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1. 发明申请

US20150044128A1 DEACIDIFICATION PROCESS AND APPARATUS THEREOF 有权
标题翻译：防腐方法及其设备
公开(公告)号：US20150044128A1
公开(公告)日：2015-02-12
申请号：US14362076
申请日：2012-03-23
申请人： Chunlei Wu , Xianjian Duan , Chengkun Long , Yuelin Wang
发明人： Chunlei Wu , Xianjian Duan , Chengkun Long , Yuelin Wang
IPC分类号： F27D17/00 , F27D1/00 , B01J19/00
CPC分类号： F27D17/001 , B01D46/0068 , B01D53/40 , B01D53/685 , B01D2257/2045 , B01J19/00 , C01B33/12 , C01B33/18 , F23J15/02 , F23J2217/101 , F27D1/0033
摘要： A deacidification apparatus and a deacidification process using the apparatus are disclosed. The deacidification apparatus includes a deacidification furnace, of which a furnace upper section, a furnace middle section and a furnace lower section are provided in upper, middle and lower portions respectively, wherein a gas-solid mixture inlet (1), a exhaust outlet (3) and a filtered air port (2) are provided on the furnace upper section, a product outlet (13) is provided on the furnace lower section, the upper portion of the deacidification is mounted with a filter (5) to which the gas-solid mixture inlet (1), the exhaust outlet (2) and the filtered air port (3) are connected, the filtered air port (2) is connected with a gas pulse device and a vacuum device by a three-way connecting device, and the exhaust outlet (3) is connected with atmosphere or connected with the vacuum device.
摘要翻译：公开了一种使用该装置的脱酸装置和脱酸方法。脱酸装置包括脱酸炉，其分别在上部，中部和下部设置炉上部，炉中部和炉下部，其中气固混合物入口（1），排气出口 3）和过滤空气口（2）设置在炉上部，在炉下部设置有产品出口（13），脱酸装置的上部安装有过滤器（5），气体固体混合物入口（1），排气出口（2）和过滤空气口（3）连接，过滤空气口（2）通过三通连接装置与气体脉冲装置和真空装置连接，排气口（3）与大气连接或与真空装置连接。

2. 发明授权

US08765988B2 Lycopene intermediate 1, 3, 6, 10-tetra-double bond pentadec-carbon phosphonate as well as preparation method and use thereof 有权
标题翻译：番茄红素中间体1,3,6,10-四 - 双十五碳酸膦酸酯及其制备方法和用途
公开(公告)号：US08765988B2
公开(公告)日：2014-07-01
申请号：US13583635
申请日：2011-03-09
申请人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Yibin Wu , Liujiang Hu
发明人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Yibin Wu , Liujiang Hu
IPC分类号： C07F9/40
CPC分类号： C07F9/4015
摘要： The invention relates to a novel important lycopene intermediate 3,7,11-trimethyl-1,3,6,10-tetraene-dodecyl diethyl phosphonate. A current lycopene intermediate 2,4,6,10-tetra-double bond pentadec-carbon phosphonate is difficult to synthesize. The invention provides a novel intermediate, which has the following synthesis steps of: preparing 2,6,10-trimethyl-3,5,9-undecane triene-1-aldehyde from pseudoionone; preparing 2,6,10-trimethyl-2,5,9-undecane triene-1-aldehyde from the 2,6,10-trimethyl-3,5,9-undecane triene-1-aldehyde; and subjecting the 2,6,10-trimethyl-2,5,9-undecane triene-1-aldehyde and tetraethyl methylenediphosphonate to condensation reaction to obtain target product. The invention can generate novel intermediate from raw material pseudoionone only by four reactions, thus the reactions are easy to control and great industrial value are achieved.
摘要翻译：本发明涉及新型重要的番茄红素中间体3,7,11-三甲基-1,3,6,10-四烯十二烷基二乙基膦酸酯。目前的番茄红素中间体2,4,6,10-四 - 双十五碳酸膦难以合成。本发明提供了一种新的中间体，其具有以下合成步骤：由假雄酮制备2,6,10-三甲基-3,5,9-十一烷三烯-1-醛; 由2,6,10-三甲基-3,5,9-十一烷三烯-1-醛制备2,6,10-三甲基-2,5,9-十一烷三烯-1-醛; 并使2,6,10-三甲基-2,5,9-十一烷三烯-1-醛和四亚乙基二膦酸四乙酯进行缩合反应，得到目标产物。本发明只能通过四个反应从原料假雄酮生成新的中间体，因此反应易于控制，实现了巨大的工业价值。

3. 发明授权

US10527014B2 Demount-free electrical cleanable filter 有权
公开(公告)号：US10527014B2
公开(公告)日：2020-01-07
申请号：US15469605
申请日：2017-03-27
申请人： Chunlei Wu
发明人： Chunlei Wu
IPC分类号： F02M37/22 , B08B1/00 , B07B1/52 , B01D29/58 , B01D29/64 , B01D29/33 , B01D46/00 , B08B7/00
摘要： The present invention relates to a demount-free electrical cleanable filter, which includes a housing and a main filter cylinder in the housing. the housing is provided with a cleaning hoop and a reciprocating driving device. The cleaning hoop is sleeved on cylinder filtering material of the main filter cylinder. The reciprocating driving device drives the cleaning hoop to move up and down repeatedly, so as to conduct a clean-up operation on the main filter cylinder. The beneficial effect of the present invention is as follows. The present invention can be used in vehicle using fuel, engine and industry, environmental filtering, according to the flow rate and different designs of material. By a novel structure design, the lifetime of the present filter is greatly improved. During the entire life cycle of the filter, an apparatus which uses the present filter does not need to replace the fuel filter.

4. 发明申请

US20120316366A1 Method of Preparing 2,6,10-Trimethyl-1,1-Dialkoxy-3,5,9-Undecatriene Used as an Intermediate of Lycopene 有权
标题翻译：制备用作番茄红素中间体的2,6,10-三甲基-1,1-二烷氧基-3,5,9-十一碳三烯的方法
公开(公告)号：US20120316366A1
公开(公告)日：2012-12-13
申请号：US13493971
申请日：2012-06-11
申请人： PENGFEI ZHANG , CHAO SHEN , RUNPU SHEN , WEI LIU , CHUNLEI WU
发明人： PENGFEI ZHANG , CHAO SHEN , RUNPU SHEN , WEI LIU , CHUNLEI WU
IPC分类号： C07C41/01
CPC分类号： C07C41/48 , C07C43/303
摘要： The present invention describes a novel synthetic method for preparing the key intermediate 2,6,10-trimethyl-1,1-dialkoxy-3,5,9-undecatriene of lycopene. An existing synthetic method have some disadvantages that it is very difficult to gain the raw material dialkyl 4-methyl-5,5-diakoxy-1-pentene-1-phosphonate (10) because no effective synthetic method can be adopted, and furthermore the obtained target compound is composed of several cis/trans isomers. This invention relates to a process comprising a condensation step wherein a starting C10-phosphonate is changed to its carbanion completely at a temperature of −40˜30 under an atmosphere of a non-reactive gas in an organic solvent catalyzed by base, and then C4-dialkyl is added to undergo Wittig-Horner condensation. This invention affords all trans C14-acetal and this method is characterized with the advantages of simple procedure, easy access to raw material and low cost, which makes it has the value of industrial application.
摘要翻译：本发明描述了一种制备番茄红素关键中间体2,6,10-三甲基-1,1-二烷氧基-3,5,9-十一碳三烯的新型合成方法。现有的合成方法有一些缺点，因为没有有效的合成方法，难以获得原料的4-甲基-5,5-二烷氧基-1-戊烯-1-膦酸二烷基酯（10），此外，得到的目标化合物由几种顺式/反式异构体组成。本发明涉及一种包括缩合步骤的方法，其中起始C10-膦酸酯在-40〜30℃的温度下在非反应性气体的气氛中在由碱催化的有机溶剂中完全变成其碳负离子，然后将C4 加入二烷基以进行Wittig-Horner冷凝。本发明提供全反式C14-缩醛，该方法的特点是操作简单，易于获得原料，成本低廉，具有工业应用价值。

5. 发明授权

US08697919B2 1-methoxyl-2, 6, 10-trimethyl-1, 3, 5, 9-undec-tetraene, and preparation method and uses thereof 有权
标题翻译： 1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯及其制备方法和用途
公开(公告)号：US08697919B2
公开(公告)日：2014-04-15
申请号：US13639852
申请日：2011-04-06
申请人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Xiongsheng Sun , Siping Hu
发明人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Xiongsheng Sun , Siping Hu
IPC分类号： C07C45/42 , C07C41/30 , C07C43/15
CPC分类号： C07C43/16 , C07C41/30 , C07C45/42 , C07C47/21
摘要： The invention discloses an intermediate 1-methoxyl-2,6,10-trimethyl-1,3,5, 9-undec-tetraene, and a preparation method and uses thereof. In the synthesis method for the current lycopene intermediate 2-pos double bond C-14 aldehyde (2,6,10-trimethyl-2,5,9-undecatriene-1-aldehyde), expensive methyl iodide, polluting dimethyl sulphide and dangerous strong base are needed, so that the method is hardly applied to industrial production. The invention provides a new compound 1-methoxyl-2,6,10-trimethyl-1,3,5,9-undec-tetraene, and pure 2-pos double bond C-14 aldehyde can be prepared by hydrolyzing and refining the compound. The synthetic route is simplified and the great suitability for industrial production is achieved.
摘要翻译：本发明公开了中间体1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯及其制备方法和用途。在目前番茄红素中间体2-pos双键C-14醛（2,6,10-三甲基-2,5,9-十一碳三烯-1-醛）的合成方法中，昂贵的甲基碘，污染二甲基硫化物和危险的强需要这种方法，这种方法几乎不适用于工业生产。本发明提供了一种新的化合物1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯，纯的2-位双键C-14醛可以通过水解和精制化合物。合成路线简化，实现了工业生产的良好适应性。

6. 发明授权

US08536361B2 1,4,6,10-tetra-double bond pentadec-carbon phosphonate, preparation method thereof, and preparation method of lycopene using the same 有权
标题翻译： 1,4,6,10-四 - 双键十五碳酸膦酸酯，其制备方法以及使用其的番茄红素的制备方法
公开(公告)号：US08536361B2
公开(公告)日：2013-09-17
申请号：US13576659
申请日：2011-01-30
申请人： Runpu Shen , Weidong Ye , Shiqing Pi , Xuejun Lao , Luo Liu , Xiaohua Song , Chunlei Wu , Zhigang Wu
发明人： Runpu Shen , Weidong Ye , Shiqing Pi , Xuejun Lao , Luo Liu , Xiaohua Song , Chunlei Wu , Zhigang Wu
IPC分类号： C07F9/142
CPC分类号： C07F9/4015 , C07C1/34 , C07C11/21
摘要： 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4), and preparation method thereof are provided. The preparation method comprises: reacting a pseudo ionone of formula (2) with sulfonium salt to prepare a epoxide of formula (9), and then reacting the epoxide of formula (9) with magnesium bromide to prepare a C-14 aldehyde of formula (3); condensing the C-14 aldehyde of formula (3) with tetra-alkyl methylene diphosphonate to obtain 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4). Furthermore, the preparation method of lycopene via 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4) is also provided. The present method has the advantages of short route, easily obtained raw materials, and low cost.
摘要翻译：提供式（4）的1,4,6,10-四 - 双十五碳 - 碳膦酸酯及其制备方法。制备方法包括：使式（2）的假紫罗酮与锍盐反应以制备式（9）的环氧化物，然后使式（9）的环氧化物与溴化镁反应以制备式（C） 3）; 将式（3）的C-14醛缩合成四烷基亚甲基二膦酸盐，得到式（4）的1,4,6,10-四 - 双十五碳酸膦酸酯。此外，还提供了通式（4）的1,4,6,10-四 - 双十五碳碳酸膦酸酯的番茄红素的制备方法。本发明方法路线短，原料易得，成本低。

7. 发明申请

US20130046114A1 1-Methoxyl-2, 6, 10-Trimethyl-1, 3, 5, 9-Undec-Tetraene, and Preparation Method and Uses thereof 有权
标题翻译： 1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯及其制备方法和用途
公开(公告)号：US20130046114A1
公开(公告)日：2013-02-21
申请号：US13639852
申请日：2011-04-06
申请人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Xiongsheng Sun , Siping Hu
发明人： Xuejun Lao , Runpu Shen , Weidong Ye , Xiaohua Song , Luo Liu , Chunlei Wu , Xiongsheng Sun , Siping Hu
IPC分类号： C07C41/30 , C07C43/15 , C07C45/42
CPC分类号： C07C43/16 , C07C41/30 , C07C45/42 , C07C47/21
摘要： The invention discloses an intermediate 1-methoxyl-2,6,10-trimethyl-1,3,5,9-undec-tetraene, and a preparation method and uses thereof. In the synthesis method for the current lycopene intermediate 2-pos double bond C-14 aldehyde (2,6,10-trimethyl-2,5,9-undecatriene-1-aldehyde), expensive methyl iodide, polluting dimethyl sulphide and dangerous strong base are needed, so that the method is hardly applied to industrial production. The invention provides a new compound 1-methoxyl-2,6,10-trimethyl-1,3,5,9-undec-tetraene, and pure 2-pos double bond C-14 aldehyde can be prepared by hydrolyzing and refining the compound. The synthetic route is simplified and the great suitability for industrial production is achieved.
摘要翻译：本发明公开了中间体1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯及其制备方法和用途。在目前番茄红素中间体2-pos双键C-14醛（2,6,10-三甲基-2,5,9-十一碳三烯-1-醛）的合成方法中，昂贵的甲基碘，污染二甲基硫化物和危险的强需要这种方法，这种方法几乎不适用于工业生产。本发明提供了一种新的化合物1-甲氧基-2,6,10-三甲基-1,3,5,9-十一四烯，纯的2-位双键C-14醛可以通过水解和精制化合物。合成路线简化，实现了工业生产的良好适应性。

8. 发明申请

US20120310002A1 1,4,6,10-Tetra-Double Bond Pentadec-Carbon Phosphonate, Preparation Method Thereof, And Preparation Method Of Lycopene Using The Same 有权
标题翻译： 1,4,6,10-四 - 双键十五碳膦酸酯及其制备方法及其使用番茄红素的制备方法
公开(公告)号：US20120310002A1
公开(公告)日：2012-12-06
申请号：US13576659
申请日：2011-01-30
申请人： Runpu Shen , Weidong Ye , Shiqing Pi , Xuejun Lao , Luo Liu , Xiaohua Song , Chunlei Wu , Zhigang Wu
发明人： Runpu Shen , Weidong Ye , Shiqing Pi , Xuejun Lao , Luo Liu , Xiaohua Song , Chunlei Wu , Zhigang Wu
IPC分类号： C07C1/34 , C07F9/40
CPC分类号： C07F9/4015 , C07C1/34 , C07C11/21
摘要： 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4), and preparation method thereof are provided. The preparation method comprises: reacting a pseudo ionone of formula (2) with sulfonium salt to prepare a epoxide of formula (9), and then reacting the epoxide of formula (9) with magnesium bromide to prepare a C-14 aldehyde of formula (3); condensing the C-14 aldehyde of formula (3) with tetra-alkyl methylene diphosphonate to obtain 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4). Furthermore, the preparation method of lycopene via 1,4,6,10-tetra-double bond pentadec-carbon phosphonate of formula (4) is also provided. The present method has the advantages of short route, easily obtained raw materials, and low cost.
摘要翻译：提供式（4）的1,4,6,10-四 - 双十五碳 - 碳膦酸酯及其制备方法。制备方法包括：使式（2）的假紫罗酮与锍盐反应以制备式（9）的环氧化物，然后使式（9）的环氧化物与溴化镁反应以制备式（C） 3）; 将式（3）的C-14醛缩合成四烷基亚甲基二膦酸盐，得到式（4）的1,4,6,10-四 - 双十五碳酸膦酸酯。此外，还提供了通式（4）的1,4,6,10-四 - 双十五碳碳酸膦酸酯的番茄红素的制备方法。本发明方法路线短，原料易得，成本低。

9. 发明申请

US20170356337A1 DEMOUNT-FREE ELECTRICAL CLEANABLE FILTER 审中-公开
公开(公告)号：US20170356337A1
公开(公告)日：2017-12-14
申请号：US15469605
申请日：2017-03-27
申请人： Chunlei WU
发明人： Chunlei WU
IPC分类号： F02B77/04 , B01D46/00 , B08B7/00 , F02M37/22
CPC分类号： F02M37/22 , B01D29/33 , B01D29/58 , B01D29/64 , B01D29/6484 , B01D46/00 , B07B1/526 , B08B1/008 , B08B7/00
摘要： The present invention relates to a demount-free electrical cleanable filter, which includes a housing and a main filter cylinder in the housing. the housing is provided with a cleaning hoop and a reciprocating driving device. The cleaning hoop is sleeved on cylinder filtering material of the main filter cylinder. The reciprocating driving device drives the cleaning hoop to move up and down repeatedly, so as to conduct a clean-up operation on the main filter cylinder. The beneficial effect of the present invention is as follows. The present invention can be used in vehicle using fuel, engine and industry, environmental filtering, according to the flow rate and different designs of material. By a novel structure design, the lifetime of the present filter is greatly improved. During the entire life cycle of the filter, an apparatus which uses the present filter does not need to replace the fuel filter.

10. 发明授权

US09273905B2 Deacidification process and apparatus thereof 有权
标题翻译：脱酸方法及其装置
公开(公告)号：US09273905B2
公开(公告)日：2016-03-01
申请号：US14362076
申请日：2012-03-23
申请人： Chunlei Wu , Xianjian Duan , Chengkun Long , Yuelin Wang
发明人： Chunlei Wu , Xianjian Duan , Chengkun Long , Yuelin Wang
IPC分类号： B01D53/40 , B01D53/68 , B01D46/00 , C01B33/12 , C01B33/18 , B01J19/00 , F27D17/00 , F23J15/02 , F27D1/00
CPC分类号： F27D17/001 , B01D46/0068 , B01D53/40 , B01D53/685 , B01D2257/2045 , B01J19/00 , C01B33/12 , C01B33/18 , F23J15/02 , F23J2217/101 , F27D1/0033
摘要： A deacidification apparatus and a deacidification process using the apparatus are disclosed. The deacidification apparatus includes a deacidification furnace, of which a furnace upper section, a furnace middle section and a furnace lower section are provided in upper, middle and lower portions respectively, wherein a gas-solid mixture inlet (1), a exhaust outlet (3) and a filtered air port (2) are provided on the furnace upper section, a product outlet (13) is provided on the furnace lower section, the upper portion of the deacidification is mounted with a filter (5) to which the gas-solid mixture inlet (1), the exhaust outlet (2) and the filtered air port (3) are connected, the filtered air port (2) is connected with a gas pulse device and a vacuum device by a three-way connecting device, and the exhaust outlet (3) is connected with atmosphere or connected with the vacuum device.
摘要翻译：公开了一种使用该装置的脱酸装置和脱酸方法。脱酸装置包括脱酸炉，其分别在上部，中部和下部设置炉上部，炉中部和炉下部，其中气固混合物入口（1），排气出口 3）和过滤空气口（2）设置在炉上部，在炉下部设置有产品出口（13），脱酸装置的上部安装有过滤器（5），气体固体混合物入口（1），排气出口（2）和过滤空气口（3）连接，过滤空气口（2）通过三通连接装置与气体脉冲装置和真空装置连接，排气口（3）与大气连接或与真空装置连接。

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