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1. 发明授权

US4169194A Process for producing polyethylene 失效
标题翻译：生产聚乙烯的方法
公开(公告)号：US4169194A
公开(公告)日：1979-09-25
申请号：US928694
申请日：1978-07-27
申请人： Neonila I. Ivancheva , Vladimir I. Pilipovsky , Rita E. Prokofieva , Elena I. Nalivaiko , Maria A. Budanova
发明人： Neonila I. Ivancheva , Vladimir I. Pilipovsky , Rita E. Prokofieva , Elena I. Nalivaiko , Maria A. Budanova
IPC分类号： C08F10/02 , C08F4/68
CPC分类号： C08F10/02
摘要： A process for producing polyethylene comprising polymerizing ethylene in a medium of a hydrocarbon solvent at a temperature within the range of from 30.degree. to 110.degree. C. under a pressure of from 1 to 60 atm.g. in the presence of a complex organometallic catalyst; said catalyst consisting of an alkylaluminiumhalide of the formula AlR.sub.n (X).sub.3-n (I), wherein R is an alkyl with a number of carbon atoms from 2 to 18; X is Cl, Br, I; n=1 or 2; an oxyvanadiumalkoxide of the formula OV(OR').sub.3 (II), wherein R' is an alkyl with a number of carbon atoms from 2 to 20; and a complex of acrylonitrile with diethylaluminiumchloride of the formula CH.sub.2 =CHCN.Al(C.sub.2 H.sub.5).sub.2 Cl (III); molar ratio between said catalytic components I:II:III being equal to 5-20:1:1-5, respectively. The process makes it possible to obtain polyethylene with a wide (5 to 10) molecular-mass distribution and with an enhanced adhesion to a metal (more than 3000 g/cm). Polyethylene possessing the above-cited characteristics is readily processed by the extrusion method to articles of household and industrial applications.
摘要翻译：一种生产聚乙烯的方法，包括在烃溶剂的介质中，在30至110℃的温度范围内，在1至60大气压的压力下聚合乙烯。在复合有机金属催化剂存在下; 所述催化剂由式AlRn（X）3-n（I）的烷基铝卤化物组成，其中R是碳原子数为2至18的烷基; X是Cl，Br，I; n = 1或2; 式（OR'）3（II）的氧钒烷氧化物，其中R'是碳原子数为2至20的烷基; 和丙烯腈与式CH 2 = CHCN.Al（C 2 H 5）2 Cl（III）的二乙基氯化铝的络合物; 所述催化组分I:II:III之间的摩尔比分别等于5-20:1:1-5。该方法可以获得具有宽（5至10）分子质量分布并且对金属（大于3000g / cm 3）的增强的粘附性的聚乙烯。具有上述特征的聚乙烯通过挤出法容易地加工成家用和工业用途。

3. 发明专利

BG42597A1 SOLVENT FOR SURFACE STRUCTURISATION 未知
公开(公告)号：BG42597A1
公开(公告)日：1988-01-15
申请号：BG7640786
申请日：1986-09-15
申请人： DONCHEVA NADKA D , JANKULOV VENCESLAV G , IVANCHEVA TINKA L , PETROVA NEDJALKA N , BONCHEVA EMILIJA N
发明人： DONCHEVA NADKA D , JANKULOV VENCESLAV G , IVANCHEVA TINKA L , PETROVA NEDJALKA N , BONCHEVA EMILIJA N
IPC分类号： C08L61/00

4. 发明专利

BG39874A1 METHOD FOR PREPARING 5(4)- METHYLIMIDAZOL 未知
公开(公告)号：BG39874A1
公开(公告)日：1986-09-15
申请号：BG7007985
申请日：1985-05-03
申请人： SBEVA JJORDANOVA , BAEVA , KOLCHAGOVA , PEJJCHEVA , GEORGIEV , IVANOVA , VITEV , MICEV , VASILEVA , IVANCHEVA , DENKOVA , GEORGIEVA , PASKALEV , KARAKOLEV , VELEV , VLEV , IVANOV , ORACHEV , ZIKOLOVA , NINOVA
发明人： SBEVA-JJORDANOVA , BAEVA , KOLCHAGOVA , PEJJCHEVA , GEORGIEV , IVANOVA , VITEV , MICEV , VASILEVA , IVANCHEVA , DENKOVA , GEORGIEVA , PASKALEV , KARAKOLEV , VELEV , VLEV , IVANOV , ORACHEV , ZIKOLOVA , NINOVA
IPC分类号： C07D233/54

5. 发明专利

BG38886A1 METHOD AND DEVICE FOR DETERMING SCALE- FORMING RESITANCE OF METALS AND ALLOYS 未知
公开(公告)号：BG38886A1
公开(公告)日：1986-03-14
申请号：BG6803184
申请日：1984-12-21
申请人： LEKOV , DIMITROV , DZHAMBAZOVA , SEMKOV , NESTOROVA , IVANCHEVA
发明人： LEKOV , DIMITROV , DZHAMBAZOVA , SEMKOV , NESTOROVA , IVANCHEVA
IPC分类号： G01N7/00 , G01N33/20

6. 发明专利

BG99853A METHOD FOR THE PREPARATION OF P-TOLUENESULPHONIC SALTS OF 2,2,6,6-TETRAMETHYL-4-PIPERIDINON 未知
公开(公告)号：BG99853A
公开(公告)日：1997-05-30
申请号：BG9985395
申请日：1995-08-08
申请人： VITEV , KLISAROVA , GEORGIEVA , TODOROVA , RUSEVA , GEORGIEV , ORACHEV , KATSOV , BIKOVA , DENKOVA , IVANCHEVA , NIKOVA , PETKOVA , AKHCHIJSKA
发明人： VITEV MATEJ I , KLISAROVA MARIJA N , GEORGIEVA LORA A , TODOROVA KATJA S , RUSEVA NINA G , GEORGIEV ALEKSANDAR KH , ORACHEV VESELIN L , KATSOV GEORGI I , BIKOVA NADEZHDA V , DENKOVA EKATERINA P , IVANCHEVA LILJANA K , NIKOVA OLIMPIJA B , PETKOVA RUMJANA TS , AKHCHIJSKA ELENA D
IPC分类号： A61K31/00 , A61K31/255 , A61K31/445 , C07C309/24 , C07D211/32
摘要： The produced p-toluenesulphonic salt of 2,2,6,6-tetramethyl-4-piperidinon is used as a tranquillizer. The compound has the formula By the method acetone reacts with concentrated hydrochloric acid and ammonia in the form of ammonia water with concentration over 20%, in a given case ammonium hydrogen carbonate. The produced 2,2,6,6-tetramethyl-4-piperidinon reacts with the p-toluenesulphonic acid in an alcohol solvent in the presence of antioxidant, and pure product is being directly produced. For a medium ethyl or methyl alcohol is mostly used, and sodium sulphite, sodium metabisulphite or sodium hydrosulphite (sodium dithionite) are used as antioxidants. By the method the processes are compactly materialized, yields are increased and the quality of the product is improved.

7. 发明专利

BG61251B1 METHOD FOR THE PREPARATION OF MEDICAMENT OF HYPERTENSIVE,SPASMOLYTIC AND CAPILLARY-CONSOLIDATING EFFECT 未知
公开(公告)号：BG61251B1
公开(公告)日：1997-04-30
申请号：BG9786393
申请日：1993-06-11
申请人： IVANCHEVA STEFANKA V. , GEORGIEV GRIGOR S. , TEREZOV VASIL P. , PRAMATAROVA VELICHKA K. , TODOROV LJUBEN B.
发明人： IVANCHEVA STEFANKA V , GEORGIEV GRIGOR S , TEREZOV VASIL P , PRAMATAROVA VELICHKA K , TODOROV LJUBEN B
IPC分类号： A61K35/78
摘要： The method is used in medicine. The medicament produced isnot toxic and has no side effects. According to the method,geranium rhizome is extracted under conventional conditions bymeans of organic solvents. The extract is concentrated subjectedto double chromatography on silicagel and polyamide S and isconcentrated.

8. 发明专利

BG38398A1 CRYSTAL ALPHA- FORM OF 2- CHLOR- 11- (4- METHYL- 1- PIPERAZINYL)- DIBENZ [B, F] [1, 4]- OXAZEPINE SUCCINATE AND METHOD FOR ITS PREPARATION 未知
公开(公告)号：BG38398A1
公开(公告)日：1985-12-16
申请号：BG5943883
申请日：1983-01-25
申请人： EVSTATIEVA , IVANCHEVA , VITEV , DENKOVA , GEORGIEV , ZIKOLOVA , JANKOVA , BCHVAROVA , TODOROVA , ILIEV , TODOROV , LUNA , JJORDANOV , IVANOVA
发明人： EVSTATIEVA , IVANCHEVA , VITEV , DENKOVA , GEORGIEV , ZIKOLOVA , JANKOVA , BCHVAROVA , TODOROVA , ILIEV , TODOROV , LUNA , JJORDANOV , IVANOVA
IPC分类号： C07D267/20

9. 发明专利

BG35658A1 METHOD FOR PREPARING 4- METHYL- 1- PIPERAZINE- THIOCARBOXY MIDDLE OPENING BRACKET 2- (4- CHLORPHENOXY)- ANILIDE MIDDLE CLOSED BRACKET 未知
公开(公告)号：BG35658A1
公开(公告)日：1984-06-15
申请号：BG6020283
申请日：1983-03-21
申请人： IVANCHEVA , VITEV , DENKOVA , GEORGIEV , ZIKOLOVA , TODOROV
发明人： IVANCHEVA , VITEV , DENKOVA , GEORGIEV , ZIKOLOVA , TODOROV
IPC分类号： C07D241/04

10. 发明专利

BG41555A1 METHOD FOR PREPARING OF 4- METHYL- 2'- (4- CHLOROPHENOXY)- 1- PIPERAZINE CARBOXANILIDE HYDROCHLORIDE 未知
公开(公告)号：BG41555A1
公开(公告)日：1987-07-15
申请号：BG7439886
申请日：1986-04-02
申请人： IVANCHEVA , VITEV , DENKOVA , GEORGIEV , GEORGIEVA , EVSTATIEVA , ZIKOLOVA , TODOROV , ILIEV
发明人： IVANCHEVA , VITEV , DENKOVA , GEORGIEV , GEORGIEVA , EVSTATIEVA , ZIKOLOVA , TODOROV , ILIEV
IPC分类号： C07D295/20

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