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    • 1. 发明申请
    • METHOD AND APPARATUS TO PRODUCE PULP USING PRE-HYDROLYSIS AND KRAFT COOKING
    • 使用预水解和克拉夫烹饪生产纸浆的方法和装置
    • US20120211183A1
    • 2012-08-23
    • US13363680
    • 2012-02-01
    • Aaron LEAVITTJussi PakarinenBrian F. Greenwood
    • Aaron LEAVITTJussi PakarinenBrian F. Greenwood
    • D21C3/00D21C7/10
    • D21C1/04D21C3/02D21C3/24
    • A pulp cooking system including: a cellulosic material feed system, a pre-hydrolysis reactor vessel and a Kraft cooking reactor vessel. The feed material system includes a steaming chip bin and a high pressure transfer device. The pre-hydrolysis reactor vessel maintains the feed material in a mildly acidic condition and allows hydrolysate to be extracted through screens below a hydrolysis zone in the vessel. A wash zone is below the screens and allows wash liquid to flow through the feed material in a cross-current direction. The wash liquid and hydrolysate removed from the feed material is extracted through the screens. The feed material is maintained in a mildly acidic condition through the pre-hydrolysis reactor vessel until the material enters the Kraft cooking vessel where the feed material is treated with alkaline cooking liquors.
    • 一种纸浆蒸煮系统,包括:纤维素材料进料系统,预水解反应器容器和硫酸盐蒸煮反应器容器。 进料系统包括蒸汽屑仓和高压输送装置。 预水解反应器容器将进料保持在温和的酸性状态,并允许水解物通过容器中水解区下方的筛网提取。 洗涤区位于筛网的下面,并允许洗涤液体在横向电流方向上流过进料。 从进料中除去的洗涤液和水解物通过筛子提取。 饲料通过预水解反应器容器保持在温和的酸性状态,直到材料进入硫酸盐蒸煮容器,其中饲料用碱性烹饪液处理。
    • 2. 发明授权
    • Method for steaming comminuted cellulosic fibrous material during
continuous solvent pulping
    • 在连续溶剂制浆期间蒸粉碎的纤维素纤维材料的方法
    • US5865948A
    • 1999-02-02
    • US473194
    • 1995-06-07
    • Jairo H. LoraJohn Patrick MaleyBrian F. GreenwoodJoseph R. PhillipsDavid J. Lebel
    • Jairo H. LoraJohn Patrick MaleyBrian F. GreenwoodJoseph R. PhillipsDavid J. Lebel
    • D21C3/18D21C1/02D21C3/20D21C3/22D21C3/24D21C7/00D21C7/14D21C9/02D21C9/04D21C11/00
    • D21C1/02D21C11/00D21C3/20D21C3/24D21C7/00D21C9/02D21C9/04
    • A continuous solvent pulping process is practiced with oxygen free gas (e.g. nitrogen) purges of all major treatment vessels during the time when the process is arrested or terminated. The wood chips or other cellulosic fibrous material to be pulped is steamed in a first horizontal steaming zone at pressure of about 10-20 psi, and then in a second horizontal steaming zone at a pressure of about 20-75 psi. The first and second zones are isolated by a low pressure feeder. Steam is introduced into the material in the second steaming zone to flow cocurrently with it. Gases, including vaporized solvent (e.g. ethanol or other alcohol) are vented from the steaming zones, and solvent is added to the steamed material prior to feeding to a high pressure feeder. The high pressure feeder introduces the material into the top of a single digesting vessel, liquid and chips being separated at the top of the digester vessel without mechanical means that could cause a spark. Lignin containing liquid is withdrawn from a central portion of the digester and passed through flash tanks and ultimately for lignin and alcohol recovery. A recirculating screen and system is disposed between the central extraction portion and the top of the digester vessel. A portion of the liquid removed for recirculation is instead passed to lignin recovery, while fresh solvent containing liquid is added to the rest of the recirculated liquid.
    • 连续溶剂制浆过程在所有主要处理容器的无氧气体(如氮气)清洗过程被捕获或终止的时间内进行。 要制浆的木屑或其他纤维素纤维材料在约10-20psi压力的第一卧式蒸汽区中蒸汽,然后在约20-75psi压力的第二卧式蒸汽区中蒸汽。 第一和第二区域由低压进料器隔离。 蒸汽被引入第二蒸汽区中的材料以与其并流流动。 气体,包括蒸发的溶剂(例如乙醇或其他醇)从蒸汽区域排出,并且在进料到高压进料器之前将溶剂加入到蒸汽材料中。 高压给料器将材料引入单个消化容器的顶部,液体和碎屑在蒸煮器容器的顶部分离,而不会引起火花的机械装置。 含木质素的液体从消化器的中心部分排出并通过闪蒸罐,最终用于木质素和酒精回收。 再循环筛网和系统设置在中央提取部分和蒸煮器容器的顶部之间。 取代用于再循环的一部分液体被转移到木质素回收中,同时将含有新鲜溶剂的液体加入剩余的再循环液体中。
    • 5. 发明授权
    • Medium consistency pulp ozone bleaching
    • 中等稠度纸浆臭氧漂白
    • US5411633A
    • 1995-05-02
    • US693287
    • 1991-04-30
    • Joseph R. PhillipsBrian F. GreenwoodErwin FunkStephen Dunn
    • Joseph R. PhillipsBrian F. GreenwoodErwin FunkStephen Dunn
    • D21C9/153
    • D21C9/153
    • Medium consistency (e.g. about 6-15%) paper pulp is effectively bleached with ozone in a carrier gas (typically oxygen) by effecting efficient separation of carrier gas from the pulp after reaction with the ozone, and introducing the ozone into the pulp at a pressure of about 10-13 bar. Ozone in oxygen and medium consistency paper pulp are fed to a fluidizing mixer; the intimate uniform mixture produced is then passed upwardly in a reaction vessel until about 99% of the ozone has been consumed, and then separation of gas from the pulp is initiated by moving the pulp mixture into a generally horizontal tube leading to a gas zone in a large diameter retention vessel. A pressurized gas pad is maintained at and above the introduction of the pulp into the retention vessel, while the level of pulp in the retention vessel is maintained below the point of introduction. The pulp may be withdrawn from the retention vessel with a fluidizing degassing pump, and the pressurized gas removed from the top of the vessel may be fed to an apparatus using oxygen gas under pressure.
    • 中等稠度(例如约6-15%)纸浆通过在与臭氧反应后有效地从纸浆中分离出载体气体(通常为氧气)中,用臭氧有效漂白,并将臭氧引入到纸浆中 压力约10-13巴。 将氧气和中等稠度纸浆中的臭氧进料到流化混合器中; 然后将产生的紧密的均匀混合物在反应容器中向上通入,直到约99%的臭氧消耗掉,然后通过将纸浆混合物移动到通向一个气体区域的气体区域中而从纸浆中分离气体 大直径保留容器。 加压气垫保持在纸浆引入到保留容器中和之上,而保留容器中的纸浆水平保持在引入点以下。 纸浆可以用流化脱气泵从保留容器中取出,并且从容器顶部除去的加压气体可以在压力下使用氧气进料至设备。
    • 9. 发明授权
    • Medium consistency ozone bleaching
    • 中等稠度臭氧漂白
    • US5411634A
    • 1995-05-02
    • US710439
    • 1991-06-07
    • Kaj HenricsonJoseph PhillipsBrian F. GreenwoodErwin D. FunkStephen J. Dunne
    • Kaj HenricsonJoseph PhillipsBrian F. GreenwoodErwin D. FunkStephen J. Dunne
    • D21C9/10D21C9/153
    • D21C9/153
    • In a method of bleaching medium consistency pulp with ozone using a mixer, ozone containing gas and about 6-15% consistency pulp are fed to the mixer, and then discharged in a first, preferably vertical, path. The mixture of pulp and ozone moves in a first part of the vertical path a time period of about 1-5 seconds at a velocity of about 1-5 m/s so that the gas and pulp do not separate during movement in this first part, and the vast majority of the pulp brightening reaction between the ozone and pulp takes place. This is preferably accomplished by passing the mixture upwardly in a small diameter conduit having a height of about 3-20 meters. Then the velocity of the pulp is slowed while still moving in the first path, preferably by feeding it directly to a much larger diameter (e. g. 1.5-10 times) conduit, so the height of the unit may be kept under 100 feet. The pulp flows in the large diameter conduit for about 0.5-5 minutes so that residual reactions take place.
    • 在使用混合器将具有臭氧的中等稠度纸浆漂白的方法中,将含臭氧的气体和约6-15%浓度的纸浆送入混合器中,然后以第一,优选垂直的路径排出。 纸浆和臭氧的混合物以约1-5m / s的速度在垂直路径的第一部分中移动大约1-5秒的时间段,使得气体和纸浆在该第一部分的运动期间不分离 ,并且发生了臭氧和纸浆之间绝大多数纸浆增白反应。 这优选通过将混合物向上通过高度为约3-20米的小直径导管来完成。 然后,纸浆的速度在第一路径中仍然运动时减速,优选通过将其直接送入更大直径(例如1.5-10倍)的导管,因此该单元的高度可以保持在100英尺以下。 纸浆在大直径导管中流动约0.5-5分钟,从而发生残留反应。