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1. 发明授权

US5453554A Process for preparing short chain alkyl aromatic compounds 失效
标题翻译：制备短链烷基芳族化合物的方法
公开(公告)号：US5453554A
公开(公告)日：1995-09-26
申请号：US249609
申请日：1994-05-26
申请人： Jane C. Cheng , Anthony S. Fung , Donald J. Klocke , Stephen L. Lawton , Daria N. Lissy , Wieslaw J. Roth , C. Morris Smith , Dennis E. Walsh
发明人： Jane C. Cheng , Anthony S. Fung , Donald J. Klocke , Stephen L. Lawton , Daria N. Lissy , Wieslaw J. Roth , C. Morris Smith , Dennis E. Walsh
IPC分类号： B01J20/18 , B01J29/03 , B01J29/06 , B01J29/40 , B01J29/70 , C01B33/38 , C01B35/00 , C01B39/00 , C01B39/02 , C01B39/48 , C07C2/66 , C07C15/02 , C10G35/06 , C10G35/095
CPC分类号： B01J29/70 , B01J37/0009 , C01B33/38 , B01J2229/42
摘要： Relatively short chain alkyl aromatic compounds are prepared by alkylating an alkylatable aromatic compound with a relatively short chain alkylating agent under sufficient reaction conditions in the presence of a catalyst comprising zeolite MCM-56. The liquid phase syntheses of ethylbenzene and cumene are particular examples of such MCM-56 catalyzed reactions.
摘要翻译：通过在含有沸石MCM-56的催化剂的存在下，在足够的反应条件下，用相对短链的烷基化剂烷基化可烷基化芳族化合物来制备相对短链烷基芳族化合物。乙苯和枯烯的液相合成是这种MCM-56催化反应的具体实例。

2. 发明授权

US5237121A Highly selective N-olefin isomerization process using microcrystalline ZSM-22 失效
标题翻译：使用微晶ZSM-22的高选择性N-烯烃异构化方法
公开(公告)号：US5237121A
公开(公告)日：1993-08-17
申请号：US925442
申请日：1992-08-11
申请人： Iraj Rahmim , Albin Huss, Jr. , Daria N. Lissy , Donald J. Klocke , Ivy D. Johnson
发明人： Iraj Rahmim , Albin Huss, Jr. , Daria N. Lissy , Donald J. Klocke , Ivy D. Johnson
IPC分类号： C07C5/27
CPC分类号： C07C5/2775
摘要： A process is disclosed for the highly selective skeletal isomerization of linear olefin-containing organic feeds to iso-olefins at high levels of feed conversion wherein linear olefins, e.g., n-butenes, are contacted with catalyst comprising ZSM-22 having a crystal size whose largest dimension is no greater than 0.5 micron. The process is carried out under isomerization conditions to produce iso-olefins of corresponding carbon number, e.g., isobutene. High overall iso-olefin yields thus can be obtained, even at relatively low temperatures.
摘要翻译：公开了一种用于在高水平进料转化率下将含线性烯烃的有机原料高度选择性骨架异构化成异烯烃的方法，其中线性烯烃例如正丁烯与包含ZSM-22的催化剂接触，ZSM-22的晶体尺寸最大尺寸不大于0.5微米。该方法在异构化条件下进行以产生相应碳数的异烯烃，例如异丁烯。即使在相对较低的温度下也能获得高的全部异烯烃收率。

3. 发明授权

US5053374A Method for preparing a zeolite catalyst bound with a refractory oxide of low acidity 失效
$Method for preparing a zeolite catalyst bound with a refractory oxide of low acidity$
标题翻译：制备与低酸度的难熔氧化物结合的沸石催化剂的方法
公开(公告)号：US5053374A
公开(公告)日：1991-10-01
申请号：US431002
申请日：1989-11-02
申请人： Robert P. L. Absil , Philip J. Angevine , Joseph A. Herbst , Donald J. Klocke , John P. McWilliams , Scott Han , David S. Shihabi
发明人： Robert P. L. Absil , Philip J. Angevine , Joseph A. Herbst , Donald J. Klocke , John P. McWilliams , Scott Han , David S. Shihabi
IPC分类号： B01J29/08 , B01J29/70 , B01J37/00
CPC分类号： B01J37/0009 , B01J29/084 , B01J29/7007
摘要： Low acidity refractory oxide-bound zeolite catalysts, for example, silica-bound ultrastable Y zeolite, possessing physical properties, e.g., crush strength, similar to those of their alumina-bound counterparts are described. Since low acidity refractory oxide-bound catalysts are inherently less active than alumina-bound zeolite catalysts, the former are particularly useful in hydrocarbon conversion processes in which reduced coke make increases catalyst cycle length. Due to their stability in acid environments, the low acidity refractory oxide-bound zeolite extrudate herein can be acid treated without unduly compromising its structural integrity.
摘要翻译：描述了具有类似于其氧化铝结合的对应物的物理性能，例如粉碎强度的低酸度难熔氧化物结合的沸石催化剂，例如二氧化硅结合的超稳定Y沸石。由于低酸度难熔氧化物结合的催化剂固有地比氧化铝结合的沸石催化剂具有更低的活性，因此前者在烃转化方法中特别有用，其中减少的焦炭使催化剂循环长度增加。由于其在酸性环境中的稳定性，本文中低酸度难熔氧化物结合的沸石挤出物可以进行酸处理，而不会不利地损害其结构完整性。

4. 发明授权

US4617288A Low nitrogen iron-containing Fischer-Tropsch catalyst for conversion of synthesis gas and process for preparing the catalyst 失效
标题翻译：用于转化合成气的低含氮铁的费 - 托催化剂和用于制备催化剂的方法
公开(公告)号：US4617288A
公开(公告)日：1986-10-14
申请号：US687695
申请日：1984-12-31
申请人： Weldon K. Bell , Werner O. Haag , Garry W. Kirker , Donald J. Klocke
发明人： Weldon K. Bell , Werner O. Haag , Garry W. Kirker , Donald J. Klocke
IPC分类号： B01J23/745 , B01J23/75 , B01J23/80 , B01J23/881 , B01J23/89 , C07C1/04 , B01J23/72 , B01J23/85
CPC分类号： B01J23/745 , B01J23/75 , B01J23/80 , B01J23/881 , B01J23/8906 , C07C1/0445 , C07C2521/02 , C07C2523/04 , C07C2523/06 , C07C2523/26 , C07C2523/28 , C07C2523/44 , C07C2523/72 , C07C2523/745 , C07C2523/75
摘要： Synthesis gas (a mixture of hydrogen gas and carbon monoxide) is converted to hydrocarbons by flowing the gas first over iron-containing Fischer-Tropsch catalyst and then over a zeolite. The Fischer-Tropsch catalyst contains relatively little nitrogen as a result of its preparation by continuous precipitation at a pH ranging from about 6.6 to 6.9 and a temperature ranging from about 80.degree. to about 100.degree. C.
摘要翻译：将气体首先流过含铁费 - 托催化剂，然后通过沸石，将合成气（氢气和一氧化碳的混合物）转化成烃。由于其在约6.6至6.9的pH和约80至约100℃的温度下连续沉淀制备，费 - 托催化剂含有相对较少的氮。

5. 发明授权

US07038100B2 Aromatics alkylation 有权
公开(公告)号：US07038100B2
公开(公告)日：2006-05-02
申请号：US09845856
申请日：2001-04-30
申请人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
发明人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/085
摘要： The present invention provides a process for producing an alkylaromatic compound comprising the step of contacting an alkylatable aromatic compound with an alkylating agent under alkylation conditions in the presence of a alkylation catalyst comprising phosphorus and a porous crystalline inorganic oxide material having an X-ray diffraction pattern including the d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom.

6. 发明授权

US5554274A Manufacture of improved catalyst 失效
标题翻译：改良催化剂的制造
公开(公告)号：US5554274A
公开(公告)日：1996-09-10
申请号：US325838
申请日：1994-10-19
申请人： Thomas F. Degnan , Donald J. Klocke , Mae K. Rubin
发明人： Thomas F. Degnan , Donald J. Klocke , Mae K. Rubin
IPC分类号： B01J29/08 , B01J29/40 , B01J29/80 , C10G11/05 , C10G47/02
CPC分类号： B01J29/80 , C10G11/05 , B01J2229/26 , B01J2229/42 , B01J29/088 , B01J29/40
摘要： This invention relates the use of a catalyst composition having the structure of ZSM-5 and a matrix material, which has been manufactured by a new and useful method, for organic compound, e.g., hydrocarbon compound, conversion. The organic compound conversion processes described include catalytic cracking, gasoline hydrofinishing, toluene disproportionation, xylene isomerization, and ethylbenzene production.
摘要翻译：本发明涉及具有ZSM-5结构的催化剂组合物和通过新的和有用的方法制造的基质材料用于有机化合物例如烃化合物转化的用途。所述的有机化合物转化方法包括催化裂化，汽油加氢精制，甲苯歧化，二甲苯异构化和乙苯生产。

7. 发明授权

US5523511A Highly selective n-olefin isomerization process using low zeolite content ZSM-35 catalyst 失效
标题翻译：使用低沸石含量的ZSM-35催化剂的高选择性正烯烃异构化方法
公开(公告)号：US5523511A
公开(公告)日：1996-06-04
申请号：US228779
申请日：1994-04-18
申请人： Claus-Peter Haelsig , Albin Huss, Jr. , Donald J. Klocke , Daria N. Lissy , Iraj I. Rahmim
发明人： Claus-Peter Haelsig , Albin Huss, Jr. , Donald J. Klocke , Daria N. Lissy , Iraj I. Rahmim
IPC分类号： B01J29/65 , B01J29/70 , C07C5/27
CPC分类号： B01J29/65 , B01J29/7042 , B01J29/7046 , C07C5/2775 , B01J2229/26 , B01J2229/42
摘要： A process is disclosed for the highly selective skeletal isomerization of linear olefin-containing organic feeds to iso-olefins at high levels of feed conversion wherein linear olefins, e.g., n-butenes, are contacted with catalyst comprising ZSM-35 under skeletal isomerization conditions which can include temperatures of 100.degree. to 750.degree. C. and linear olefin space velocities of less than 30 WHSV. The process uses a catalyst composition comprising 5 to 40 wt % ZSM-35, and 60 to 95 wt % inorganic oxide matrix, e.g., silica.
摘要翻译：公开了一种用于在高水平进料转化率下将含线性烯烃的有机原料高度选择性骨架异构化为异烯烃的方法，其中线性烯烃例如正丁烯在骨架异构化条件下与包含ZSM-35的催化剂接触，可以包括100℃至750℃的温度和低于30WHSV的线性烯烃空速。该方法使用包含5至40重量％的ZSM-35和60至95重量％的无机氧化物基质如二氧化硅的催化剂组合物。

8. 发明授权

US5369071A Manufacture of improved catalyst 失效
标题翻译：改良催化剂的制造
公开(公告)号：US5369071A
公开(公告)日：1994-11-29
申请号：US988992
申请日：1992-12-11
申请人： Thomas F. Degnan , Donald J. Klocke , Mae K. Rubin
发明人： Thomas F. Degnan , Donald J. Klocke , Mae K. Rubin
IPC分类号： B01J29/08 , B01J29/40 , B01J29/80 , C10G11/05 , B01J29/28
CPC分类号： C10G11/05 , B01J29/80 , B01J2229/26 , B01J2229/42 , B01J29/088 , B01J29/40
摘要： This invention relates to a new and useful method for manufacturing a catalyst composition comprising a crystalline molecular sieve having the structure of ZSM-5 and a matrix material, the new catalyst composition, and use of the new catalyst composition in accordance herewith as a catalyst component for organic compound, e.g., hydrocarbon compound, conversion.
摘要翻译：本发明涉及一种新的有用的制造催化剂组合物的方法，该催化剂组合物包括具有ZSM-5结构的结晶分子筛和基质材料，新的催化剂组合物，以及根据本发明的新的催化剂组合物作为催化剂组分用于有机化合物，例如烃化合物，转化。

9. 发明授权

US5240892A Small crystal ZSM-5, as a catalyst 失效
标题翻译：小晶体ZSM-5，作为催化剂
公开(公告)号：US5240892A
公开(公告)日：1993-08-31
申请号：US823408
申请日：1992-01-21
申请人： Donald J. Klocke
发明人： Donald J. Klocke
IPC分类号： C01B39/38
CPC分类号： C01B39/38 , Y10S423/22
摘要： A process for preparing, in the absence of organic directing agent, a porous crystalline silicate having the structure of ZSM-5 having a sorption capacity for mesitylene of at least about 3 weight percent which comprises:a) providing a crystallization reaction mixture which includes a source of at least one component of crystalline silicate framework element, including silicon, wherein the solids content of said source in the crystallization reaction mixture is at least 35 weight percent;b) maintaining the crystallization temperature at less than about 250.degree. C.c) maintaining agitation conditions during crystallization sufficient to result in said crystal size;d) maintaining a mole ratio of OH.sup.- /SiO.sub.2 in the reaction mixture of at least about 0.11; ande) recovering porous crystalline silicate crystals.
摘要翻译：在不存在有机导向剂的情况下制备具有至少约3重量％的均三甲苯的吸附容量的ZSM-5结构的多孔结晶硅酸盐的方法，其包括：a）提供结晶反应混合物，其包含至少一种结晶硅酸盐骨架元素组分的源，包括硅，其中所述结晶反应混合物中所述源的固体含量为至少35重量％; b）保持结晶温度低于约250℃。c）在结晶期间保持搅拌条件足以导致所述晶体尺寸; d）保持反应混合物中OH- / SiO 2的摩尔比至少约为0.11; 和e）回收多孔结晶硅酸盐晶体。

10. 发明授权

US4985223A Crystalline aluminosilicate 失效
标题翻译：结晶硅铝酸盐
公开(公告)号：US4985223A
公开(公告)日：1991-01-15
申请号：US651149
申请日：1984-09-17
申请人： Pochen Chu , Joseph A. Herbst , Donald J. Klocke , James Vartuli
发明人： Pochen Chu , Joseph A. Herbst , Donald J. Klocke , James Vartuli
IPC分类号： B01J29/70 , B01J29/86 , C01B39/12 , C01B39/48 , C07C1/20
CPC分类号： C01B39/12 , B01J29/70 , B01J29/86 , C01B39/48 , C07C1/20 , B01J2229/20 , B01J2229/36 , C07C2529/06 , C07C2529/86
摘要： There is provided an aluminum-containing aluminosilicate zeolite corresponding to the substantially aluminum free silicate zeolite described in the Hinnenkamp et al U.S. Pat. No. 4,376,757. Also provided are methods for making this aluminosilicate zeolite and methods for the catalytic conversion of organic charges to desired products with this aluminosilicate zeolite.
摘要翻译：提供对应于Hinnenkamp等人的美国专利中描述的基本上不含铝的硅酸盐沸石的含铝硅铝酸盐沸石。 4,376,757。还提供了制备该硅铝酸盐沸石的方法和用该硅铝酸盐沸石将有机电荷催化转化为所需产物的方法。

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