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61. 发明授权

US5433752A Use of rection products of Homo- or copolymers based on monoethylenically unsaturated dicarboxylic anhydrides with amines or alcohols for fatliquoring and filling leather and fur skins 失效
标题翻译：使用基于单烯键式不饱和二羧酸酐的均聚物或共聚物与胺或醇的反应产物用于加脂和填充皮革和毛皮
公开(公告)号：US5433752A
公开(公告)日：1995-07-18
申请号：US290779
申请日：1994-08-26
申请人： Hermann Birkhofer , Peter Danisch , Walter Denzinger , Heinrich Hartmann , Norbert Greif , Knut Oppenlaender
发明人： Hermann Birkhofer , Peter Danisch , Walter Denzinger , Heinrich Hartmann , Norbert Greif , Knut Oppenlaender
IPC分类号： C14C9/00 , C14C3/22 , C14C9/02
CPC分类号： C14C9/00
摘要： Products useful for fatliquoring and filling leather and fur skins are obtained on reactingA) homo- or copolymers based on monoethylenically unsaturated dicarboxylic anhydrides and obtainable by free-radically initiated polymerization ofa) from 30 to 100 mol % of one or more monoethylenically unsaturated dicarboxylic anhydrides of from 4 to 10 carbon atoms,b) from 0 to 70 mol % of one or more aromatic vinyl compounds of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, methyl or ethyl and k is 1 or 2,(c) from 0 to 70 mol % of one or more vinyl esters of C.sub.1 - to C.sub.8 -carboxylic acids,(d) from 0 to 50 mol % of one or more C.sub.2 - to C.sub.6 -olefins, and(e) from 0 to 30 mol % of one or more monoethylenically unsaturated C.sub.3 - to C.sub.5 -carboxylic acids, which mixture of monomers (a) to (e) may additionally contain up to 10% by weight of further copolymerizable monomers, withB) amines of the general formula R.sub.4 R.sub.5 NH, where R.sup.4 is hydrogen, C.sub.1 - to C.sub.20 -alkyl, C.sub.5 - to C.sub.8 -cycloalkyl or C.sub.2 - to C.sub.4 -hydroxyalkyl and R.sup.5 is C.sub.6 - to C.sub.30 -alkyl, C.sub.6 - to C.sub.30 -alkenyl, C.sub.5 - to C.sub.8 -cycloalkyl or C.sub.2 - to C.sub.4 -hydroxyalkyl, or alcohols of the general formula R.sup.6 --O--(C.sub.m H.sub.2m O).sub.p --(C.sub.n H.sub.2n O).sub.q --H, where R.sup.6 is C.sub.1 - to C.sub.30 -alkyl, C.sub.2 - to C.sub.30 -alkenyl, C.sub.5 - to C.sub.8 -cycloalkyl or--if p+q>0--hydrogen, m and n are each from 2 to 4 and p and q are each from 0 to 50, or mixtures of such amines and alcohols.
摘要翻译： PCT No.PCT / EP93 / 00354 Sec。 371日期1994年8月26日 102（e）日期1994年8月26日PCT提交1993年2月15日PCT公布。公开号WO93 / 17130 PCT 日期：1993年9月2日。用于加脂和填充皮革和毛皮的产品可以通过A）基于单烯键式不饱和二羧酸酐的均聚物或共聚物获得，可通过自由基引发的a）30至100摩尔％的一种或多种具有4-10个碳原子的单烯键式不饱和二羧酸酐，b）0-70摩尔％的一种或多种通式I的芳族乙烯基化合物，其中R 1，R 2和R 3各自为氢，甲基或乙基，k为1或2，（c）0至70摩尔％的一种或多种C 1至C 8羧酸的乙烯基酯，（d）0至50摩尔％的一种或多种C 2 - C6-烯烃，和（e）0-30mol％的一种或多种单烯键式不饱和C3-至C5-羧酸，单体（a）至（e）的混合物可另外含有高达10重量％可共聚的单体，B）通式为R4R5NH的胺，其中R4是氢，C1-至C20-烷基，C5-至 C 5 -C 8 - 环烷基或C 2 -C 4羟基烷基，R 5为C 6至C 30 - 烷基，C 6至C 30 - 烯基，C 5 -C 8 - 环烷基或C 2至C 4 - 羟烷基，或通式为R 6 -O - （CmH2mO）p-（CnH2nO）qH，其中R6是C1-至C30-烷基，C2-至C30-烯基，C5-至C8-环烷基或 - 如果p + q> O-氢，m和n各自 2至4，p和q各自为0至50，或这些胺和醇的混合物。

62. 发明授权

US5286263A Use of copolymers based on long-chain alkyl vinyl ethers and ethylenically unsaturated dicarboxylic anhydrides for rendering leathers and skins water-repellent 失效
标题翻译：使用基于长链烷基乙烯基醚和烯键式不饱和二羧酸酐的共聚物，用于使皮革和皮肤防水
公开(公告)号：US5286263A
公开(公告)日：1994-02-15
申请号：US829062
申请日：1992-02-10
申请人： Ortwin Schaffer , Herbert Bay , Karl Stork , Norbert Greif , Knut Oppenlaender , Walter Denzinger , Heinrich Hartmann
发明人： Ortwin Schaffer , Herbert Bay , Karl Stork , Norbert Greif , Knut Oppenlaender , Walter Denzinger , Heinrich Hartmann
IPC分类号： C08F8/32 , C08F8/44 , C08F16/16 , C08F216/16 , C08F220/04 , C08F222/06 , C14C9/00 , C14C3/08
CPC分类号： C14C9/00 , C08F8/44
摘要： Copolymers which are obtainable by free radical copolymerization of (a) C.sub.8 -C.sub.40 -alkyl vinyl ethers, if necessary as a mixture with not more than 50 mol % of C.sub.8 -C.sub.40 -monoolefins, with (b) ethylenically unsaturated C.sub.4 -C.sub.8 -dicarboxylic anhydrides at from 80.degree. to 300.degree. C. to give copolymers having molecular weights of from 500 to 20,000 g/mol, subsequent solvolysis of the anhydride groups of the copolymers and partial or complete neutralization of the carboxyl groups formed during the solvolysis, in an aqueous medium by means of a base, and which are present in the form of aqueous dispersions or solutions, are used as agents for imparting water repellency to leathers and skins.
摘要翻译：（a）C8与C40烷基乙烯基醚的自由基共聚得到的共聚物，可能与高达50mol％的C 8〜C 40单烯烃混合，与（B）烯属不饱和C4〜C8二羧酸酐在80〜300℃的温度 C以500至200000g / mol的摩尔质量共聚，然后将共聚物的酸酐基溶剂分解，并且在水性介质中至少部分中和，其中通过溶剂解产生的羧基的碱可以以水性分散体或防水皮革和毛皮的解决方案。

63. 发明授权

US4914167A Polymeric organic acids, their preparation and their use in detergents and cleansers 失效
标题翻译：聚合有机酸，它们的制备及其在洗涤剂和清洁剂中的应用
公开(公告)号：US4914167A
公开(公告)日：1990-04-03
申请号：US752013
申请日：1985-07-08
申请人： Juergen Hambrecht , Heinrich Hartmann , Walter Denzinger , Albert Hettche , Wolfgang Trieselt , Rolf Schneider
发明人： Juergen Hambrecht , Heinrich Hartmann , Walter Denzinger , Albert Hettche , Wolfgang Trieselt , Rolf Schneider
IPC分类号： C08F2/02 , C08F220/04 , C11D3/37
CPC分类号： C11D3/3761 , C08F220/04
摘要： Organic polyacids are prepared from monomeric monofunctional acids, such as acrylic acid or methacrylic acid and monomers without an acid group, with or without dicarboxylic acids or their anhydrides, by continuous free radical mass copolymerization under superatmospheric pressure at from 200.degree. to 400.degree. C., followed, if desired, by neutralization of the polyacids obtained. The polyacids obtained by the novel process are useful as phosphate substitutes and scale inhibitors in detergents and cleansers.
摘要翻译：有机多元酸通过在200-400℃的超大气压下连续自由基基团共聚，由单体单官能酸例如丙烯酸或甲基丙烯酸和无酸基的单体制备，含或不含二羧酸或其酸酐。，如果需要，通过中和获得的多元酸。通过该方法获得的多酸可用作洗涤剂和清洁剂中的磷酸盐替代物和防垢剂。

64. 发明授权

US4814102A Detergents containing oxyalkylated, carboxyl-containing polymers 失效
标题翻译：含有烷氧基化的含羧基聚合物的洗涤剂
公开(公告)号：US4814102A
公开(公告)日：1989-03-21
申请号：US175176
申请日：1988-03-31
申请人： Richard Baur , Walter Denzinger , Albrecht Eckell , Heinrich Hartmann , Josef Mueller , Hans-Juergen Raubenheimer , Wolfgang Trieselt
发明人： Richard Baur , Walter Denzinger , Albrecht Eckell , Heinrich Hartmann , Josef Mueller , Hans-Juergen Raubenheimer , Wolfgang Trieselt
IPC分类号： C08F8/14 , C08G65/26 , C11D3/37 , D06L1/12 , C11D17/00
CPC分类号： C11D3/378 , C08F8/14 , C11D3/3757 , C11D3/3773 , C11D3/3784
摘要： Detergents which contain from 0.01 to 20% by weight of oxyalkylated, carbonyl-containing polymers can be prepared by reacting.(A) a polymer which contains, as copolymerized units, one or more monoethylenically unsaturated C.sub.3 -C.sub.6 -carboxylic acids with(B) ethylene oxide, propylene oxide, n-butylene oxide, isobutylene oxide or a mixture of these, in an aqueous medium at up to 150.degree. C.
摘要翻译：含有0.01至20重量％的烷氧基化的含羰基的聚合物的洗涤剂可通过使其反应来制备。（A）一种聚合物，其在水性介质中含有一种或多种单烯属不饱和C3-C6-羧酸与（B）环氧乙烷，环氧丙烷，正丁烯氧化物，异丁烯氧化物或它们的混合物作为共聚单元在150℃

65. 发明授权

US4621127A Preparation of carboxyl-containing polymers 失效
标题翻译：含羧基聚合物的制备
公开(公告)号：US4621127A
公开(公告)日：1986-11-04
申请号：US777328
申请日：1985-09-18
申请人： Walter Denzinger , Heinrich Hartmann , Johannes Perner , Hans-Juergen Raubenheimer
发明人： Walter Denzinger , Heinrich Hartmann , Johannes Perner , Hans-Juergen Raubenheimer
IPC分类号： C08F2/00 , C08F2/10 , C08F2/38 , C08F2/44 , C08F20/00 , C08F20/04 , C08F20/06 , C08F22/00 , C08F22/02 , C08F120/04 , C08F22/04
CPC分类号： C08F20/04 , C08F2/10
摘要： Carboxyl-containing polymers which are water-soluble at least in the neutralized form are prepared by a method in which a monoethylenically unsaturated C.sub.3 -C.sub.5 -carboxylic acid is polymerized in the presence or absence of a carboxyl-free copolymerizable ethylenically unsaturated monomer in aqueous solution in the presence of polymerization initiator and of from 0.01 to 5% by weight, based on the monomers, of an inorganic acid of phosphorus in which the phosphorus has an oxidation state of from 1 to 4, its water-soluble salts, a water-soluble --PO(OH).sub.2 -containing compound and/or its water-soluble salts and, if required, a polymerization regulator. Virtually colorless or only slightly colored polymer solutions are obtained.
摘要翻译：至少以中和形式具有水溶性的含羧基聚合物是通过在存在或不存在无羧基的可共聚烯键式不饱和单体的水溶液中聚合单烯属不饱和C3-C5-羧酸的方法制备的在聚合引发剂存在下，基于单体为0.01〜5重量％的磷的氧化态为1〜4的磷的无机酸，其水溶性盐，水溶性盐，可溶性的含PO（OH）2的化合物和/或其水溶性盐，如果需要，可以使用聚合调节剂。获得几乎无色或仅有微量的聚合物溶液。

66. 发明授权

US4402937A Preparation of PVP-iodine 失效
标题翻译：制备PVP-碘
公开(公告)号：US4402937A
公开(公告)日：1983-09-06
申请号：US188908
申请日：1980-09-19
申请人： Walter Denzinger , Heinrich Hartmann , Wolfgang Schwarz
发明人： Walter Denzinger , Heinrich Hartmann , Wolfgang Schwarz
IPC分类号： C08F8/00 , A01N59/12 , C08F8/20 , C08F8/22 , A61K31/79 , A61K33/18
CPC分类号： A01N59/12 , C08F8/22
摘要： A process for the preparation of PVP-iodine having an iodine:iodide ratio of about 2:1 and a partition coefficient of 180-250, by reacting PVP with elementary iodine in the presence of formic acid, oxalic acid or an ammonium salt or amide of carbonic acid, formic acid or oxalic acid, in aqueous solution.
摘要翻译：在甲酸，草酸或铵盐或酰胺存在下，使PVP与元素碘反应，制备碘碘化物比约为2:1，分配系数180-250的PVP-碘的方法的碳酸，甲酸或草酸，在水溶液中。

67. 发明授权

US4370454A Preparation of maleic anhydride copolymers 失效
标题翻译：马来酸酐共聚物的制备
公开(公告)号：US4370454A
公开(公告)日：1983-01-25
申请号：US350356
申请日：1982-02-19
申请人： Karlheinz Messmer , Hermann Fischer , Heinrich Hartmann , Walter Denzinger , Rolf Schneider , Klaus Wulz , Hans-Juergen Raubenheimer
发明人： Karlheinz Messmer , Hermann Fischer , Heinrich Hartmann , Walter Denzinger , Rolf Schneider , Klaus Wulz , Hans-Juergen Raubenheimer
IPC分类号： C08F20/00 , B01F17/52 , C08F20/02 , C08F210/00 , C08F222/06 , C11D3/37 , D21H17/43 , D21H19/58 , C08L37/00
CPC分类号： C11D3/3773 , C08F222/06 , C11D3/3757 , C11D3/3769 , D21H17/43 , D21H19/58
摘要： Maleic anhydride copolymer powders are prepared by a process wherein a solution or dispersion of maleic anhydride in an alkyl vinyl ether and/or an alkene, containing from 3 to 25 moles of the alkyl vinyl ether and/or alkene per mole of maleic anhydride, is brought into contact with a powder bed under polymerization conditions, and is polymerized in the bed while the reaction mass is circulated and the powder state is maintained, and the heat generated during polymerization is removed by evaporating excess monomer which boils lower than maleic anhydride.
摘要翻译：马来酸酐共聚物粉末通过以下方法制备：其中马来酸酐在烷基乙烯基醚和/或烯烃中的溶液或分散体含有3至25摩尔烷基乙烯基醚和/或烯烃/摩尔马来酸酐的方法是在聚合条件下与粉末床接触，并且在反应物料循环并保持粉末状态的同时在床中聚合，并且通过蒸发沸腾低于马来酸酐的过量单体来除去聚合期间产生的热量。

68. 发明授权

US06174946B1 Agglomerated particles of water-swellable addition polymers, preparation thereof and use thereof 失效
标题翻译：水溶胀性加成聚合物的聚集颗粒，其制备及其用途
公开(公告)号：US06174946B1
公开(公告)日：2001-01-16
申请号：US08894373
申请日：1997-08-22
申请人： Martin R{umlaut over (u)}benacker , Reinhard Schneider , J{umlaut over (u)}rgen Nieberle , Harald Meyer , Heinrich Hartmann
发明人： Martin R{umlaut over (u)}benacker , Reinhard Schneider , J{umlaut over (u)}rgen Nieberle , Harald Meyer , Heinrich Hartmann
IPC分类号： C08J312
CPC分类号： C08J3/12 , C08F6/18 , C08F220/02 , C08F226/00 , C08J3/16 , C08J2300/14 , C08L71/02 , C09D7/43 , D06P1/5214 , D06P1/5242 , D06P1/5257 , D06P1/613
摘要： Agglomerated particles of water-swellable addition polymers, the agglomerated particles having an average particle diameter of from 20 to 5000 &mgr;m and consisting of primary particles having an average particle diameter of from 0.1 to 15 &mgr;m, being preparable by polymerization of water-soluble monomers in the presence of from 1′ to 10% by weight of a regulator and at least 2000 ppm, each based on the monomers, of a crosslinking agent in the manner of a water-in-oil polymerization and subsequent azeotropic removal of water from the water-in-oil polymer emulsions, containing the primary particles, in the presence of agglomerating polyalkylene glycols which (a) are obtainable by an addition reaction of C2-C4-alkylene oxides with alcohols, phenols, amines or carboxylic acids, and (b) contain at least 2 polymerized alkylene oxide units, and disintegrating into the primary particles on introduction into an aqueous medium, processes for preparing the agglomerated polymer particles and use of the agglomerated particles as thickeners for print pastes.
摘要翻译：聚水凝胶颗粒的水溶胀性加成聚合物，凝聚颗粒的平均粒径为20-5000μm，由平均粒径为0.1至15μm的一次颗粒组成，可通过水溶性单体的聚合制备以油包水聚合的方式存在1至10重量％的调节剂和至少2000ppm（基于单体）的交联剂，并且随后从水中共沸除去水（a）可以通过C 2 -C 4 - 烯化氧与醇，酚，胺或羧酸的加成反应获得的聚亚烷基二醇存在下的含有一次颗粒的油中聚合物乳液，和（b）含有至少2个聚合的烯化氧单元，并且在引入水性介质时分解成初级颗粒，制备聚集的聚合物颗粒的方法和使用附聚颗粒作为印刷浆料的增稠剂。

69. 发明授权

US5639723A Reaction products of polybasic carboxylic acids and amino-containing compounds, their preparation and their use in detergents and cleaning agents 失效
标题翻译：多元羧酸和含氨基化合物的反应产物，它们的制备及其在洗涤剂和清洁剂中的应用
公开(公告)号：US5639723A
公开(公告)日：1997-06-17
申请号：US367322
申请日：1995-01-23
申请人： Matthias Kroner , Heinrich Hartmann , Dieter Boeckh , Richard Baur , Alexander Kud , Volker Schwendemann
发明人： Matthias Kroner , Heinrich Hartmann , Dieter Boeckh , Richard Baur , Alexander Kud , Volker Schwendemann
IPC分类号： C08G69/00 , C08G73/00 , C11D3/20 , C11D3/37
CPC分类号： C11D3/2082 , C08G69/00 , C08G73/00 , C11D3/2086 , C11D3/37
摘要： Reaction products of polybasic acids and amino-containing compounds, which are obtainable by heating a mixture of (a) a polybasic carboxylic acid selected from the group consisting of citric acid, isocitric acid, aconitic acid, itaconic acid and/or tartaric acid and (b) an amino-containing compound in a molar ratio of (a) to (b) of from 1:0.1 to 1:10 to at least 80.degree. C. are used as additives in low-phosphate and phosphate-free detergents and cleaning agents.
摘要翻译： PCT No.PCT / EP93 / 01893 Sec。 371日期1995年1月23日 102（e）日期1995年1月23日PCT提交1993年7月17日PCT公布。出版物WO94 / 03576 日期：1994年2月17日多元酸和含氨基化合物的反应产物，其可通过加热（a）选自柠檬酸，异柠檬酸，乌头酸，衣康酸和/或其中的多元羧酸的混合物和/ 或酒石酸，（b）摩尔比为（a）〜（b）为1：0.1〜1:10〜80的氨基化合物作为低磷酸盐和磷酸盐的添加剂 - 清洁剂和清洁剂。

70. 发明授权

US5292800A Water-in-oil polymer emulsions 失效
标题翻译：油包水聚合物乳液
公开(公告)号：US5292800A
公开(公告)日：1994-03-08
申请号：US929025
申请日：1992-08-13
申请人： Dietmar Moench , Heinrich Hartmann , Hans-Ulrich Wekel
发明人： Dietmar Moench , Heinrich Hartmann , Hans-Ulrich Wekel
IPC分类号： B01F17/42 , C08F2/32 , C08L101/00 , C09K8/36 , C08K5/11
CPC分类号： C08F2/32 , C09K8/36
摘要： Water-in-oil emulsions of water-soluble or water-swellable polymers, in which the oil phase of the emulsion consists of not less than 50% by weight of an oil of vegetable or animal origin, contain, as water-in-oil emulsifiers, compounds which are obtainable by(A) reacting a C.sub.10 -C.sub.22 -fatty alcohol with epichlorohydrin in a molar ratio of from 1:0.5 to 1:1.5 to give a glycidyl ether,(B) reacting the glycidyl ether with (1) a saturated C.sub.2 -C.sub.6 -alcohol containing from 2 to 6 OH groups or (2) the monoether thereof with a C.sub.10 -C.sub.22 -fatty alcohol, in a molar ratio of glycidyl ether to (1) or (2) of from 1:0.5 to 1:6, in the presence of an acid or base and(C) alkoxylating the reaction product from (B) with one or more C.sub.2 -C.sub.4 -alkylene oxides in a molar ratio of from 1:1 to 1:6,if necessary, from 5 to 95% by weight of the stated water-in-oil emulsifier being replaced with other water-in-oil emulsifiers.
摘要翻译：水溶性或水溶胀性聚合物的油包水乳液，其中乳液的油相由不少于50重量％的植物或动物来源的油包含作为油包水乳化剂，可通过（A）使C 10 -C 22脂肪醇与摩尔比为1:0.5至1:1.5的表氯醇反应得到缩水甘油醚得到的化合物，（B）缩水甘油醚与（1）含有2至6个OH基团的饱和C 2 -C 6醇或（2）其单醚与C 10 -C 22脂肪醇，缩水甘油醚与（1）或（2）的摩尔比为1:0.5 至1：6，在酸或碱的存在下，和（C）将（B）的反应产物与一种或多种摩尔比为1:1至1:6的C 2 -C 4 - 氧化烯烷氧基化，如必要时，将所述油包水乳化剂的重量从5至95％重量替换为其它油包水乳化剂。

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