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1. 发明专利

SK278660B6 SYNTHETIC ZEOLITE AND PREPARATION METHOD THEREOF 未知
公开(公告)号：SK278660B6
公开(公告)日：1997-12-10
申请号：SK256790
申请日：1990-05-25
申请人： POCHEN CHU , MAE KOENIG RUBIN
发明人： POCHEN CHU , MAE KOENIG RUBIN
IPC分类号： B01J29/04 , C01B39/00
摘要： This patent is dealing with synthetic zeolite, a character of which is seen based on the X-ray diagram, represented by the values described in the table I and this zeolite is prepared based on the reaction mixture containing YO2/X2O3 = 10 up to 80, H20/YO2 = 5 up to 100, OH/YO2 = 0,01 up to 1,0 M/YO2 = 0,01 up to 2,0, R/YO2=0,05 up to 1,0, while these measures are expressed in molar ratio, and where R means hexamethylenimine and M alkaline metal or metal closed to alkaline earth, where the resource of Y oxide contains minimum 30 weight percent of the solid YO2 and this reaction mixture is being kept at the temperature of 80 up to 300 Celsius degrees, for 24 hours up to 60 days, until the crystals closed to the above mentioned material are not created.

2. 发明授权

US5334795A Production of ethylbenzene 失效
标题翻译：生产乙苯
公开(公告)号：US5334795A
公开(公告)日：1994-08-02
申请号：US967954
申请日：1992-10-27
申请人： Pochen Chu , Michael E. Landis , Quang N. Le
发明人： Pochen Chu , Michael E. Landis , Quang N. Le
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/70
摘要： Ethylbenzene is produced by the alkylation of benzene with ethylene in the presence of an alkylation catalyst having a particular structure defined by its X-ray diffraction pattern. A preferred catalyst is the zeolite MCM-22. The process is typically carried out at a temperature of 300.degree. to 1000.degree. F. but the catalyst provides sufficient activity for the reaction to be carried out at temperatures below 700.degree. F. Liquid phase operation is preferred, giving a lower yield of polyethylated products. The use of the selected catalyst also results in a reduction of the xylene impurity level to values below 500 ppm in the product.
摘要翻译：在具有由其X射线衍射图形定义的特定结构的烷基化催化剂存在下，通过苯与乙烯的烷基化生产乙苯。优选的催化剂是沸石MCM-22。该方法通常在300至1000°F的温度下进行，但催化剂提供足够的活性以使反应在低于700°F的温度下进行。液相操作是优选的，从而降低聚乙烯化产物的产率。使用所选择的催化剂还导致二甲苯杂质水平降低到产品中低于500ppm的值。

3. 发明授权

US5179054A Layered cracking catalyst and method of manufacture and use thereof 失效
标题翻译：层状裂化催化剂及其制造方法和用途
公开(公告)号：US5179054A
公开(公告)日：1993-01-12
申请号：US735225
申请日：1991-07-24
申请人： Paul H. Schipper , Hartley Owen , Joseph A. Herbst , Garry W. Kirker , Albin Huss, Jr. , Pochen Chu
发明人： Paul H. Schipper , Hartley Owen , Joseph A. Herbst , Garry W. Kirker , Albin Huss, Jr. , Pochen Chu
IPC分类号： B01J33/00 , C10G11/05
CPC分类号： B01J33/00 , C10G11/05 , B01J2229/12 , B01J2229/42 , C10G2300/70
摘要： A layered catalyst suited to the catalytic cracking of heavy feeds comprises a core and a shell. The shell comprises at least 5 wt % of at least 1 molecular sieve having openings of at least 8 angstroms. The core comprises at least 10 wt % of at least 1 molecular sieve having openings comprising a 12 or less-membered ring and has a reduced, if any, content of said molecular sieve having openings of at least 8 angstroms, relative to its concentration in the shell. Suitable molecular sieve materials having openings of at least 8 angstroms include MCM-41, VPI-5, MCM-9 and layered metal oxides, e.g., pillared clays. The required molecular sieve of the core can include zeolite Y, Ultrastable Y or intermediate pore size zeolites such as ZSM-5. The shell which may further contain a metals passivator can act as a metals sink, and can remove metals from the unit by attrition. The catalyst is preferably prepared by forming the core and then coating or encapsulating the core with a shell material. The shell may also comprise an attritable coating of an amorphous rare earth oxide, aluminum oxide and aluminum phosphate composite, which traps metals.
摘要翻译：适用于重料的催化裂化的层状催化剂包括核和壳。该壳包含至少5重量％的具有至少8埃的开口的至少1个分子筛。核心包含至少10重量％的具有包含12个或更少元环的开口的至少1个分子筛，并且具有至少8埃的开口的所述分子筛的含量降低（如果有的话），相对于其浓度贝壳。具有至少8埃开口的合适的分子筛材料包括MCM-41，VPI-5，MCM-9和层状金属氧化物，例如柱状粘土。核心所需的分子筛可包括沸石Y，超稳定Y或中等孔径沸石如ZSM-5。可以进一步包含金属钝化剂的壳体可以用作金属沉槽，并且可以通过磨损从单元中去除金属。催化剂优选通过形成核心然后用壳材料涂覆或包封核心来制备。外壳还可以包含捕获金属的无定形稀土氧化物，氧化铝和磷酸铝复合材料的可磨损涂层。

4. 发明授权

US5140949A Zeolite-clay composition and uses thereof 失效
公开(公告)号：US5140949A
公开(公告)日：1992-08-25
申请号：US758668
申请日：1991-09-12
申请人： Pochen Chu , William E. Garwood
发明人： Pochen Chu , William E. Garwood
IPC分类号： A23K1/175 , B01J20/16 , B01J20/18
CPC分类号： B01J20/18 , A23K20/28 , B01J20/16
摘要： A hydrous aluminosilicate adsorbent composition in which the active adsorbent is a mixture of non-fibrous clay with non-fibrous zeolite. The composition is useful as a feed supplement in animal husbandry, and as a topical adsorbent for veterinary use. The mixture has a high capacity for adsorption of ammonium cations, and a synergistically high selectivity for their adsorption. Beneficial effects as feed supplement may arise from lowering the amount of ammonia passed to the liver from the alimentary canal.

5. 发明授权

US5026943A Catalytic conversion over catalyst comprising synthetic crystal MCM-35 失效
标题翻译：催化剂催化转化，包括合成晶体MCM-35
公开(公告)号：US5026943A
公开(公告)日：1991-06-25
申请号：US587837
申请日：1990-09-25
申请人： Mae K. Rubin , Pochen Chu
发明人： Mae K. Rubin , Pochen Chu
IPC分类号： B01J29/04 , B01J29/70 , C01B39/48 , C07C2/66 , C07C63/34
CPC分类号： C07C2/66 , B01J29/041 , B01J29/70 , C01B35/1009 , C01B39/48 , B01J2229/26 , B01J2229/42
摘要： This invention relates to catalytic conversion of organic compounds over MCM-35, a new crystalline material exhibiting a distinctive X-ray diffraction pattern. The conversion process includes the mechanisms of cracking, hydrocracking, dewaxing, dehydrogenation and aromatic alkylation.
摘要翻译：本发明涉及有机化合物对MCM-35的催化转化，MCM-35是一种具有独特X射线衍射图的新型结晶材料。转化过程包括裂化，加氢裂化，脱蜡，脱氢和芳族烷基化的机理。

6. 发明授权

US4919787A Metal passivating agents 失效
标题翻译：金属钝化剂
公开(公告)号：US4919787A
公开(公告)日：1990-04-24
申请号：US335069
申请日：1989-04-07
申请人： Arthur W. Chester , Pochen Chu , Albin Huss, Jr. , Garry W. Kirker
发明人： Arthur W. Chester , Pochen Chu , Albin Huss, Jr. , Garry W. Kirker
IPC分类号： B01J33/00 , C10G11/05
CPC分类号： B01J33/00 , C10G11/05 , B01J2229/12 , B01J2229/42 , C10G2300/70 , Y10S502/521
摘要： An improved method for passivating metals in a hydrocarbon feedstock during catalytic cracking has been discovered. The method involves contacting the feedstock with a passivating agent comprising a precipitated porous rare earth oxide, alumina, and aluminum phosphate precipitate. The passivating agent may be coated on a cracking catalyst, be part of the matrix of a cracking catalyst, or be added to the cracking operation as discrete particles.
摘要翻译：已经发现了一种在催化裂化过程中钝化烃原料中的金属的改进方法。该方法包括使原料与包含沉淀的多孔稀土氧化物，氧化铝和磷酸铝沉淀物的钝化剂接触。钝化剂可以涂覆在裂化催化剂上，作为裂化催化剂的基质的一部分，或作为离散颗粒加入到裂化操作中。

7. 发明授权

US4899007A Aromatic conversion reactions with zeolitic catalyst composition of improved shape selectivity 失效
标题翻译：具有改进的形状选择性的沸石催化剂组合物的芳族转化反应
公开(公告)号：US4899007A
公开(公告)日：1990-02-06
申请号：US679673
申请日：1984-12-10
申请人： Pochen Chu , Francis G. Dwyer , Albert B. Schwartz
发明人： Pochen Chu , Francis G. Dwyer , Albert B. Schwartz
IPC分类号： B01J29/40 , B01J29/46 , C07C2/66 , C07C6/12 , C07C15/00
CPC分类号： C07C6/123 , B01J29/40 , B01J29/46 , C07C2/66 , B01J2229/20 , B01J2229/26 , B01J2229/36 , B01J2229/42 , C07C2529/46 , C07C2529/68 , C07C2529/76
摘要： There are provided aromatic conversion reactions for preparation of dialkyl benzenes, such as xylene and ethyltoluene, of enhanced para isomer content with a zeolitic catalyst composition of improved shape selectivity. The catalysts comprise certain zeolites which have been calcined at a high temperature of at least 649.degree. C. (i.e., 1200.degree. F.). These zeolites have a silica/alumina ratio of at least about 12 and a constraint index within the approximate range of 1 to 12. Examples of such zeolites include ZSM-5 and ZSM-11.
摘要翻译：提供芳族转化反应，用于制备具有改进的形状选择性的沸石催化剂组合物，具有增强的对位异构体含量的二烷基苯如二甲苯和乙基甲苯。催化剂包括已在至少649℃（即1200°F）的高温下煅烧的某些沸石。这些沸石的二氧化硅/氧化铝比至少约为12，约束指数在1至12的近似范围内。这种沸石的实例包括ZSM-5和ZSM-11。

8. 发明授权

US4898662A Catalytic cracking process using high equilibrium activity additive catalyst 失效
标题翻译：催化裂化工艺采用高平衡活性添加剂催化剂
公开(公告)号：US4898662A
公开(公告)日：1990-02-06
申请号：US264577
申请日：1988-10-31
申请人： Pochen Chu , Sadi Mizrahi
发明人： Pochen Chu , Sadi Mizrahi
IPC分类号： B01J29/40 , C10G11/05
CPC分类号： B01J29/40 , C10G11/05 , B01J2229/26 , B01J2229/36 , B01J2229/42
摘要： A catalytic cracking process is disclosed in which octane improvement is attained by the addition to conventional cracking catalysts of small amounts of additive catalyst comprising a class of zeolites characterized by a silica to alumina mole ratio greater than about 12 and a Constraint Index of about 1 to 12 bound in a matrix chosen such that the matrix component forms a thermodynamically favored compound with selected cations. Sustained catalytic activity is achieved by pre-exchanging the catalyst to a high level of selected cation loading. By extending the active life of the additive catalyst, markedly lower makeup catalyst addition rates are required.
摘要翻译：公开了一种催化裂解方法，其中通过加入少量添加剂催化剂的常规裂化催化剂来实现辛烷值改进，所述催化剂包含一类沸石，其特征在于二氧化硅与氧化铝的摩尔比大于约12，约束指数为约1至 12以选定的矩阵结合，使得基质组分与选择的阳离子形成热力学上有利的化合物。通过将催化剂预交换为高水平的选择的阳离子负载来实现持续的催化活性。通过延长添加剂催化剂的活性，需要显着降低催化剂添加量。

9. 发明授权

US4778666A Crystallization method employing microwave radiation 失效
标题翻译：使用微波辐射的结晶方法
公开(公告)号：US4778666A
公开(公告)日：1988-10-18
申请号：US937809
申请日：1986-12-04
申请人： Pochen Chu , Francis G. Dwyer , James C. Vartuli
发明人： Pochen Chu , Francis G. Dwyer , James C. Vartuli
IPC分类号： B01D20060101 , B01J20060101 , C01B25/36 , C01B25/45 , C01B37/04 , C01B39/02 , C01B39/14 , C01B39/38 , C01B39/40 , C01B33/20 , C01B33/26 , C01B33/28
CPC分类号： C01B39/40 , C01B33/2884 , C01B35/1009 , C01B37/04 , C01B39/02 , C01B39/14 , C01B39/38 , Y10S423/21 , Y10S423/22 , Y10S423/23 , Y10S423/24 , Y10S423/28 , Y10S423/29 , Y10S423/33 , Y10S423/35 , Y10S423/36
摘要： A crystallization process employing microwave energy is described. The process is especially useful in the manufacture of porous crystalline materials.
摘要翻译：描述了采用微波能量的结晶过程。该方法在制造多孔结晶材料中特别有用。

10. 发明授权

US4743572A Magnesia-alumina-aluminum phosphate catalyst and catalyst product thereof 失效
标题翻译：氧化镁 - 铝 - 磷酸铝催化剂及其催化剂产物
公开(公告)号：US4743572A
公开(公告)日：1988-05-10
申请号：US938476
申请日：1986-12-05
申请人： Philip J. Angevine , Pochen Chu , Thomas F. Degnan , Garry W. Kirker
发明人： Philip J. Angevine , Pochen Chu , Thomas F. Degnan , Garry W. Kirker
IPC分类号： B01J27/18 , B01J27/16 , B01J27/185 , B01J32/00 , B01J35/10 , B01J37/03 , C10G45/04 , C10G47/10 , B01J29/06 , B01J27/14
CPC分类号： B01J37/03 , B01J29/84 , B01J35/10 , B01J35/1014 , B01J35/1019 , B01J35/1042 , B01J35/1047 , B01J35/108
摘要： This invention relates to a method of preparing a metal-containing amorphous magnesia-alumina-aluminum phosphate catalyst support involving the admixture of an organic cation having a size equal to or greater than 2 Angstroms, the organic cation preferably being a tertiary or a tetraalkylammonium or phosphonium cation, the method permits recovery of a catalyst support having a controlled pore size distribution. The invention also relates to an improved catalytic support as well as an improved petroleum residua upgrading process comprising hydrotreating residua in the presence of the improved catalyst support.

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