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1. 发明授权

US5527877A Sinterable semi-crystalline powder and near-fully dense article formed therewith 失效
公开(公告)号：US5527877A
公开(公告)日：1996-06-18
申请号：US298076
申请日：1994-08-30
申请人： Elmer D. Dickens, Jr. , Biing L. Lee , Glenn A. Taylor , Angelo J. Magistro , Hendra Ng , Kevin McAlea , Paul F. Forderhase
发明人： Elmer D. Dickens, Jr. , Biing L. Lee , Glenn A. Taylor , Angelo J. Magistro , Hendra Ng , Kevin McAlea , Paul F. Forderhase
IPC分类号： C08L101/00 , B29C35/08 , B29C41/00 , B29C67/00 , B29C67/04 , B29K23/00 , B29K77/00 , C08G69/14 , C08J3/12 , C08J9/24 , C08L23/04 , C08L23/10 , C08L23/26 , C08L59/00 , C08L77/00
CPC分类号： C08J3/12 , B29C41/003 , B29C67/0077 , B29C67/04 , C08J9/24 , B29C2035/0838 , B29K2023/00 , B29K2023/06 , B29K2023/12 , B29K2059/00 , B29K2067/006 , B29K2077/00 , B29K2079/00 , B29K2995/0094 , Y10S521/919 , Y10S525/902 , Y10T428/249958 , Y10T428/249986 , Y10T428/252
摘要： A laser-sinterable powder product has been prepared having unique properties which allow the powder to be sintered in a selective laser sintering machine to form a sintered part which is near-fully dense. For most purposes, the sintered part is indistinguishable from another part having the same dimensions made by isotropically molding the powder. In addition to being freely flowable at a temperature near its softening temperature, a useful powder is disclosed that has a two-tier distribution in which substantially no primary particles have an average diameter greater than 180 .mu.m, provided further that the number average ratio of particles smaller than 53 .mu.m is greater than 80%, the remaining larger particles being in the size range from 53 .mu.m to 180 .mu.m. A powder with slow recrystallization rates, as evidenced by non-overlapping endothermic and exothermic peaks in their differential scanning calorimetry characteristics for scan rates of on the order of 10.degree. C. to 20.degree. C. per minute, will also result in sintered parts that are near-fully dense, with minimal dimensional distortion.

2. 发明授权

US5733497A Selective laser sintering with composite plastic material 失效
标题翻译：选择性激光烧结与复合塑料材料
公开(公告)号：US5733497A
公开(公告)日：1998-03-31
申请号：US527840
申请日：1995-09-13
申请人： Kevin P. McAlea , Paul F. Forderhase , Mark E. Ganninger , Frederic W. Kunig , Angelo J. Magistro
发明人： Kevin P. McAlea , Paul F. Forderhase , Mark E. Ganninger , Frederic W. Kunig , Angelo J. Magistro
IPC分类号： C08J9/24 , B29C39/00 , B29C41/00 , B29C67/00 , B29C67/20 , B29K105/04 , C08J9/32 , C08K7/20 , C08L77/00 , C08L101/00 , B29C35/08 , B29C41/02
CPC分类号： C08K7/20 , B29C39/003 , B29C41/003 , B29C67/0077
摘要： A composite powder specially adapted for use in selective laser sintering is disclosed. The composite powder includes a polymer powder dry mixed with a reinforcement powder, where the polymer powder has a melting temperature substantially lower than that of the reinforcement powder. In the case where nearfully dense parts are to be formed, the first constituent powder is preferably a semi-crystalline powder, for example nylon 11, of a composition suitable for forming near-fully dense parts when used unblended in selective laser sintering; if porous parts are desired, the polymer powder is an amorphous powder, such as polycarbonate, polystyrene, acrylates, and styrene/acrylate copolymers. The reinforcement powder is preferably microspheres of glass, preferably coated to enhance wetting and adhesion with the polymer powder when selective laser sintering is performed. Besides improving the stiffness and heat resistance of the part produced, the composite powder widens the process window over that provided by unblended powder, provides improved dimensional accuracy in the part produced, and facilitates roughbreakout and smooth finishing of the part produced.
摘要翻译：公开了一种特别适用于选择性激光烧结的复合粉末。复合粉末包括与增强粉末混合的聚合物粉末，其中聚合物粉末的熔融温度基本上低于加强粉末的熔融温度。在要形成接近密集部分的情况下，第一组分粉末优选为半结晶粉末，例如尼龙11，适合于在选择性激光烧结中未掺杂时形成近乎致密部分的组合物; 如果需要多孔部分，聚合物粉末是无定形粉末，例如聚碳酸酯，聚苯乙烯，丙烯酸酯和苯乙烯/丙烯酸酯共聚物。增强粉末优选是玻璃微球体，优选涂覆以在选择性激光烧结时增强与聚合物粉末的润湿性和粘合性。除了提高所生产部件的刚度和耐热性之外，复合材料粉末使工艺窗口比非混合粉末提高了加工窗口的尺寸，提高了产品尺寸精度，并促进了生产部件的破裂和光滑整理。

3. 发明授权

US5178938A Composition for adhesion of polyurethane-coated nylon fabrics 失效
标题翻译：聚氨酯涂层尼龙织物的粘合组合物
公开(公告)号：US5178938A
公开(公告)日：1993-01-12
申请号：US680225
申请日：1991-04-04
申请人： Angelo J. Magistro , Phillip S. Neal
发明人： Angelo J. Magistro , Phillip S. Neal
IPC分类号： B32B7/12 , C09J175/04
CPC分类号： C09J175/04 , B32B7/12 , Y10T428/31562 , Y10T428/31739 , Y10T442/365 , Y10T442/3854
摘要： Aromatic mono-, di-, or trihydroxy compounds are used alone or containing peel strength-improving additives, in association with a polyurethane adhesive, for adhering a polyurethane-coated nylon fabric to another polyurethane-coated nylon fabric to form a polyurethane-coated nylon composite, and for adhering a nylon fabric coated with an aluminum flake-containing polyurethane to a polyurethane-coated nylon fabric. Additionally, aromatic mono-, di-, or trihydroxy compounds are utilized in association with a polyurethane adhesive for forming a lamina composition comprising a polyurethane film adhered to a nylon fabric.
摘要翻译：芳族单 - ，二 - 或三羟基化合物单独使用或含有剥离强度改进添加剂，与聚氨酯粘合剂相结合，用于将聚氨酯涂覆的尼龙织物粘附到另一种聚氨酯涂覆的尼龙织物上以形成聚氨酯涂覆的尼龙复合材料，并将用含铝薄片的聚氨酯涂覆的尼龙织物粘附到聚氨酯涂覆的尼龙织物上。此外，芳香族单 - ，二 - 或三羟基化合物与聚氨酯粘合剂一起使用，用于形成包含粘附到尼龙织物上的聚氨酯膜的薄片组合物。

4. 发明授权

US5087791A Process for the preparation of ethylene and vinyl chloride from ethane in the presence of water 失效
标题翻译：在水存在下由乙烷制备乙烯和氯乙烯的方法
公开(公告)号：US5087791A
公开(公告)日：1992-02-11
申请号：US615193
申请日：1990-11-19
申请人： Angelo J. Magistro
发明人： Angelo J. Magistro
IPC分类号： C07C5/48
CPC分类号： C07C5/48 , Y02P20/52
摘要： Ethylene is prepared in an oxydehydrogenation reaction of ethane by contacting a charge amount of ethane, an oxygen source, a chlorine source and water in the presence of a solid solution catalyst at an effective temperature. A low yield of vinyl chloride and a high yield of ethylene are obtained at a high ethane conversion.

5. 发明授权

US5304329A Method of recovering recyclable unsintered powder from the part bed of a selective laser-sintering machine 失效
标题翻译：从选择性激光烧结机床部分回收可回收的未烧结粉末的方法
公开(公告)号：US5304329A
公开(公告)日：1994-04-19
申请号：US980003
申请日：1992-11-23
申请人： Elmer D. Dickens, Jr. , Glenn A. Taylor , Frederic W. Kunig , Angelo J. Magistro , Eric M. Weissman , Timothy R. Hradek
发明人： Elmer D. Dickens, Jr. , Glenn A. Taylor , Frederic W. Kunig , Angelo J. Magistro , Eric M. Weissman , Timothy R. Hradek
IPC分类号： B29C67/00 , B29C35/08
CPC分类号： B29C67/0077
摘要： This method teaches how to recover and reuse a powder of a thermally degradable material which is used in a selective laser sintering (SLS) process. To recycle such a laser-sinterable powder successfully in a SLS machine it is protected against degradation by cooling the hot bed while layer-upon-layer (layer-wise) of powder is being sintered, seriatim, to form successive slices fused together to form an article of arbitrary shape (part). The process requires maintaining the powder which has more than 80% of the number of particles
摘要翻译：该方法教导了如何回收和再利用用于选择性激光烧结（SLS）工艺的可热降解材料的粉末。为了在SLS机器中成功地回收这样的可激光烧结粉末，通过冷却热床来保护其免受降解，同时层压（层）上的粉末被烧结，形成连续的切片，以形成熔合在一起形成任意形状的文章（部分）。该方法需要将具有超过80％的颗粒数量（m 3）的颗粒保持为静止床，其仍然是足够多孔的，以允许冷却气体向下流动穿过床而不破坏其表面。由于每个切片形成在表面，并且部件在其形成时被支撑在绝热的床中，与切片相邻的粉末的温度比床的其余部分中的粉末高得多，但是对于冷却气体，会过热。过热粉末不仅会降解，而且会熔化到热部件的表面，形成“成长”，从而使零件不能用于其预定目的。该方法允许经济地将未使用的粉末从床中回收到灭绝。如果粉末在热时也对氧气敏感，则使用惰性气体作为冷却气体。

6. 发明授权

US5112793A Catalyst composition for the preparation of ethylene from ethane 失效
标题翻译：用于从乙烷制备乙烯的催化剂组合物
公开(公告)号：US5112793A
公开(公告)日：1992-05-12
申请号：US691647
申请日：1991-04-25
申请人： Angelo J. Magistro
发明人： Angelo J. Magistro
IPC分类号： B01J23/78 , B01J23/86 , B01J23/889 , C07C5/48 , C07C17/154
CPC分类号： C07C5/48 , B01J23/78 , B01J23/862 , B01J23/864 , B01J23/8892 , C07C17/154 , Y02P20/52
摘要： Solid solution catalyst in particulate form consisting of attrition resistant .alpha.-Al.sub.2 O.sub.3 particles with 0.5 to 10% by weight, expressed as the oxide, of iron cations substituted for aluminum cations in said catalyst support stabilized with 0.5 to 10% by weight, expressed as the oxide, of lanthanum and modified with at least two, preferably three, metal cations selected from the metals consisting of chromium, cobalt, magnesium, manganese, and barium; wherein one of said metal cations is barium and said catalyst has X-ray diffraction pattern with peak positions different than that of the .alpha.-Al.sub.2 O.sub.3 structure. A process is disclosed which produces ethylene from ethane while producing reduced amounts of vinyl chloride from said ethane to ethylene process.
摘要翻译：以0.5至10重量％稳定的以所述催化剂载体中的阳离子取代的阳离子的铁阳离子为0.5-10重量％，表示为氧化物的耐磨性α-Al2O3颗粒组成的颗粒形式的固溶体催化剂，以氧化物，并用选自铬，钴，镁，锰和钡的金属中的至少两种，优选三种金属阳离子进行改性; 其中所述金属阳离子之一是钡，所述催化剂具有不同于α-Al 2 O 3结构的峰位的X射线衍射图。公开了一种从乙烷生产乙烯，同时从所述乙烷生产减少量的氯乙烯至乙烯工艺的方法。

7. 发明授权

US4874858A Triazine-containing multisilane coupling agents for coating glass fibers, for adhesives, and for protective coatings 失效
标题翻译：用于涂覆玻璃纤维，用于粘合剂和保护涂层的含有三嗪的多硅烷偶联剂
公开(公告)号：US4874858A
公开(公告)日：1989-10-17
申请号：US173898
申请日：1988-03-28
申请人： Angelo J. Magistro
发明人： Angelo J. Magistro
IPC分类号： C08J5/08 , C03C25/10 , C03C25/40 , C07F7/18 , C08K5/544 , C09D7/12 , C09J11/06 , C09J175/04 , C09J201/00
CPC分类号： C08K5/5442 , C03C25/40 , C07F7/182 , C09J175/04
摘要： At least three, and as many as eighteen, most preferably at least nine, crosslinking sites are provided through the alkoxy groups in multiple chains on a triazine ring (hence "multisilane"), on a single molecule of the multisilane. The multisilane, useful as a coupling agent, is formed by reacting a triazine-containing compound with a suitable aminoalkyl-alkoxysilane, or, alkyl-aminoalkyl-alkoxysilane in either an anhydrous, or an aqueous liquid medium. A size containing the multisilane, enhances the reinforced properties of organic synthetic resinous materials in which the fibers are used, and most particularly those of rigid poly(vinyl chloride) (PVC) with which it provides cohesive bonding of glass fiber surfaces. Glass fibers coated with a basic film former and the multisilane are covalently bonded on the one hand through some of at least nine alkoxy groups on each of the multisilane molecules, to Si atoms of a glass surface, and on the other hand, through at least some of the amine groups on each of the molecules, to the vinyl chloride (VC) resin in a reaction which involves allylic chloride bonds in the VC resin. The multisilane is effective in adhesives for a wide variety of materials, and in protective coatings.

8. 发明授权

US4339620A Copper-catalyzed fluid-bed ethylene oxhydrochlorination process 失效
标题翻译：铜催化流化床乙烯氯化氢过程
公开(公告)号：US4339620A
公开(公告)日：1982-07-13
申请号：US239806
申请日：1981-03-02
申请人： Joseph A. Cowfer , Jamal S. Eden , Angelo J. Magistro
发明人： Joseph A. Cowfer , Jamal S. Eden , Angelo J. Magistro
IPC分类号： B01J23/72 , C07C17/156 , C07C17/15
CPC分类号： B01J23/72 , C07C17/156
摘要： There is disclosed a method and composition for improving the fluidization characteristics and alleviating or inhibiting stickiness in a supported cupric chloride catalyst used as fluid bed catalyst in oxyhydrochlorinations reactions. The method involves the in situ preparation of the supported cupric chloride catalyst by addition of bare support on which no cupric chloride is deposited to the supported cupric chloride catalyst in the fluidized bed, or the use in the bed as the initial charge or as addition to the bed as makeup, of a composition which is a mixture of supported cupric chloride catalyst and bare support. In either event, as the oxyhydrochlorination proceeds, a portion of the cupric chloride on the supported catalyst becomes released therefrom and deposited in situ on the bare support, and stickiness of the cupric chloride containing catalyst particles to one another in the fluid bed is alleviated or inhibited.
摘要翻译：公开了一种改善流化特性并减轻或抑制用于羟基氢氯化反应中作为流化床催化剂的负载型氯化铜催化剂中的粘性的方法和组合物。该方法包括通过添加裸式载体来原位制备负载的氯化铜催化剂，其上没有将氯化铜沉积在流化床中的负载的氯化铜催化剂上，或者在床中用作初始电荷或作为添加作为化妆品的床，作为负载的氯化铜催化剂和裸支撑物的混合物的组合物。在任一情况下，随着氧化氢氯化的进行，载体催化剂上的一部分氯化铜被释放出来，并在裸露的载体上原位沉积，并且在流化床中彼此含有氯化铜的催化剂颗粒的粘性得到缓解或抑制。

9. 发明授权

US4158645A Catalyst for the preparation of ethylene and vinyl chloride from ethane 失效
标题翻译：用于从乙烷制备乙烯和氯乙烯的催化剂
公开(公告)号：US4158645A
公开(公告)日：1979-06-19
申请号：US887166
申请日：1978-03-16
申请人： Angelo J. Magistro
发明人： Angelo J. Magistro
IPC分类号： B01J23/83 , C07C5/48 , C07C17/154 , B01J21/04 , B01J23/10 , B01J23/74 , B01J23/84
CPC分类号： C07C5/48 , B01J23/83 , C07C17/154 , Y02P20/52
摘要： Ethane is reacted with oxygen and a chlorine source in the presence of a solid solution catalyst containing iron cations which is stabilized with lanthanum and/or lanthanides and modified with selected metal cations, to yield ethylene, vinyl chloride, and other valuable by-products. Conversion of ethane to products approaches 100 percent, ethylene is prepared in up to 90 mole percent yield, and the combined yield of ethylene, vinyl chloride and ethyl chloride is over 90 mole percent.
摘要翻译：在含有铁阳离子的固溶体催化剂的存在下，乙烷与氧和氯源反应，该铁阳离子用镧和/或镧系元素稳定并用选择的金属阳离子改性，得到乙烯，氯乙烯和其它有价值的副产物。乙烷转化成产物接近100％，乙烯的产率高达90％，乙烯，氯乙烯和乙基氯的合并产率高于90％。

10. 发明授权

US5210358A Catalyst composition and process for the preparation of ethylene from ethane 失效
标题翻译：催化剂组合物和从乙烷制备乙烯的方法
公开(公告)号：US5210358A
公开(公告)日：1993-05-11
申请号：US842869
申请日：1992-02-27
申请人： Angelo J. Magistro
发明人： Angelo J. Magistro
IPC分类号： B01J23/78 , B01J23/86 , B01J23/889 , C07C5/48 , C07C17/154
CPC分类号： C07C5/48 , B01J23/78 , B01J23/862 , B01J23/864 , B01J23/8892 , C07C17/154 , Y02P20/52
摘要： Solid solution catalyst in particulate form consisting of attrition resistant .alpha.-Al.sub.2 0.sub.3 particles with 0.5 to 10% by weight, expressed as the oxide, of iron cations substituted for aluminum cations in said catalyst support stabilized with 0.5 to 10% by weight, expressed as the oxide, of lanthanum and modified with at least two, preferably three, metal cations selected from the metals consisting of chromium, cobalt, magnesium, manganese, and barium; wherein one of said metal cations is barium and said catalyst has X-ray diffraction pattern with peak positions different than that of the .alpha.-Al.sub.2 0.sub.3 structure. A process is disclosed which produces ethylene from ethane while producing reduced amounts of vinyl chloride from said ethane to ethylene process.
摘要翻译：颗粒形式的固溶体催化剂由0.5％至10％（重量比）的耐摩擦α-Al 2 O 3颗粒组成，其中0.5-10％（重量），表示为氧化物，在所述催化剂载体中取代铝阳离子的铁阳离子以0.5至10重量％稳定，表示为氧化物，并用选自铬，钴，镁，锰和钡的金属中的至少两种，优选三种金属阳离子进行改性; 其中所述金属阳离子之一是钡，所述催化剂具有与α-Al 2 O 3结构的峰位置不同的X射线衍射图。公开了一种从乙烷生产乙烯，同时从所述乙烷生产减少量的氯乙烯至乙烯工艺的方法。

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