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    • 3. 发明授权
    • Preparation of quinacridone pigment compositions
    • 喹吖啶酮颜料组合物的制备
    • US06494948B2
    • 2002-12-17
    • US09747465
    • 2000-12-22
    • Daphne J. RiceIbraheem T. Badejo
    • Daphne J. RiceIbraheem T. Badejo
    • C09B4800
    • C09B48/00C09B67/0036
    • This invention relates to a process for preparing quinacridone pigment compositions by (a) heating a reaction mixture containing (i) 2,5-dianilinoterephthalic acid or 2,5-dianilino-6,13-dihydroterephthalic acid or a derivative thereof, (ii) about 0.1 to about 5 percent, based on component (a)(i), of 2,5-di(sulfamoylanilino)terephthalic acid and/or 2,5-di(sulfamoylanilino)-6,13-dihydroterephthalic acid or a derivative thereof, (iii) about 0.1 to about 15 percent by weight, based on component (a)(i), of other sulfonyl-containing derivatives of 2,5-dianilinoterephthalic acid and/or 2,5-dianilino-6,13-dihydroterephthalic acid, (iv) about 3 to about 20 parts by weight, per part of component (a)(i), of a dehydrating agent, and (v) optionally, a solvent; (b) drowning the reaction mixture from step (a) with a liquid in which the quinacridone pigment composition is substantially insoluble; and (c) isolating the quinacridone pigment composition.
    • 本发明涉及一种通过(a)加热含有(i)2,5-二苯胺基对苯二甲酸或2,5-二苯胺基-6,13-​​二氢对苯二甲酸或其衍生物的反应混合物制备喹吖啶酮颜料组合物的方法,(ii) 基于组分(a)(i)的2,5-二(氨磺酰苯胺基)对苯二甲酸和/或2,5-二(氨磺酰苯胺基)-6,13-​​二氢对苯二甲酸或其衍生物的约0.1至约5% ,(iii)基于组分(a)(i)约0.1至约15重量%的其它含2,5-二苯胺基对苯二甲酸磺酰基衍生物和/或2,5-二苯胺基-6,13-​​二氢对苯二甲酸 酸,(iv)每份组分(a)(i)约3至约20重量份的脱水剂,和(v)任选的溶剂;(b)将反应混合物从步骤(a ),其中喹吖啶酮颜料组合物基本上不溶; 和(c)分离喹吖啶酮颜料组合物。
    • 4. 发明授权
    • Organic pigment compositions
    • 有机颜料组合物
    • US5879444A
    • 1999-03-09
    • US923743
    • 1997-09-02
    • Ibraheem T. BadejoDaphne J. Rice
    • Ibraheem T. BadejoDaphne J. Rice
    • C09B67/22C09D11/02G03G9/09C09B48/00C07D471/00
    • C09D11/037C09B67/0034C09B67/0036G03G9/092G03G9/0924
    • This invention relates to pigment compositions containing an organic pigment treated with a pigment derivative having the formula (I) ##STR1## wherein Q represents an organic pigment moiety;X is O, S, or N--R.sup.1 ;Y is N--R.sup.2, O, or a direct bond;Z is --CO--, --Alk--, --Ar--, or chemically reasonable combinations thereof;Alk is C.sub.1 -C.sub.5 alkylene, C.sub.2 -C.sub.5 alkenylene, or C.sub.4 -C.sub.5 alkadienylene, or substituted derivatives thereof;Ar is arylene;R.sup.1 is hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.7 -C.sub.16 aralkyl, or --CN; andR.sup.2 is hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.5 -C.sub.7 cycloalkyl, C.sub.7 -C.sub.16 aralkyl, or C.sub.6 -C.sub.10 aryl;with the provisos that(1) the cyclic moiety represented by the formula ##STR2## must be a four- to seven-membered ring, (2) Z can contain a C.dbd.O group adjacent to the nitrogen atom of the Q--CH.sub.2 --N moiety only if Y is N--R.sup.2 or O, and(3) X can be O only if Y is N--R.sup.2 or O.
    • 本发明涉及包含用具有式(I)的颜料衍生物(I)处理的有机颜料的颜料组合物,其中Q表示有机颜料部分; X是O,S或N-R 1; Y是N-R2,O或直接键; Z是-CO-,-Alk-,-Ar-或其化学合理的组合; Alk是C1-C5亚烷基,C2-C5亚烯基或C4-C5链二烯或其取代的衍生物; Ar是亚芳基; R1是氢,C1-C6烷基,C7-C16芳烷基或-CN; 和R 2是氢,C 1 -C 6烷基,C 5 -C 7环烷基,C 7 -C 16芳烷基或C 6 -C 10芳基; 条件是(1)由式“IMAGE”表示的环状部分必须是4至7元环,(2)Z可以含有邻近Q-CH 2 - 的氮原子的C = O基团, N部分,只有Y为N-R2或O时,(3)仅当Y为N-R2或O时X为O。
    • 6. 发明授权
    • Heterocyclic-substituted quinacridone pigments
    • 杂环取代的喹吖啶酮颜料
    • US5868828A
    • 1999-02-09
    • US81849
    • 1998-05-20
    • Ibraheem T. BadejoGuenter Franke
    • Ibraheem T. BadejoGuenter Franke
    • C09B48/00
    • C09B48/00
    • This invention relates to quinacridone pigments of formula (I) ##STR1## wherein X is O, S, or NR;R is hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.5 -C.sub.7 cycloalkyl, or C.sub.7 -C.sub.16 aralkyl;Y is C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 alkoxy, or halogen;the dashed line represents an optional double bond;R.sup.1 and R.sup.2 are independently hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.5 -C.sub.7 cycloalkyl, C.sub.6 -C.sub.10 aryl, C.sub.7 -C.sub.16 aralkyl, nitrile, or carboxyl or an ester or an amide thereof, or R.sup.1 and R.sup.2 together form a C.sub.5 -C.sub.8 cycloaliphatic ring or a fused-on aromatic or heteroaromatic ring;R.sup.3 is hydrogen or C.sub.1 -C.sub.6 alkyl; andm is 0, 1, or 2.This invention further relates to the preparation and use of such quinacridone pigments.
    • 本发明涉及式(I)的化合物(I)其中X是O,S或NR的喹吖啶酮颜料; R是氢,C 1 -C 6烷基,C 5 -C 7环烷基或C 7 -C 16芳烷基; Y是C1-C6烷基,C1-C6烷氧基或卤素; 虚线表示可选的双键; R 1和R 2独立地是氢,C 1 -C 6烷基,C 5 -C 7环烷基,C 6 -C 10芳基,C 7 -C 16芳烷基,腈或羧基或其酯或酰胺,或者R 1和R 2一起形成C 5 -C 8环脂族 环或稠合的芳族或杂芳族环; R3是氢或C1-C6烷基; 并且m为0,1或2.本发明还涉及这种喹吖啶酮颜料的制备和用途。
    • 10. 发明申请
    • Controlled Exotherm of Cyanoacrylate Formulations
    • 氰基丙烯酸酯配方的控制放热
    • US20100030258A1
    • 2010-02-04
    • US12183295
    • 2008-07-31
    • Ibraheem T. BADEJOAndres RIVERAMelanie VANDER KLOK
    • Ibraheem T. BADEJOAndres RIVERAMelanie VANDER KLOK
    • A61B17/03C08F2/00A61F13/00
    • C09J4/00
    • An adhesive composition includes one or more polymerizable cyanoacrylate monomers, a polymerization initiator and a polymerization accelerator for the one or more polymerizable cyanoacrylate monomers. A system for treating living tissue includes a first reservoir containing one or more polymerizable cyanoacrylate monomers, a second reservoir in a non-contacting relationship with the first reservoir containing a polymerization initiator and accelerator for the one or more polymerizable cyanoacrylate monomers, and an applicator capable of combining the polymerizable cyanoacrylate monomer and the polymerization initiator and accelerator to form an adhesive composition and then applying the adhesive composition to living tissue. The initiator may be a quaternary ammonium salt, and the accelerator may be a trihydroxy tertiary amine.
    • 粘合剂组合物包含一种或多种可聚合的氰基丙烯酸酯单体,一种或多种可聚合的氰基丙烯酸酯单体的聚合引发剂和聚合促进剂。 一种用于治疗活组织的系统包括含有一种或多种可聚合的氰基丙烯酸酯单体的第一储存器,与所述第一储存器非接触关系的第二储存器,所述第一储存器含有用于所述一种或多种可聚合的氰基丙烯酸酯单体的聚合引发剂和促进剂, 将可聚合氰基丙烯酸酯单体与聚合引发剂和促进剂结合以形成粘合剂组合物,然后将粘合剂组合物施加到活组织。 引发剂可以是季铵盐,促进剂可以是三羟基叔胺。