低聚氨酯和(甲基)丙烯酸烷基酯组成的热固性(甲基)丙烯酸酯成型液体树脂在指定的比例范围内。 这种特定类型的不饱和低聚氨酯可以通过(甲基)丙烯酸2-异氰酸烷基酯与多元醇反应或通过使异氰酸烷基(甲基)丙烯酸酯与多元醇与官能团NCO / OH的摩尔比在1.1和1.6之间反应获得, 形成氨基甲酸酯化合物,并使(甲基)丙烯酸羟烷基酯与官能团OH / NCO的摩尔比在1.0和1.5之间的残留部分的(甲基)丙烯酸-2-异氰酸烷基酯反应。 本发明还包括含有这种液体树脂和特定类型的无机填料和/或某种类型的热塑性高分子化合物的模塑组合物以及通过在模具中固化这种组合物而获得的模制物品。
    • 5. 发明授权
    • Polymerizable compositions and in-mold cured products using same
    • 可聚合组合物和使用其的模内固化产物
    • US5382619A
    • 1995-01-17
    • US54554
    • 1993-04-28
    • Yuji TakayamaHirokazu MatsuedaMasato SugiuraTatsuhiko OzakiHirotaka WadaToshiharu SuzukiIwao Komiya
    • Yuji TakayamaHirokazu MatsuedaMasato SugiuraTatsuhiko OzakiHirotaka WadaToshiharu SuzukiIwao Komiya
    • C08F283/00C08K3/22C08F226/02C08F271/00C08L39/00
    • C08F283/008
    • A polymerizable composition contains unsaturated urethane shown by Formula (1) given below, vinyl monomer which is copolymerizable with this unsaturated urethane, and an inorganic powder filler at weight ratio of (unsaturated urethane)/(vinyl monomer)=10/90-90/10, the inorganic powder filler being 30-300 weight parts with respect to 100 weight parts of the sum of the unsaturated urethane and vinyl monomer: ##STR1## where X is a residual group obtained by removing isocyanate groups from polyisocyanate; Y is a residual group obtained by removing hydroxyl groups from polyol; R.sup.1 is a residual group obtained by removing hydroxyl group from non-radical polymerizable mono-ol having aliphatic hydrocarbon group with 6-22 carbon atoms; R.sup.2 is H or CH.sub.3 ; and p, q and r are each an integer 1-3 such that 2.ltoreq.p+q.ltoreq.4 and qr.gtoreq.2. In-mold cured products obtained from such a polymerizable composition have superior external appearance and water-resistance, and their mold shrinkage is small.
    • 聚合性组合物含有下述式(1)所示的不饱和氨基甲酸酯,可与该不饱和氨基甲酸酯共聚的乙烯基单体和(不饱和氨基甲酸酯)/(乙烯基单体)= 10/90〜90 / 10,无机粉末填料相对于不饱和聚氨酯和乙烯基单体总和的100重量份为30-300重量份:其中X是通过从多异氰酸酯除去异氰酸酯基团而获得的残基; Y是通过从多元醇中除去羟基获得的残基; R1是通过从具有6-22个碳原子的脂族烃基的不可自由基聚合的单醇中除去羟基而获得的残基; R2是H或CH3; 并且p,q和r各自是整数1-3,使得2 = p + q 4和qr> / = 2。 由这种可聚合组合物获得的模内固化产物具有优异的外观和耐水性,并且它们的模具收缩率小。