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81. 发明授权

US09493355B2 Solvent-based methods for production of graphene nanoribbons 有权
标题翻译：用于生产石墨烯纳米带的基于溶剂的方法
公开(公告)号：US09493355B2
公开(公告)日：2016-11-15
申请号：US14345016
申请日：2012-09-14
申请人： James M. Tour , Wei Lu , Bostjan Genorio
发明人： James M. Tour , Wei Lu , Bostjan Genorio
IPC分类号： C01B31/02 , C07C29/32 , C08F112/08 , C01B31/04
CPC分类号： C08F112/08 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B32/178 , C01B32/18 , C01B32/184 , C01B32/194 , C01B2202/06 , C01B2204/06 , C07C2/76 , C07C15/56 , C07C29/32 , C07C67/035 , C07C69/76 , D01F9/12 , Y10S977/734 , Y10S977/846 , Y10S977/961
摘要： The present invention provides methods of preparing functionalized graphene nanoribbons. Such methods include: (1) exposing a plurality of carbon nanotubes (CNTs) to an alkali metal source in the presence of an aprotic solvent to open them; and (2) exposing the opened CNTs to an electrophile to form functionalized graphene nanoribbons (GNRs). The methods may also include a step of exposing the opened CNTs to a protic solvent to quench any reactive species on them. Additional methods include preparing unfunctionalized GNRs by: (1) exposing a plurality of CNTs to an alkali metal source in the presence of an aprotic solvent to open them; and (2) exposing the opened CNTs to a protic solvent to form unfunctionalized GNRs.
摘要翻译：本发明提供了制备官能化石墨烯纳米带的方法。这些方法包括：（1）在非质子溶剂的存在下将多个碳纳米管（CNT）暴露于碱金属源以将其打开; 和（2）将开放的CNT暴露于亲电子试剂以形成官能化的石墨烯纳米带（GNR）。所述方法还可以包括将开放的CNT暴露于质子溶剂以淬灭其上的任何反应性物质的步骤。另外的方法包括：通过以下步骤制备未官能化的GNR：（1）在非质子溶剂存在下将多个CNT暴露于碱金属源以打开它们; 和（2）将开放的CNT暴露于质子溶剂以形成未官能化的GNR。

82. 发明申请

US20160251225A1 CARBON NANOTUBES 有权
标题翻译：碳纳米管
公开(公告)号：US20160251225A1
公开(公告)日：2016-09-01
申请号：US15030975
申请日：2014-10-31
申请人： ZEON CORPORATION
发明人： Hirokazu TAKAI , Mitsugu UEJIMA
IPC分类号： C01B31/02
CPC分类号： C01B32/178 , B82Y30/00 , C01B32/16 , C01B2202/36 , Y10S977/742 , Y10S977/842
摘要： Provided are carbon nanotubes that allow effective utilization of the insides thereof as-synthesized, without undergoing opening formation treatment. The provided carbon nanotubes have not undergone opening formation treatment and exhibit a convex upward shape in a t-plot obtained from an adsorption isotherm.
摘要翻译：提供了允许有效利用其合成的内部的碳纳米管，而不进行开口形成处理。所提供的碳纳米管没有进行开口形成处理，并且在从吸附等温线获得的t图中呈现凸起的向上形状。

83. 发明申请

US20150023858A1 REBAR HYBRID MATERIALS AND METHODS OF MAKING THE SAME 有权
标题翻译： REBAR混合材料及其制备方法
公开(公告)号：US20150023858A1
公开(公告)日：2015-01-22
申请号：US14335566
申请日：2014-07-18
申请人： James M. Tour , Zheng Yan , Zhiwei Peng , Robert H. Hauge , Yilun Li
发明人： James M. Tour , Zheng Yan , Zhiwei Peng , Robert H. Hauge , Yilun Li
IPC分类号： C01B31/36 , B29C39/00 , H01B1/04 , C01B31/04 , C01B31/02
CPC分类号： C01B32/956 , B29C39/003 , B29K2105/124 , B29K2995/0005 , B29L2007/00 , C01B21/064 , C01B32/178 , C01B32/18 , C01B32/184 , C01B32/186 , C01P2004/13
摘要： In some embodiments, the present disclosure pertains to methods of forming a reinforcing material by: (1) depositing a first material onto a catalyst surface; and (2) forming a second material on the catalyst surface, where the second material is derived from and associated with the first material. In some embodiments, the first material includes, without limitation, carbon nanotubes, graphene nanoribbons, boron nitride nanotubes, chalcogenide nanotubes, carbon onions, and combinations thereof. In some embodiments, the formed second material includes, without limitation, graphene, hexagonal boron nitride, chalcogenides, and combinations thereof. In additional embodiments, the methods of the present disclosure also include a step of separating the formed reinforcing material from the catalyst surface, and transferring the separated reinforcing material onto a substrate without the use of polymers. Additional embodiments of the present disclosure pertain to reinforcing materials formed by the aforementioned methods.
摘要翻译：在一些实施方案中，本公开涉及通过以下步骤形成增强材料的方法：（1）将第一材料沉积到催化剂表面上; 和（2）在所述催化剂表面上形成第二材料，其中所述第二材料衍生并与所述第一材料相关联。在一些实施方案中，第一材料包括但不限于碳纳米管，石墨烯纳米带，氮化硼纳米管，硫族化物纳米管，碳鎓和它们的组合。在一些实施例中，所形成的第二材料包括但不限于石墨烯，六方氮化硼，硫族化合物及其组合。在另外的实施方案中，本公开的方法还包括将形成的增强材料从催化剂表面分离并将分离的增强材料转移到基材上而不使用聚合物的步骤。本公开的另外的实施方案涉及通过上述方法形成的增强材料。

84. 发明申请

US20140302322A1 SINGLE WALL CARBON NANOTUBE PURIFICATION PROCESS AND IMPROVED SINGLE WALL CARBON NANOTUBES 审中-公开
标题翻译：单壁碳纳米管净化工艺和改进的单壁碳纳米管
公开(公告)号：US20140302322A1
公开(公告)日：2014-10-09
申请号：US14342735
申请日：2012-08-28
申请人： Ricardo Prada Silvy , Yongqiang Tan
发明人： Ricardo Prada Silvy , Yongqiang Tan
IPC分类号： C01B31/02
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/17 , C01B32/178 , C01B2202/02 , C01B2202/32 , Y10S977/743 , Y10S977/75 , Y10S977/845 , Y10S977/848 , Y10T428/2982
摘要： Disclosed are methods for decapping single wall carbon nanotubes and purifying the decapped single wall carbon nanotubes. The disclosed methods include the steps of oxidizing the single wall carbon nanotubes to remove the terminal end cap and subsequently acid washing the single wall carbon nanotubes to remove the catalyst particles. The resulting carbon nanotubes have improved BET surface area and pore volume.
摘要翻译：公开了拆开单壁碳纳米管并净化已拆除的单壁碳纳米管的方法。所公开的方法包括以下步骤：氧化单壁碳纳米管以除去终端帽，随后酸洗单壁碳纳米管以除去催化剂颗粒。所得碳纳米管具有改善的BET表面积和孔体积。

85. 发明申请

US20120121683A1 FUNCTIONAL NANOPARTICLE FILLED NANOTUBES AND METHODS OF THEIR PRODUCTION 审中-公开
标题翻译：功能纳米材料填充纳米管及其生产方法
公开(公告)号：US20120121683A1
公开(公告)日：2012-05-17
申请号：US13348907
申请日：2012-01-12
申请人： YURY GOGOTSI , GUZELIYA KORNEVA , GENNADY FRIEDMAN
发明人： YURY GOGOTSI , GUZELIYA KORNEVA , GENNADY FRIEDMAN
IPC分类号： H01F1/01 , H01F41/00 , A61K9/70 , B05D5/00 , B82Y30/00 , B82Y5/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/178 , Y10T428/2918 , Y10T428/2982
摘要： Carbon nanotubes with a suspension or colloidal solution of functional nanoparticles and methods for production of carbon nanotubes loaded with functional nanoparticles are provided.
摘要翻译：提供具有功能性纳米颗粒的悬浮液或胶体溶液的碳纳米管和用于生产负载有功能性纳米颗粒的碳纳米管的方法。

86. 发明申请

US20120092758A1 NANOCOMPOSITES, METHOD FOR PRODUCING SAME, AND USE THEREOF IN DEVICES FOR PROTECTING AGAINST ELECTROMAGNETIC WAVES 审中-公开
标题翻译：纳米复合材料，其制造方法及其在用于防止电磁波的装置中的应用
公开(公告)号：US20120092758A1
公开(公告)日：2012-04-19
申请号：US13201596
申请日：2010-02-16
申请人： Valerie Keller-Spitzer , Anne Teissier , Yves Lutz , Jean-Pierre Moeglin , Olivier Muller , Fabrice Lacroix
发明人： Valerie Keller-Spitzer , Anne Teissier , Yves Lutz , Jean-Pierre Moeglin , Olivier Muller , Fabrice Lacroix
IPC分类号： G02B5/20 , G02F1/355 , D01F9/12 , B82Y40/00 , B82Y20/00
CPC分类号： B82Y20/00 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B32/178 , C01B2202/10 , C01G23/047 , C01G23/053 , C01G33/00 , C01G41/02 , C01P2004/04 , C01P2004/13 , C01P2004/80 , Y10T428/2918 , Y10T428/2958
摘要： A nanocomposite, comprising single-wall and/or multi-wall one-dimensional nanomaterials, and at least one nanooxide of at least one transition metal, said nanooxide filling said nanotubes and covering their walls. A process for preparing such a nanocomposite and an optical limiting device comprising such a nanocomposite in suspension in a medium that is transparent to visible and infrared radiation are disclosed.
摘要翻译：一种纳米复合材料，包括单壁和/或多壁一维纳米材料，以及至少一种至少一种过渡金属的纳米氧化物，所述纳米氧化物填充所述纳米管并覆盖其壁。公开了一种制备这种纳米复合材料的方法和包括在对可见光和红外辐射透明的介质中悬浮的这种纳米复合材料的光学限制装置。

87. 发明申请

US20110206932A1 SURFACE-MODIFIED CARBON NANOTUBE AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译：表面改性碳纳米管及其生产方法
公开(公告)号：US20110206932A1
公开(公告)日：2011-08-25
申请号：US12910759
申请日：2010-10-22
申请人： Keiko Waki , Do-Hyun Kim , Masashi Takano
发明人： Keiko Waki , Do-Hyun Kim , Masashi Takano
IPC分类号： D01F9/12 , D02J3/00 , C01B31/00 , B82Y40/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/168 , C01B32/178 , C01B2202/36 , Y10T428/2978
摘要： A carbon nanotube (CNT) is provided having micropores with a diameter of 1 to 10 nm in the side wall and in turn, having a large specific surface area. A production method of a surface-modified CNT (DMWCNT), comprises heating CNT having supported on the surface thereof a metal oxide or metal nitrate fine particle at a temperature of 100 to 1000° C., such as, 200 to 500° C., in an atmosphere containing oxygen. A cyclical solid phase oxidation-reduction reaction between the metal oxide and CNT occurs on the surface of the metal oxide fine particle supported on CNT, and carbon of CNT is oxidized to open a micropore. The metal oxide is preferably cobalt oxide, and the metal nitrate is preferably cobalt nitrate.
摘要翻译：在侧壁中提供具有直径为1至10nm的微孔并且具有大的比表面积的碳纳米管（CNT）。表面改性CNT（DMWCNT）的制造方法包括在100〜1000℃，例如200〜500℃的温度下加热在其表面上具有金属氧化物或金属硝酸盐微粒的CNT。，在含氧气氛中。金属氧化物和CNT之间的周期性固相氧化还原反应发生在负载在CNT上的金属氧化物微粒的表面上，并且碳的碳被氧化以打开微孔。金属氧化物优选为氧化钴，金属硝酸盐优选为硝酸钴。

88. 发明申请

US20110183139A1 ORGANIZED CARBON AND NON-CARBON ASSEMBLY 审中-公开
标题翻译：有机碳和非碳集合
公开(公告)号：US20110183139A1
公开(公告)日：2011-07-28
申请号：US13073865
申请日：2011-03-28
申请人： Leonid Grigorian , Steven G. Colbern , Alex E. Moser , Robert L. Gump , Daniel A. Niebauer , Sean Imtiaz Brahim
发明人： Leonid Grigorian , Steven G. Colbern , Alex E. Moser , Robert L. Gump , Daniel A. Niebauer , Sean Imtiaz Brahim
IPC分类号： D01F8/18 , D01F9/12 , B82Y40/00 , B82Y30/00 , B82Y20/00 , B82Y15/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/168 , C01B32/178 , C01B32/18 , C01B2202/02 , Y10S977/734 , Y10S977/742 , Y10S977/744 , Y10S977/75 , Y10S977/752 , Y10S977/842 , Y10S977/847 , Y10T428/292
摘要： This invention relates generally to organized assemblies of carbon and non-carbon compounds and methods of making such organized structures. In preferred embodiments, the organized structures of the instant invention take the form of nanorods or their aggregate forms. More preferably, a nanorod is made up of a carbon nanotube filled, coated, or both filled and coated by a non-carbon material. This invention is further drawn to the separation of single-wall carbon nanotubes. In particular, it relates to the separation of semiconducting single-wall carbon nanotubes from conducting (or metallic) single-wall carbon nanotubes. It also relates to the separation of single-wall carbon nanotubes according to their chirality and/or diameter.
摘要翻译：本发明一般涉及碳和非碳化合物的有组织的组合物以及制造这种有组织结构的方法。在优选实施方案中，本发明的有组织结构采取纳米棒或其聚集体形式。更优选地，纳米棒由填充有碳纳米管的碳纳米管，或者由非碳材料填充和涂覆。本发明进一步涉及单壁碳纳米管的分离。特别地，它涉及半导体单壁碳纳米管与导电（或金属）单壁碳纳米管的分离。它还涉及根据其手性和/或直径分离单壁碳纳米管。

89. 发明授权

US07833366B1 Method for making single walled carbon nanotubes by activation with hydrazoic acid 失效
标题翻译：用叠氮酸活化制备单壁碳纳米管的方法
公开(公告)号：US07833366B1
公开(公告)日：2010-11-16
申请号：US11998982
申请日：2007-10-31
申请人： Farhad Forohar , Magdy Bichay
发明人： Farhad Forohar , Magdy Bichay
IPC分类号： C06B45/00 , C06B45/04 , C06B35/00 , D03D23/00 , D03D43/00
CPC分类号： C06B45/20 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B32/178 , C01B2202/02 , C01B2202/10 , C06B23/005
摘要： The present invention relates generally to methods of making carbon nanotubes, and more particularly to the interaction of single wall carbon nanotubes with hydrazoic acid to introduce energetic azide groups into the nanotubes to form activated carbon nanotubes.
摘要翻译：本发明一般涉及制备碳纳米管的方法，更具体地说涉及单壁碳纳米管与氢氮酸的相互作用，以将能量叠氮化物基团引入到纳米管中以形成活性碳纳米管。

90. 发明申请

US20080318049A1 Single-Walled Carbon Nanotube and Aligned Single-Walled Carbon Nanotube Bulk Structure, and Their Production Process, Production Apparatus and Application Use 有权
标题翻译：单壁碳纳米管和对称单壁碳纳米管散装结构及其生产工艺，生产设备及应用使用
公开(公告)号：US20080318049A1
公开(公告)日：2008-12-25
申请号：US11658577
申请日：2005-07-27
申请人： Kenji Hata , Sumio Ijima , Motoo Yumura , Don Futaba
发明人： Kenji Hata , Sumio Ijima , Motoo Yumura , Don Futaba
IPC分类号： D01F9/12 , C23C16/26 , B32B9/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/17 , C01B32/178 , C01B2202/02 , C01B2202/08 , C01B2202/30 , C01B2202/34 , Y02E60/324 , Y10S977/742 , Y10S977/75 , Y10T428/2918 , Y10T428/30
摘要： This invention provides an aligned single-layer carbon nanotube bulk structure, which comprises an assembly of a plurality of aligned single-layer carbon nanotube and has a height of not less than 10 μm, and an aligned single-layer carbon nanotube bulk structure which comprises an assembly of a plurality of aligned single-layer carbon nanotubes and has been patterned in a predetermined form. This structure is produced by chemical vapor deposition (CVD) of carbon nanotubes in the presence of a metal catalyst in a reaction atmosphere with an oxidizing agent, preferably water, added thereto. An aligned single-layer carbon nanotube bulk structure, which has realized high purify and significantly large scaled length or height, its production process and apparatus, and its applied products are provided.
摘要翻译：本发明提供了一种对齐的单层碳纳米管块结构，其包括多个排列的单层碳纳米管的组件，其高度不小于10微米，并且排列的单层碳纳米管块结构包括多个对准的单层碳纳米管的组件，并且已经以预定形式图案化。该结构通过在金属催化剂的存在下在与添加有氧化剂，优选水的反应气氛中的碳纳米管的化学气相沉积（CVD）来制备。提供了实现高净化和大尺寸长度或高度的对准单层碳纳米管块结构，其生产工艺和装置及其应用产品。

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