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1. 发明授权

US4590129A Fluoroaliphatic-thio,-sulfinyl, or sulfonyl substituted bicycloaliphatic amic acid amine salts, and compositions and use thereof 失效
标题翻译：氟脂族硫代， - 亚磺酰基或磺酰基取代的双环脂肪族酰胺胺盐，及其组合物和用途
公开(公告)号：US4590129A
公开(公告)日：1986-05-20
申请号：US692256
申请日：1985-01-17
申请人： Jurgen Kaschig , Eduard K. Kleiner , Karl F. Mueller , Thomas W. Cooke
发明人： Jurgen Kaschig , Eduard K. Kleiner , Karl F. Mueller , Thomas W. Cooke
IPC分类号： C07D307/77 , C07D307/93 , D21D3/00 , B32B9/02 , B32B27/00
CPC分类号： C07D307/77 , C07D307/93 , Y10T428/31591 , Y10T428/31725 , Y10T428/31993
摘要： Fluoroaliphatic-thio,-sulfinyl and -sulfonyl substituted bicycloaliphatic amic acid amine salts of the formula ##STR1## where R.sub.f is perfluoroalkyl, R' is alkylene optionally interrupted by --O--, --S-- or ##STR2## where R.sub.a is hydrogen or alkyl, Y is lower alkylene or --O--, n is 0-2, R.sub.1 and R.sub.2 are independently hydrogen, lower alkyl, hydroxy lower alkyl or together with the nitrogen to which they are attached, represent morpholino, R.sub.3, R.sub.4 and R.sub.5 are independently hydrogen, lower alkyl, or hydroxy lower alkyl, R.sub.6 is lower alkyl, carboxy lower alkyl, sulfo lower alkyl, hydroxy lower alkyl, benzyl or together with R.sub.5 and the nitrogen to which they are attached represent morpholino, and R is hydrogen or methyl are provided. These salts applied in the form of aqueous solutions, dispersions or emulsions are useful in rendering cellulosic and natural and synthetic polyamide materials oil and water repellent.
摘要翻译：其中R f为全氟烷基，R'为任选被-O-，-S-或其中R a为间隔的亚烷基的氟脂肪族 - 硫代 - 亚磺酰基和 - 磺酰基取代的双环脂肪族酰胺酸胺，其中R a为氢或烷基，Y是低级亚烷基或-O-，n是0-2，R1和R2独立地是氢，低级烷基，羟基低级烷基或与它们相连的氮一起代表吗啉代，R3，R4和 R5独立地是氢，低级烷基或羟基低级烷基，R6是低级烷基，羧基低级烷基，磺基低级烷基，羟基低级烷基，苄基或与R5一起，并且与它们相连的氮代表吗啉代，R是氢或甲基。以水溶液，分散体或乳液的形式施用的这些盐可用于使纤维素和天然和合成的聚酰胺材料具有防油和防水性能。

2. 发明授权

US4238575A Stabilized compositions containing polymeric thiosynergists 失效
标题翻译：含有聚合硫代增效剂的稳定组合物
公开(公告)号：US4238575A
公开(公告)日：1980-12-09
申请号：US11275
申请日：1979-02-12
申请人： Eduard K. Kleiner , Martin Dexter
发明人： Eduard K. Kleiner , Martin Dexter
IPC分类号： C08L23/02 , C08L33/14 , C08L23/00
CPC分类号： C08L23/02 , C08K5/24 , C08L23/0815 , C08L23/10 , C08L33/14
摘要： Polymeric thiosynergists, such as poly[2-(alkylthio)ethyl methacrylate], are stabilizers for organic materials subject to oxidative, thermal and/or light induced deterioration. These polymeric synergists are made by normal free radical polymerization of the corresponding (alkylthio)alkyl polymerizable esters. The esters are prepared by conventional esterification procedures. These compounds are used in conjunction with phenolic antioxidants to stabilize organic materials, particularly polyolefins and hydrocarbon compositions, against the deleterious effects of heat and oxygen.
摘要翻译：聚合硫代增效剂，如聚[2-（烷硫基）乙基甲基丙烯酸酯]，是有机材料的稳定剂，受到氧化，热和/或光诱导的退化。这些聚合增效剂通过相应的（烷硫基）烷基可聚合酯的正常自由基聚合制备。酯通过常规酯化方法制备。这些化合物与酚类抗氧化剂结合使用以稳定有机材料，特别是聚烯烃和烃组合物，以抵抗热和氧的有害影响。

3. 发明授权

US5616273A Synergistic surfactant compositions and fire fighting concentrates thereof 失效
标题翻译：协同表面活性剂组合物及其灭火浓缩物
公开(公告)号：US5616273A
公开(公告)日：1997-04-01
申请号：US289060
申请日：1994-08-11
申请人： Kirtland P. Clark , Eduard K. Kleiner
发明人： Kirtland P. Clark , Eduard K. Kleiner
IPC分类号： A62D1/02 , A62D1/00
CPC分类号： A62D1/0085 , Y10S516/05
摘要： This invention relates to synergistic surfactant compositions based on water insoluble amphoteric fluorochemical surfactants and water soluble anionic hydrocarbon or fluorochemical surfactants of the sulfate or sulfonate type and aqueous film forming foam agents derived from such synergistic surfactant compositions and a method to treat the aqueous waste stream generated by such aqueous film forming foam agents.
摘要翻译：本发明涉及基于水不溶性两性含氟表面活性剂和硫酸盐或磺酸盐型水溶性阴离子烃或含氟表面活性剂的协同表面活性剂组合物以及衍生自这种协同性表面活性剂组合物的水性膜形成泡沫剂以及产生的含水废水流的方法通过这种水性成膜泡沫剂。

4. 发明授权

US5571779A Method of lubrication using perfluoroalkyl terminated urethanes 失效
标题翻译：使用全氟烷基封端的聚氨酯润滑方法
公开(公告)号：US5571779A
公开(公告)日：1996-11-05
申请号：US558905
申请日：1995-11-15
申请人： Eduard K. Kleiner , Athanasios Karydas
发明人： Eduard K. Kleiner , Athanasios Karydas
IPC分类号： C07C271/12 , C07C271/20 , C07C271/24 , C07C333/04 , C09G3/00 , C10M105/68 , C10M105/72 , C10M133/16 , C10M135/26 , C10M105/08 , C10M105/54
CPC分类号： C07C271/24 , C07C271/12 , C07C271/20 , C07C333/04 , C09G3/00 , C10M105/68 , C10M105/72 , C10M133/16 , C10M135/26 , C07C2101/14 , C10M2201/00 , C10M2201/041 , C10M2201/042 , C10M2201/061 , C10M2201/16 , C10M2201/18 , C10M2205/022 , C10M2205/14 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10M2215/10 , C10M2215/102 , C10M2219/085 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： This invention relates to perfluoroalkyl group terminated urethanes, thiourethanes and ureas of the general formula(R--X--CONH).sub.m Awhere m is 1, 2 or 3, R is R.sub.f --E and optionally R.sub.1 with the proviso that at least one R is R.sub.f --E, R.sub.f is a perfluoroalkyl group, R.sub.1 is a hydrocarbon group, E is a divalent linking group, X is --O--, --S--, --NR.sub.2 -- and R.sub.2 is H or lower alkyl and A is R.sub.f E or R.sub.1 if m is 1 and a divalent or trivalent linking group if m is 2 or 3 respectively. Compounds of this general formula are useful as solid lubricants or as additives for waxes and resins providing lubricating properties.
摘要翻译：本发明涉及通式（RX-CONH）mA的全氟烷基封端的氨基甲酸酯，硫代氨基甲酸酯和脲，其中m为1,2或3，R为R f -E且任选地为R 1，条件是至少一个R为Rf-E Rf为全氟烷基，R 1为烃基，E为二价连接基团，X为-O - ， - S - ， - NR2-，R 2为H或低级烷基，A为RfE或R 1，如果m为1 如果m分别为2或3，则为二价或三价连接基团。该通式的化合物可用作固体润滑剂或作为提供润滑性能的蜡和树脂的添加剂。

5. 发明授权

US4439329A Aqueous based fire fighting foam compositions containing hydrocarbyl sulfide terminated oligomer stabilizers 失效
标题翻译：含有烃基硫化物封端的低聚物稳定剂的水性消防泡沫组合物
公开(公告)号：US4439329A
公开(公告)日：1984-03-27
申请号：US335119
申请日：1981-12-28
申请人： Eduard K. Kleiner , Robert A. Falk
发明人： Eduard K. Kleiner , Robert A. Falk
IPC分类号： C09K21/10 , A62D1/00 , A62D1/02 , A62D1/04 , C09K21/14 , A62C1/12
CPC分类号： A62D1/0071
摘要： This invention relates to aqueous based fire fighting foams containing a stabilizing amount of an oligomer of the formulaR.sub.1 --E--S(O).sub.n [M.sub.1 ].sub.x [M.sub.2 ].sub.y [M.sub.3 ].sub.z Hwherein R.sub.1 is an oleophilic aryl, araliphatic, aliphatic or cycloaliphatic group having up to 25 carbon atoms; E is a direct bond, or an organic covalently bonded divalent linking group, n is 0, 1 or 2, [M.sub.1 ] is a hydrophilic acrylamido monomer unit, [M.sub.2 ] is a copolymerizable non-acrylamido hydrophilic monomer unit, [M.sub.3 ] is a copolymerizable hydrophobic monomer unit, the average of the sum of x, y and z is between about 3 and about 500, and x/x+y+z is between 1 and about 0.5. These stabilizing oligomer additives in aqueous based fire fighting foams improve foam expansion, foam drainage and fire extinguishing times.
摘要翻译：本发明涉及含有稳定量的式R1-ES（O）n [M1] x [M2] y [M3] zH的低聚物的水性消防泡沫，其中R1是亲油芳基，芳脂族，脂族或环脂族具有多达25个碳原子的基团; E是直接键合，或有机共价键合的二价连接基团，n为0,1或2，[M1]为亲水性丙烯酰氨基单体单元，[M2]为可共聚的非丙烯酰氨基亲水单体单元，[M3]为可共聚的疏水单体单元，x，y和z之和的平均值在约3至约500之间，x / x + y + z在1至约0.5之间。这些在水性消防泡沫中的稳定低聚物添加剂改善了泡沫膨胀，泡沫排放和灭火时间。

6. 发明授权

US4075237A Perfluorinated esters of fumaric acid and certain other ethylenically unsaturated poly-basic acid and soil repellant polymers thereof 失效
标题翻译：富马酸的全氟化酯和某些其它烯属不饱和多元碱性酸和污垢排斥性聚合物
公开(公告)号：US4075237A
公开(公告)日：1978-02-21
申请号：US720370
申请日：1968-04-10
申请人： Eduard K. Kleiner , Martin Knell
发明人： Eduard K. Kleiner , Martin Knell
IPC分类号： C07C69/60 , C07C203/04 , C08F22/18 , C08F28/00 , C08F222/10 , C14C11/00 , D06M15/277 , C07C67/16
CPC分类号： D06M15/277 , C07C203/04 , C07C323/00 , C07C327/00 , C08F22/18 , C08F28/00 , C14C11/003
摘要： Monomeric esters of fumaric, maleic, citraconic, mesaconic, itaconic, aconitic, or methylene malonic acid and alcohols of the formula C.sub.m F2.sub.m+1 C.sub.n H2.sub.n OH and mercaptans of the formula C.sub.m F2.sub.m+1 C.sub.n H2.sub.n SH form homopolymers and form copolymers with other ethylenically unsaturated comonomers. The polymers obtained have valuable soil repellent properties and are especially useful in textile finishes. Preferred compounds are bis (1,1,2,2-tetrahydroperfluorononyl) fumarate and bis (1,1-dihydroperfluorooctyl) fumarate.

7. 发明授权

US3965148A Perfluoroalkyl alcohols 失效
标题翻译：全氟烷基醇
公开(公告)号：US3965148A
公开(公告)日：1976-06-22
申请号：US574496
申请日：1975-05-05
申请人： Eduard K. Kleiner , Robert A. Falk
发明人： Eduard K. Kleiner , Robert A. Falk
IPC分类号： C07C149/20
CPC分类号： C07C323/00 , C07C327/00
摘要： Perfluoroalkyl group containing alcohols are disclosed with utility as intermediates for the synthesis of oil and water repellent fluorochemicals. The alcohols are obtained by the addition of mercaptoalcohols to perfluoroalkyl group containing esters of fumaric, maleic, citraconic, mesaconic, itaconic, methylene malonic or aconitic acids.
摘要翻译：公开了含全氟烷基的醇作为合成防油和防水氟化合物的中间体。醇是通过向含全氟烷基的富马酸，马来酸，柠康酸，中康酸，衣康酸，亚甲基丙二酸或乌头酸的酯加成巯基醇得到的。

8. 发明授权

US5502225A Perfluoroalkyl terminated urethane lubricants 失效
标题翻译：全氟烷基封端氨基甲酸酯润滑剂
公开(公告)号：US5502225A
公开(公告)日：1996-03-26
申请号：US972825
申请日：1992-11-09
申请人： Eduard K. Kleiner , Athanasios Karydas
发明人： Eduard K. Kleiner , Athanasios Karydas
IPC分类号： C07C271/12 , C07C271/20 , C07C271/24 , C07C333/04 , C09G3/00 , C10M105/68 , C10M105/72 , C10M133/16 , C10M135/26 , C07C231/00 , C07C261/00
CPC分类号： C07C271/24 , C07C271/12 , C07C271/20 , C07C333/04 , C09G3/00 , C10M105/68 , C10M105/72 , C10M133/16 , C10M135/26 , C07C2101/14 , C10M2201/00 , C10M2201/041 , C10M2201/042 , C10M2201/061 , C10M2201/16 , C10M2201/18 , C10M2205/022 , C10M2205/14 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10M2215/10 , C10M2215/102 , C10M2219/085 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： This invention relates to perfluoroalkyl group terminated urethanes, thiourethanes and ureas of the general formula(R--X--CONH).sub.m Awhere m is 1, 2 or 3, R is R.sub.f -E and optionally R.sub.1 with the proviso that at least one R is R.sub.f -E, R.sub.f is a perfluoroalkyl group, R.sub.1 is a hydrocarbon group, E is a divalent linking group, X is --O--, --S--, --NR.sub.2 -- and R.sub.2 is H or lower alkyl and A is R.sub.f E or R.sub.1 if m is 1 and a divalent or trivalent linking group if m is 2 or 3 respectively.Compounds of this general formula are useful as solid lubricants or as additives for waxes and resins providing lubricating properties.
摘要翻译：本发明涉及通式（RX-CONH）mA的全氟烷基封端的聚氨酯，硫代氨基甲酸酯和脲，其中m为1,2或3，R为R f -E，任选R 1为条件是至少一个R为R f- E，Rf为全氟烷基，R 1为烃基，E为二价连接基团，X为-O-，-S-，-NR2-，R2为H或低级烷基，A为RfE或R1，如果m为 1，如果m分别为2或3，则为二价或三价连接基团。该通式的化合物可用作固体润滑剂或作为提供润滑性能的蜡和树脂的添加剂。

9. 发明授权

US4460480A Protein hydrolyzate compositions for fire fighting containing perfluoroalkyl sulfide terminated oligomers 失效
标题翻译：用于消防的蛋白质水解物组合物，其含有全氟烷基硫化物封端的低聚物
公开(公告)号：US4460480A
公开(公告)日：1984-07-17
申请号：US129872
申请日：1980-03-13
申请人： Eduard K. Kleiner , Thomas W. Cooke , Robert A. Falk
发明人： Eduard K. Kleiner , Thomas W. Cooke , Robert A. Falk
IPC分类号： A62D1/02 , B01F17/00 , C08F2/38 , C11D1/00 , A62D1/00 , C07D211/70 , C07D211/82 , C07D213/56
CPC分类号： C11D1/004 , A62D1/0085 , B01F17/0057 , C08F2/38
摘要： The present invention relates to novel oligomers of the formula R.sub.f --E--S--M.sub.1 ].sub.x [M.sub.2 ].sub.y H, and mixutes thereof, wherein R.sub.f is a perfluoroalkyl group, E is a linkage group, --M.sub.1 -- represents a hydrophilic monomer unit, --M.sub.2 -- represents a hydrophobic monomer unit, x and y represent the number of monomer units present in the novel oligomers. The sum of x and y is between 4 and 500 and x/(x+y) is between 1 and 0.5. The novel oligomers are useful as additives in protein foam type fire fighting compositions improving foam expansion, foam drainage and extinguishing times and reducing flammability of hydrocarbon contaminated protein foams. The novel oligomers are further useful as surface tension depressants providing improved wetting, spreading and leveling properties in aqueous systems.
摘要翻译：本发明涉及式Rf-ES-M1] x [M2] yH的新型低聚物及其混合物，其中Rf为全氟烷基，E为连接基，-M1-表示亲水性单体单元， M2-表示疏水单体单元，x和y表示存在于新型低聚物中的单体单元的数目。 x和y之和在4和500之间，x /（x + y）在1和0.5之间。新型低聚物可用作蛋白质泡沫型消防组合物中的添加剂，其改善泡沫膨胀，泡沫排放和灭火时间并降低碳氢化合物污染的蛋白质泡沫的可燃性。新型低聚物还可用作表面张力抑制剂，其在水性体系中提供改善的润湿，铺展和流平性能。

10. 发明授权

US4136250A Polysiloxane hydrogels 失效
标题翻译：聚硅氧烷氢化物
公开(公告)号：US4136250A
公开(公告)日：1979-01-23
申请号：US817405
申请日：1977-07-20
申请人： Karl F. Mueller , Eduard K. Kleiner
发明人： Karl F. Mueller , Eduard K. Kleiner
IPC分类号： G02C7/04 , A01N25/04 , A01N25/10 , A61K9/70 , A61K47/34 , A61L9/04 , C08F30/08 , C08F212/08 , C08F216/12 , C08F218/04 , C08F218/08 , C08F220/00 , C08F220/18 , C08F230/08 , C08F283/12 , C08F290/00 , C08F290/06 , C08F290/14 , C08F299/00 , C08F299/08 , C08G18/61 , C08G18/67 , C08G77/20 , C08G77/388 , C08G77/42 , C08G77/442 , C08G77/458 , C08L83/04 , C11B9/00 , G02B1/04 , C08G77/04
CPC分类号： G02B1/043 , A01N25/04 , A01N25/10 , A61K47/34 , A61L9/048 , C08F290/068 , C08F290/148 , C08G18/61 , C08G18/671 , C08G2210/00 , Y10S514/944
摘要： A water-insoluble hydrophilic gel comprising (A) about 20 to about 90% by weight of a hydrophilic (a) polymer of identical or different water-soluble monoolefinic monomers, or (b) copolymer of said water-soluble monomers with 1 to 80% (of total monomers) of water-insoluble, identical or different monoolefinic monomers; which polymer or copolymer is cross-linked with (B) about 10 to about 80% by weight of a terminal polyolefinic siloxane macromer having a molecular weight from about 400 to about 8500.

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