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71. 发明授权

US08900711B2 Fluorooxyalkylene group-containing polymer composition, a surface treatment agent comprising the same and an article treated with the agent 有权
标题翻译：含有含氟氧化烯基的聚合物组合物，包含该组合物的表面处理剂和用该试剂处理的制品
公开(公告)号：US08900711B2
公开(公告)日：2014-12-02
申请号：US13226987
申请日：2011-09-07
申请人： Yuji Yamane , Yasunori Sakano , Koichi Yamaguchi , Noriyuki Koike , Hirofumi Kishita
发明人： Yuji Yamane , Yasunori Sakano , Koichi Yamaguchi , Noriyuki Koike , Hirofumi Kishita
IPC分类号： C08L71/00 , C08G65/336 , C08G65/00 , C08G77/24 , C08G77/46 , C09D171/02
CPC分类号： C08G77/46 , C08G65/007 , C08G65/336 , C08G77/24 , C08G2650/48 , C09D171/02 , Y10T428/3154
摘要： A fluorooxyalkylene group-containing polymer composition including a liner fluorooxyalkylene group-containing polymer represented by the formula (1) which has a hydrolysable group at a terminal and is hereinafter called “one-terminal modified polymer”, and a liner fluorooxyalkylene group-containing polymer represented by the following formula (2) which has hydrolysable groups at the both terminals and is hereinafter called “both-terminal modified polymer”, wherein an amount of the both-terminal modified polymer is 0.1 mole % or more and less than 10 mole %, relative to a total mole of the one-terminal modified polymer and the both-terminal modified polymer.
摘要翻译：含有含氧代烯烃基的聚合物组合物，包含在末端具有可水解基团，以下称为“一端改性聚合物”的由式（1）表示的含有氧化烯烷基的聚合物的聚合物和含有氧化烯烃基的聚合物的聚合物由下式（2）表示，其在两末端具有可水解基团，以下称为“双末端改性聚合物”，其中两末端改性聚合物的量为0.1摩尔％以上且小于10摩尔％，相对于单末端改性聚合物和双末端改性聚合物的总摩尔数。

72. 发明授权

US08304571B2 Perfluoropolyether-modified polysiloxane, a method for preparing the same and a defoaming agent comprising the same 有权
标题翻译：全氟聚醚改性聚硅氧烷，其制备方法和包含该聚硅氧烷的消泡剂
公开(公告)号：US08304571B2
公开(公告)日：2012-11-06
申请号：US12834439
申请日：2010-07-12
申请人： Hiromasa Yamaguchi , Noriyuki Koike
发明人： Hiromasa Yamaguchi , Noriyuki Koike
IPC分类号： C08G77/46 , C07F7/08
CPC分类号： C08G77/46 , B01D19/0427 , B01D19/0431 , B01D19/0409 , B01D19/0413
摘要： The present invention relates to a perfluoropolyether-modified polysiloxane represented by general formula (1): wherein X is a divalent group represented by formula —CH2—, —CH2O—, —CH2OCH2— or —Y—NR—CO—, R1, R2, and R3 are, independently of each other, an alkyl group having 1 to 10 carbon atoms or an aryl group; X′ is a divalent group represented by formula —CH2—, —OCH2—, —CH2OCH2— or —CO—NR—Y′—, a is, independently of each other, 0 or 1; z and z′ are, independently of each other, an integer of 5 to 100; and Rf is a divalent group represented by the following general formula (2): —CtF2t[OCF2CF(CF3)]m—OCF2(CF2)rCF2O[CF(CF3)CF2O]nCtF2t— (2) or by the following general formula (3): —Ct′F2t′(OCF2CF2)u(OCF2)vOCt′F2t′— (3).
摘要翻译：本发明涉及由通式（1）表示的全氟聚醚改性聚硅氧烷：其中X为由式-CH 2 - ， - CH 2 O - ， - CH 2 OCH 2 - 或-Y-NR-CO-，R 1，R 2表示的二价基团和R 3彼此独立地为具有1〜10个碳原子的烷基或芳基; X'是由式-CH 2 - ， - OCH 2 - ， - CH 2 OCH 2 - 或-CO-NR-Y' - 表示的二价基团，a彼此独立地为0或1; z和z'彼此独立地为5至100的整数; Rf是由以下通式（2）表示的二价基团：-CtF 2t [OCF 2 CF（CF 3）] m OCF 2（CF 2）r CF 2 O [CF（CF 3）CF 2 O] n Ct F 2t-（2） 3）：-C'2'（OCF2CF2）u（OCF2）vOCt'F2t'-（3）。

73. 发明授权

US08283480B2 Perfluoropolyether group-containing acrylate compound 有权
标题翻译：含全氟聚醚基团的丙烯酸酯化合物
公开(公告)号：US08283480B2
公开(公告)日：2012-10-09
申请号：US12797103
申请日：2010-06-09
申请人： Yasunori Sakano , Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
发明人： Yasunori Sakano , Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
IPC分类号： C07F7/21 , C07F7/08 , C07F7/10
CPC分类号： C08G77/50 , C07F7/21 , C08F230/08 , C08G77/388 , C08G77/46 , C09D183/12 , C09D183/14
摘要： The present invention relates to a photo-curable perfluoropolyether group-containing acrylate compound represented by the following formula (1): X1—[Z—Rf—Z—X2]v—Z—Rf—Z—X1 (1) wherein Rf is a divalent perfluoropolyether group; X1 is a group represented by the following formula (2): R2 is a group represented by the following formula (4): X2 is a group represented by the following formula (5): and Z is a divalent organic group.
摘要翻译：本发明涉及由下式（1）表示的可光固化的全氟聚醚基丙烯酸酯化合物：X1- [Z-Rf-Z-X2] v-Z-Rf-Z-X1（1）其中Rf为二价全氟聚醚基团; X1是由下式（2）表示的基团：R2是由下式（4）表示的基团：X2是由下式（5）表示的基团：Z是二价有机基团。

74. 发明授权

US08263724B2 Fluorine-containing surface treating agent and an article surface-treated therewith 有权
标题翻译：含氟表面处理剂和用其表面处理的物品
公开(公告)号：US08263724B2
公开(公告)日：2012-09-11
申请号：US12544668
申请日：2009-08-20
申请人： Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
发明人： Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
IPC分类号： C08G77/46 , C08G77/04
CPC分类号： C08G77/46 , C08G77/50 , C08K5/5406 , Y10T428/31663
摘要： The purpose of the present invention is to provide a surface treating agent which provides a surface where stain does not easily adhere, does not stand out and is easily wiped off.The present invention is a perfluoropolyether group-containing polyorganosiloxane represented by the following formula (1) and a surface treating agent comprising the same, Ak(R)nZ-Q-Rf-Q-Z(R)nAk (1) wherein Rf is a divalent perfluoropolyether group; Q is a divalent group linking Rf with Z; Z is a polyorganosiloxane group having at least three siloxane bonds with its valency being trivalent to undecavalent; R is a monovalent organic group having 8 to 40 carbon atoms, n is an integer of from 1 to 8; A is a group represented by the following formula (2); and k is an integer of from 1 to 9, provided that a total of n+k=the valency of Z−1 wherein R′ is an alkyl group having 1 to 4 carbon atoms or a phenyl group; X is a hydrolysable group, a is 2 or 3; and b is an integer of from 2 to 10.
摘要翻译：本发明的目的是提供一种表面处理剂，其提供不易粘附的污渍的表面，不会脱落，容易擦去。本发明是由下式（1）表示的含全氟聚醚基团的聚有机硅氧烷和包含该组合物的表面处理剂，其中，Rf（R）nZ-Q-Rf-QZ（R）nAk（1）全氟聚醚基团 Q是连接Rf与Z的二价基团; Z是具有至少三个硅氧烷键的聚有机硅氧烷基团，其化合价为三价至未降解; R为碳原子数为8〜40的1价有机基团，n为1〜8的整数， A是由下式（2）表示的基团。并且k是1至9的整数，条件是总共n + k = Z-1的化合价，其中R'是具有1至4个碳原子的烷基或苯基; X是可水解基团，a是2或3; b为2〜10的整数。

75. 发明授权

US08247078B2 Fluorine-containing acrylate 有权
标题翻译：含氟丙烯酸酯
公开(公告)号：US08247078B2
公开(公告)日：2012-08-21
申请号：US12510793
申请日：2009-07-28
申请人： Yasunori Sakano , Noriyuki Koike
发明人： Yasunori Sakano , Noriyuki Koike
IPC分类号： B32B27/00 , C08F18/20
CPC分类号： C07F7/21 , Y10T428/3154 , Y10T428/31663
摘要： Photocurable fluorine compound, compatible with non-fluorine organic compounds, of formula (1), wherein: a is 1-4, b is 0-3, c is 1-4, provided that a+b+c is 3-5; e is 2-8; R1 has formula (2), (C4H8O)f(C3H6O)g(C2H4O)h(CH2O)iR3 (2) wherein f, g, h, and i are independently 0-100, and R1 has an MW of 30-3000, these repeating units may be sequenced at random, and R3 is C1-10 hydrocarbon; R2 is independently H, F, CH3, or CF3; Rf is a perfluoropolyether residue represented by the following formula (3), wherein j, k, l, and m are independently of each other integers of 0 to 50, provided that a molecular weight of Rf is in a range of 200 to 6000, X is F or CF3, and these repeating units may be sequenced at random; Z is a divalent organic group; and d is 0 or 1.
摘要翻译：与式（1）的非氟有机化合物相容的可光固化的氟化合物，其中：a为1-4，b为0-3，c为1-4，条件是a + b + c为3-5; e为2-8; R1具有式（2），（C4H8O）f（C3H6O）g（C2H4O）h（CH2O）iR3（2）其中f，g，h和i分别为0-100，R1的MW为30-3000 ，这些重复单元可以随机排序，R3是C1-10烃; R2独立地为H，F，CH 3或CF 3; Rf是由下式（3）表示的全氟聚醚残基，其中j，k，l和m彼此独立地为0至50的整数，条件是Rf的分子量在200至6000的范围内， X是F或CF 3，这些重复单元可以随机排序; Z是二价有机基团; d为0或1。

76. 发明申请

US20110257315A1 ADHESIVE COMPOSITION 有权
标题翻译：粘合剂组合物
公开(公告)号：US20110257315A1
公开(公告)日：2011-10-20
申请号：US13085510
申请日：2011-04-13
申请人： Mikio Shiono , Noriyuki Koike
发明人： Mikio Shiono , Noriyuki Koike
IPC分类号： C09J183/07 , C09J185/00 , C09J11/06
CPC分类号： C09D183/08 , C08G77/24 , C08L71/02
摘要： An adhesive composition is provided comprising (A) a fluorinated amide compound containing at least two vinyl groups and having a polyfluoro structure, (B) a fluorinated organosilicon compound containing a fluorinated organic group, at least two SiH groups, and an alkyl, aryl or aralkyl group, and (C) a platinum catalyst, and (D) an organosiloxane containing a SiH group and an epoxy and/or trialkoxysilyl group. The composition is cured on brief heating into a product which achieves adhesion to various substrates and has solvent resistance, chemical resistance, heat resistance, low-temperature properties, low moisture permeability, electric insulation, and acid resistance.
摘要翻译：提供一种粘合剂组合物，其包含（A）含有至少两个乙烯基并具有多氟结构的氟化酰胺化合物，（B）含氟化有机基团的氟化有机硅化合物，至少两个SiH基团和烷基，芳基或芳族烷基，（C）铂催化剂，（D）含有SiH基和环氧基和/或三烷氧基甲硅烷基的有机硅氧烷。该组合物在短暂加热下固化成实现对各种基材的粘合性的产品，并具有耐溶剂性，耐化学性，耐热性，低温性，低透湿性，电绝缘性和耐酸性。

77. 发明授权

US08013096B2 Perfluoroether moiety-containing polymer and a surface treating agent comprising the same 有权
标题翻译：含全氟醚部分的聚合物和包含该聚合物的表面处理剂
公开(公告)号：US08013096B2
公开(公告)日：2011-09-06
申请号：US12511862
申请日：2009-07-29
申请人： Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
发明人： Yuji Yamane , Noriyuki Koike , Hirofumi Kishita
IPC分类号： C08G77/04
CPC分类号： C08G77/385 , C08G77/46 , C08L83/12 , C09D183/12 , Y10T428/31663
摘要： The present invention relates to a perfluoropolyoxyalkylene group-containing polymer represented by the following formula (1), wherein Rf is a group having a perfluoropolyoxyalkylene group; W1 is a divalent organosiloxane group having at least one group represented by the following formula (2); W2 is a monovalent group selected from an alkyl group, an alkenyl group, an alkenyloxyalkyl group, an aryl group and an organosiloxane group represented by the following formula (3), and the combinations thereof, the monovalent group having 1 to 300 carbon atoms and being optionally substituted with one or more fluorine atoms; Q is, independently of each other, a divalent linking group having 2 to 12 carbon atoms, optionally containing one or more oxygen atoms, nitrogen atoms, or fluorine atoms; and p is an integer of from 1 to 20, wherein X is a hydrolysable group; R1 is an alkyl group having 1 to 4 carbon atoms or a phenyl group; y is an integer of from 1 to 5; and a is 2 or 3, wherein, R2 and R3 each are, independently of each other, a group selected from an alkyl group and an aryl group, have 1 to 200 carbon atoms and may optionally be substituted with one or more fluorine atoms and; and n is an integer of from 0 to 50.
摘要翻译：本发明涉及由下式（1）表示的全氟聚氧化烯基聚合物，其中Rf是具有全氟聚氧化烯基的基团; W1是具有至少一个由下式（2）表示的基团的二价有机硅氧烷基团; W2是选自由下式（3）表示的烷基，烯基，链烯氧基烷基，芳基和有机硅氧烷基的一价基团，以及它们的组合，具有1〜300个碳原子的一价基团和任选被一个或多个氟原子取代; Q彼此独立地是具有2至12个碳原子的任选含有一个或多个氧原子，氮原子或氟原子的二价连接基团; 且p为1至20的整数，其中X为可水解基团; R1是碳原子数为1〜4的烷基或苯基; y为1〜5的整数; 和a为2或3，其中R 2和R 3各自独立地为选自烷基和芳基的基团，其具有1至200个碳原子并且可任选地被一个或多个氟原子取代，并且 ; n为0〜50的整数。

78. 发明授权

US07968741B2 Method of preparing disilanol compound and method of storing disilanol compound 有权
标题翻译：制备二硅烷醇化合物的方法和二硅烷醇化合物的储存方法
公开(公告)号：US07968741B2
公开(公告)日：2011-06-28
申请号：US11826940
申请日：2007-07-19
申请人： Yasunori Sakano , Takashi Matsuda , Noriyuki Koike
发明人： Yasunori Sakano , Takashi Matsuda , Noriyuki Koike
IPC分类号： C07F7/08
CPC分类号： C07F7/0836 , C08G65/007 , C08G65/336
摘要： A method of preparing a disilanol compound by hydrolyzing a dichlorosilane compound having Si—Cl bonds at both ends, characterized in that the method comprises the step of hydrolyzing the dichlorosilane compound in the presence of a tertiary amine compound.
摘要翻译：通过在两端水解具有Si-Cl键的二氯硅烷化合物制备二硅烷醇化合物的方法，其特征在于该方法包括在叔胺化合物存在下水解二氯硅烷化合物的步骤。

79. 发明授权

US07847015B2 Coating composition 有权
标题翻译：涂料组成
公开(公告)号：US07847015B2
公开(公告)日：2010-12-07
申请号：US11984175
申请日：2007-11-14
申请人： Noriyuki Koike , Yuji Yamane , Hirofumi Kishita , Koichi Yamaguchi
发明人： Noriyuki Koike , Yuji Yamane , Hirofumi Kishita , Koichi Yamaguchi
IPC分类号： C08L83/00 , C08G77/00 , C08G77/24
CPC分类号： C09D5/165 , C08G65/007 , C08G2650/48 , C08K5/095 , C08L2205/05 , C09D5/1675 , C09D171/02 , C09D183/08 , C09D183/12 , C09D183/14 , C08L83/00 , C08L2666/32
摘要： A coating composition comprising (A) at least one fluorine-containing organosilicon compound represented by the following formula (1) or (2) Rf1-QZ1Aα (1) AαZ1Q-Rf2-(Q-Z2-Q-Rf2)x-QZ1Aα (2) and (B) a fluorine-containing carboxylic acid having a number average molecular weight of from 100 to 10,000 and a fluorine content of at least 25 wt %, wherein an amount of (B) ranges from 0.001 to 10 parts by weight per 100 parts by weight of the component (A) wherein the amount of (B) ranges from 0.001 to 10 parts by weight per 100 parts by weight of the component (A), wherein the composition can be cured rapidly even at room temperature to produce water-repellent and antifouling coatings.
摘要翻译：一种涂料组合物，其包含（A）至少一种由下式（1）或（2）表示的含氟有机硅化合物Rf1-QZ1Aα（1）AαZ1Q-Rf2-（Q-Z2-Q-Rf2）x-QZ1Aα（ 2）和（B）数均分子量为100〜10,000，氟含量为25重量％以上的含氟羧酸，其中（B）的量为0.001〜10重量份/ 相对于（A）成分100重量份，（B）成分的（B）成分为100重量份，（B）成分为0.001〜10重量份，即使在室温下也能够迅速固化，防水防污涂料。

80. 发明授权

US07781604B2 Fluorine-containing acrylate 有权
标题翻译：含氟丙烯酸酯
公开(公告)号：US07781604B2
公开(公告)日：2010-08-24
申请号：US12619135
申请日：2009-11-16
申请人： Yasunori Sakano , Noriyuki Koike , Hirofumi Kishita
发明人： Yasunori Sakano , Noriyuki Koike , Hirofumi Kishita
IPC分类号： C07C7/10
CPC分类号： C08G77/045 , C07F7/21 , C08F220/22 , C08F220/24 , C08F230/08 , C08G18/61 , C08G18/8116 , C08G77/38 , C08G77/388 , C09D175/16
摘要： The present invention is a fluorine-containing acrylate or alpha-substituted, fluorine-containing acrylate, represented by the following formula (1): wherein a is an integer of from 1 to 4 and b is an integer of from 1 to 4, provided that a total of a and b is 3, 4, or 5; R1 is a group represented by the following formula (2): —(C4H8O)d(C3H6O)e(C2H4O)f(CH2O)g— (2) wherein d, e, f, and g are, independently of each other, an integer of from 0 to 4, provided that a molecular weight of R1 is in a range of 30 to 300, and these repeating units may be sequenced at random; R2 is an acryl group- or alpha-substituted acryl group-containing group having 4 to 20 carbon atoms and represented by the following formula (3): wherein R3 is, independently of each other, a hydrogen atom, a fluorine atom, a methyl group, or a trifluoromethyl group, R4 is a divalent or trivalent linking moiety having 1 to 18 carbon atoms, optionally having an ether bond and/or an ester bond, and n is 1 or 2; Rf is a perfluoropolyether residue represented by the following formula (4): wherein j, k, l, and m are, independently of each other, an integer of from 0 to 50, provided that a molecular weight of Rf is in a range of 200 to 6000, X is a fluorine atom or a trifluoromethyl group, and these repeating units may be sequenced at random; Z is a divalent organic group; and c is 0 or 1.
摘要翻译：本发明是由下式（1）表示的含氟丙烯酸酯或α-取代的含氟丙烯酸酯，其中a为1〜4的整数，b为1〜4的整数，总共a和b为3,4或5; R1是由下式（2）表示的基团： - （C4H8O）d（C3H6O）e（C2H4O）f（CH2O）g-（2）其中d，e，f和g彼此独立地是如果R1的分子量在30〜300的范围内，则0〜4的整数，这些重复单元可以随机排列; R2是具有4〜20个碳原子的丙烯酰基或α-取代的含丙烯酰基的基团，由下式（3）表示：其中R 3彼此独立地为氢原子，氟原子，甲基基团或三氟甲基，R 4是具有1至18个碳原子的二价或三价连接部分，任选具有醚键和/或酯键，n为1或2; Rf是由下式（4）表示的全氟聚醚残基：其中j，k，l和m彼此独立地为0至50的整数，条件是Rf的分子量在 200〜6000，X为氟原子或三氟甲基，这些重复单元可以随机排列; Z是二价有机基团; c为0或1。

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