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    • 1. 发明授权
    • Device for electrothermal atomizing of samples for spectroscopic purposes
    • 用于电光源用于光谱目的的样品的设备
    • US5066123A
    • 1991-11-19
    • US481834
    • 1990-02-16
    • Rolf TammGunther RodelErich Stengele
    • Rolf TammGunther RodelErich Stengele
    • G01N1/00G01N21/31G01N21/74
    • G01N21/74G01N1/10
    • A device for electrothermal atomization of samples for spectroscopic purposes with a furnace body made of graphite, designed such that electrical current can be passed through, and a pot-shaped sample receptacle which is separated from the furnace body and projects into a lateral aperture of the furnace body comprises a driving device by which the sample receptacle is movable into and out of thermal contact with the furnace body. The driving device together with the heating current of the furnace body is controlled by a controlling device such that the sample receptacle engages the furnace body during a drying and decomposing step and thereafter, is raised from the furnace body by the driving device. Thereafter, with raised sample receptacle, the furnace body is heated to atomization temperature until a temperature stabilization is achieved and, finally, the sample receptacle is again moved into contact with the furnace body.
    • 用于光谱雾化用于光谱目的的装置,用石墨制成的炉体,设计成能够通过电流,以及从炉体分离并突出到炉体的侧向孔中的罐形样品容器 炉体包括驱动装置,通过该驱动装置,样品容器可移动进入和离开与炉体的热接触。 驱动装置与炉体的加热电流一起由控制装置控制,使得样品容器在干燥和分解步骤期间与炉体接合,然后通过驱动装置从炉体升起。 此后,用升高的样品容器将炉体加热至雾化温度,直到达到温度稳定,最后,样品容器再次与炉体接触。