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51. 发明申请

US20080196840A1 Industrial Continuous Evaporation Apparatus 审中-公开
标题翻译：工业连续蒸发仪
公开(公告)号：US20080196840A1
公开(公告)日：2008-08-21
申请号：US11791696
申请日：2005-12-12
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： B01D1/06
CPC分类号： C08G63/785 , B01D1/22 , C08F6/003 , C08F6/005 , C08G64/205 , F28D3/00
摘要： It is an object of the present invention, in the case of an apparatus in which a liquid containing matter having a lower boiling point than the liquid is made to flow down along external surfaces of guides, during which time the low boiling point matter is evaporated, to provide a specific apparatus that can be operated stably for a prolonged period of time on an industrial scale such that not less than 1 ton/hr of the liquid is produced through the evaporation, and furthermore to provide a specific industrial evaporation apparatus according to which there are no problems due to degeneration caused by some of the liquid residing in the apparatus for a prolonged period of time. The present inventors arrived at the present invention upon discovering that the above object can be attained, and a high-quality and high-purity concentrated liquid or condensation polymer or thermoplastic polymer can easily be obtained, by using an industrial continuous evaporation apparatus having a specified structure in which there are guides that do not themselves have a heat source, a flow path controlling member having a function of making the liquid fed onto a perforated plate from a liquid receiving port flow mainly from a peripheral portion toward a central portion of the perforated plate is installed in a liquid feeding zone, the perforated plate and the holes therein satisfy specified relationships (formulae (6) and (7)), and formulae (1) to (5), preferably formulae (1) to (13), or preferably formulae (1) to (15), are satisfied.
摘要翻译：本发明的目的在于，使具有比液体沸点低的液体的液体的物质沿引导件的外表面向下流动的装置的情况下，低沸点物质蒸发以提供可以在工业规模下稳定运行的特定装置，使得通过蒸发产生不少于1吨/小时的液体，并且还提供根据下述方法的特定工业蒸发装置：由于长时间在该设备中滞留的一些液体引起的退化，不存在问题。本发明人通过发现能够实现上述目的而达成本发明，通过使用具有规定的工业连续蒸发装置，可以容易地获得高质量和高纯度的浓缩液体或缩聚物或热塑性聚合物其中存在不具有热源的导向件的结构，具有使从液体接收口供给到多孔板上的液体主要从周边部朝向穿孔的中心部分流动的功能的流路控制构件板（6）和（7））和式（1）〜（5），优选式（1）〜（13），或优选式（1）至（15）。

52. 发明申请

US20080110578A1 Industrial Evaporation Apparatus 审中-公开
公开(公告)号：US20080110578A1
公开(公告)日：2008-05-15
申请号：US11666814
申请日：2005-11-30
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： C08G85/00 , C08G69/46 , C08G64/30 , C08G63/90 , C08F6/28 , B01D1/00
CPC分类号： B01D1/22 , C08F6/001 , C08G63/785 , C08G63/90 , C08G64/205 , C08G64/406
摘要： It is an object of the present invention, in the case of an apparatus in which a liquid containing material having a lower boiling point than that of the liquid is made to flow down along an external surface of a guide, during which time the lower boiling point material is evaporated, to provide a specific apparatus that can be operated stably for a prolonged period of time on an industrial scale such that not less than 1 ton/hr of the liquid is subjected to the evaporation, and furthermore to provide a specific industrial evaporation apparatus in which there are no problems due to degeneration caused by some of the liquid residing in the apparatus for a prolonged period of time. The present inventors have reached to the present invention upon discovering that the above object can be attained, and a high-quality and high-purity concentrated liquid or condensation polymer or thermoplastic polymer can easily be obtained, by using an industrial evaporation apparatus having a specified structure in which there are guides that do not themselves have a heat source, a flow path controlling member having a function of making the liquid fed onto a perforated plate from a liquid receiving port flow mainly from a peripheral portion toward a middle portion of the perforated plate is provided in a liquid feeding zone, the ratio of the volume V (m3) of the space in which the liquid can be present in the liquid feeding zone from the bottom of the liquid receiving port (i.e. the joint between the liquid receiving port and a top internal wall of the liquid feeding zone) to an upper surface of the perforated plate, and the upper surface area T (m2) of the perforated plate including the upper surface area of the holes therein, i.e. the value of V/T, is in a specified range (formula (6)), and formulae (1) to (5), or formulae (1) to (11), or formulae (1) to (13), are satisfied.

53. 发明申请

US20070283904A1 Industrial Evaporation Apparatus 审中-公开
公开(公告)号：US20070283904A1
公开(公告)日：2007-12-13
申请号：US11667490
申请日：2005-12-01
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： F22B37/00
CPC分类号： C08F6/001 , B01D1/22 , C08G63/785 , C08G64/205
摘要： It is an object of the present invention, in the case of an apparatus in which a liquid containing material having a lower boiling point than that of the liquid is made to flow down along an external surface of a guide, during which time the lower boiling point material is evaporated, to provide a specific apparatus that can be operated stably for a prolonged period of time on an industrial scale such that not less than 1 ton/hr of the liquid is subjected to the evaporation, and furthermore to provide a specific industrial evaporation apparatus in which there are no problems due to degeneration caused by some of the liquid residing in the apparatus for a prolonged period of time. The present inventors have reached to the present invention upon discovering that the above object can be attained, and a high-quality and high-purity concentrated liquid or condensation polymer or thermoplastic polymer can easily be obtained, by using an industrial evaporation apparatus having a specified structure in which there are guides that do not themselves have a heat source, a flow path controlling member having a function of making the liquid fed onto a perforated plate from a liquid receiving port flow mainly from a peripheral portion toward a middle portion of the perforated plate is provided in a liquid feeding zone, the ratio of the volume V (m3) of the space in which the liquid can be present in the liquid feeding zone from the bottom of the liquid receiving port (i.e. the joint between the liquid receiving port and a top internal wall of the liquid feeding zone) to an upper surface of the perforated plate, and the upper surface area T (m2) of the perforated plate including the upper surface area of the holes therein, i.e. the value of V/T, is in a specified range (formula (6)), and formulae (1) to (5), or formulae (1) to (12), or formulae (1) to (14), are satisfied.

54. 发明授权

US07658817B2 Industrial evaporation apparatus 有权
标题翻译：工业蒸发装置
公开(公告)号：US07658817B2
公开(公告)日：2010-02-09
申请号：US11666464
申请日：2005-11-29
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： B01D1/00 , B01D1/30
CPC分类号： B01D1/22 , C08G63/785 , C08G63/90 , C08G64/205 , C08G64/406 , Y10S159/37
摘要： An industrial evaporation apparatus having a specified structure in which there are guides that do not themselves have a heat source, a flow path controlling member having a function of making the liquid fed onto a perforated plate from a liquid receiving port flow mainly from a peripheral portion toward a central portion of the perforated plate is provided in a liquid feeding zone, and formula (1) to (5), or formula (1) to (10), or formula (1) to (12), are satisfied.
摘要翻译：具有特定结构的工业蒸发装置，其中存在不具有热源的导向件，具有使从液体接收口供给到多孔板上的液体主要从周边部分流出的功能的流路控制构件设置在供液区域中，并且满足公式（1）至（5）或式（1）至（10）或式（1）至（12）。

55. 发明授权

US07479258B2 Method for producing an aromatic polycarbonate 有权
标题翻译：芳香族聚碳酸酯的制造方法
公开(公告)号：US07479258B2
公开(公告)日：2009-01-20
申请号：US10592523
申请日：2005-06-14
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： C08G63/00 , C08G64/00
CPC分类号： B01J19/24 , B01J2219/185 , B01J2219/1946 , C08G64/205 , C08G64/307
摘要： It is a task of the present invention to provide a method for producing a high quality, high performance aromatic polycarbonate (which is colorless and has excellent mechanical properties) from a molten aromatic polycarbonate prepolymer obtained by reacting an aromatic dihydroxy compound with a diaryl carbonate, wherein the polycarbonate can be stably produced on a commercial scale at 1 to 50 t/hr for a long time. In the present invention, this task has been accomplished by a method for producing an aromatic polycarbonate by the melt transesterification process, in which the prepolymer is polymerized by a guide-wetting fall polymerizer device having a specific structure, whereby a high quality, high performance aromatic polycarbonate as mentioned above can be stably produced on a commercial scale at 1 to 50 t/hr for a long time (more than several thousand hours, e.g., more than 5,000 hours) without fluctuation of the molecular weight thereof.
摘要翻译：本发明的任务是提供一种通过使芳族二羟基化合物与碳酸二芳酯反应获得的熔融芳族聚碳酸酯预聚物制备高质量，高性能的芳族聚碳酸酯（其为无色且具有优异的机械性能）的方法，其中聚碳酸酯可以长期以1至50t / hr的商业规模稳定地制备。在本发明中，通过熔融酯交换法制造芳族聚碳酸酯的方法已经完成了该任务，其中预聚物通过具有特定结构的引导润湿落下聚合反应器进行聚合，从而获得高品质，高性能如上所述的芳香族聚碳酸酯可以在1〜50t / hr的长时间（超过数千小时，例如5000小时以上）下稳定地以工业规模生产，而且其分子量不变。

56. 发明申请

US20070260095A1 Process for the Industrial Production of Aromatic Carbonate 审中-公开
标题翻译：芳香族碳酸盐工业生产工艺
公开(公告)号：US20070260095A1
公开(公告)日：2007-11-08
申请号：US11630324
申请日：2005-06-20
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , B01D3/14 , Y02P20/127 , C07C69/96
摘要： It is an object of the present invention to provide a specific process that enables an aromatic carbonate to be produced with high selectivity and high productivity stably for a prolonged period of time on an industrial scale of no less than 1 ton per hour using a continuous multi-stage distillation column from a dialkyl carbonate and an aromatic monohydroxy compound. Although there have been many proposals regarding the process of producing the aromatic carbonate using a reactive distillation method, these have all been on a small scale and a short operating time laboratory level, According to the present invention, there is provided a specified continuous multi-stage distillation column, and there is also provided a specific process that enables the aromatic carbonate to be produced with high selectivity and high productivity stably for a prolonged period of time on an industrial scale of not less than 1 ton per hour from the dialkyl carbonate and the aromatic monohydroxy compound.
摘要翻译：本发明的一个目的是提供一种具体方法，其可以使用连续的多次，以不低于1吨/小时的工业规模，以高选择性和高生产率稳定地长时间地制备芳族碳酸酯级烷基碳酸酯和芳族单羟基化合物。虽然关于使用反应蒸馏法生产芳族碳酸酯的方法已经有许多建议，但是这些都是在小规模和短的操作时间实验室水平。根据本发明，提供了一种特定的连续多级并且还提供了一种具体方法，其能够以高于1吨/小时的工业规模从碳酸二烷基酯稳定地长时间稳定地制备芳族碳酸酯，并且芳族单羟基化合物。

57. 发明申请

US20070148055A1 Polymerizer device for producing an aromatic polycarbonate 有权
标题翻译：用于生产芳族聚碳酸酯的聚合装置
公开(公告)号：US20070148055A1
公开(公告)日：2007-06-28
申请号：US10593394
申请日：2005-06-16
申请人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
发明人： Shinsuke Fukuoka , Hiroshi Hachiya , Kazuhiko Matsuzaki
IPC分类号： B01J19/32 , B01J19/24
CPC分类号： B01J19/24 , B01J2219/00094 , B01J2219/185 , B01J2219/1946 , C08G64/205 , C08G64/307
摘要： It is a task of the present invention to provide a polymerizer device and a polymerizer system which enable the production, by melt transesterification, of a high quality, high performance aromatic polycarbonate (which is colorless and has excellent mechanical properties) from a molten aromatic polycarbonate prepolymer obtained by reacting an aromatic dihydroxy compound with a diaryl carbonate, wherein the polycarbonate can be stably produced on a commercial scale at 1 to 50 t/hr for a long time. In the present invention, this task has been accomplished by a guide-wetting fall polymerizer device (in which a molten prepolymer is allowed to fall along and in contact with a guide, thereby effecting polymerization of the prepolymer) having a specific structure and a polymerizer system comprising such devices. That is, the device and the system have enabled the stable production of a high quality, high performance aromatic polycarbonate as mentioned above at 1 to 50 t/hr for a long time (more than several thousand hours, e.g., as long as 5,000 hours) without fluctuation of the molecular weight thereof.
摘要翻译：本发明的任务是提供一种能够通过熔融酯交换从熔融芳族聚碳酸酯生产高质量，高性能的芳族聚碳酸酯（其是无色且具有优异的机械性能）的聚合反应器装置和聚合反应器系统。通过使芳族二羟基化合物与碳酸二芳酯反应得到的预聚物，其中聚碳酸酯可以长期以1〜50t / hr的规模以商业规模稳定地制造。在本发明中，这个任务已经通过引导润湿下降聚合器装置（其中允许熔融预聚物沿着导向件落下并与导向器接触，从而实现具有特定结构的聚合反应）和聚合反应器包括这种装置的系统。也就是说，该装置和系统使得能够长时间以1至50t / hr稳定地生产如上所述的高质量，高性能的芳族聚碳酸酯（多于几千小时，例如长达5,000小时），其分子量不变。

58. 发明申请

US20050159518A1 Moldings of flame-retardant aromatic polycarbonate resin compositions 有权
标题翻译：阻燃芳香族聚碳酸酯树脂组合物的成型品
公开(公告)号：US20050159518A1
公开(公告)日：2005-07-21
申请号：US10507903
申请日：2003-03-18
申请人： Akira Miyamoto , Toshiharu Sakuma , Kazuhiro Shibuya , Hiroshi Hachiya , Hiroshi Hachiya
发明人： Akira Miyamoto , Toshiharu Sakuma , Kazuhiro Shibuya , Hiroshi Hachiya , Hiroshi Hachiya
IPC分类号： C08K5/42 , C08K7/00 , C08L69/00 , B29C45/26 , B29C45/00 , B29C45/76 , C08K3/18 , C08K3/34 , C08K5/41
CPC分类号： C08L69/00 , B29K2027/12 , B29K2069/00 , B29K2105/0026 , B29K2105/16 , B29K2995/0016 , B29K2995/0088 , C08K5/42 , C08K7/00 , C08L2666/04
摘要： A molded article produced by injection-molding a molten form of a flame-retardant aromatic polycarbonate resin composition comprising: 100 parts by weight of an aromatic polycarbonate (A) (Mw: 17,000 to 35,000), 0.01 to 3 parts by weight of inorganic compound particles (B) (average diameter: 10 nm to 10 μm), 0.001 to 0.5 part by weight of an alkali metal salt (C) of an organic sulfonic acid, and 0.01 to 0.5 part by weight of a fluoropolymer (D), wherein the largest FL/t ratio of the molded article is 50 or more, wherein FL is a flow length of the composition in a mold and t is a thickness of the molded article, the FL/t ratios being obtained by measuring the thicknesses of the molded article at portions corresponding to flow paths (L) (from a gate to points at which the flow of the composition stops) of the composition in the mold during the molding, and calculating an integral of (dL/T′) along each (L) (dL: length of a segment of (L), t′: thickness of the molded article at a portion corresponding to the segment), wherein the calculated integrals are defined as the FL/t ratios.
摘要翻译：通过注塑成型熔融形式的阻燃性芳香族聚碳酸酯树脂组合物而制造的成型体，其包含：100重量份芳香族聚碳酸酯（A）（Mw：17,000〜35,000），0.01〜3重量份的无机化合物颗粒（B）（平均直径：10nm至10μm），0.001至0.5重量份的有机磺酸的碱金属盐（C）和0.01至0.5重量份的含氟聚合物（D），其中成型体的最大FL / t比为50以上，其中，FL为成型体的成型体的流动长度，t为成型品的厚度，FL / t比是通过测定模制品在成形期间对应于流动路径（L）（从浇口到组合物流动的点停止的部分），并计算每个（dL / T'）的积分（dL / T'） L）（dL：（L）的段的长度，t'：成形品的一部分的厚度对应于该段），其中所计算的积分被定义为FL / t比。

59. 发明申请

US20120263642A1 METHOD FOR IMPROVING COERCIVE FORCE OF EPSILON-TYPE IRON OXIDE, AND EPSILON-TYPE IRON OXIDE 有权
标题翻译：改善EPSILON型氧化铁和EPSILON型氧化铁的强化力的方法
公开(公告)号：US20120263642A1
公开(公告)日：2012-10-18
申请号：US13499172
申请日：2010-09-30
申请人： Shin-ichi Ohkoshi , Shunsuke Sakurai , Asuka Namai , Sayaka Umeda , Hiroshi Hachiya , Kazuyuki Matsumoto , Takashi Gotoh
发明人： Shin-ichi Ohkoshi , Shunsuke Sakurai , Asuka Namai , Sayaka Umeda , Hiroshi Hachiya , Kazuyuki Matsumoto , Takashi Gotoh
IPC分类号： C01G55/00
CPC分类号： H01F1/047 , C01G49/0018 , C01G49/06 , C01P2002/50 , C01P2002/52 , C01P2006/42 , C04B35/26 , C04B35/62826 , C04B2235/3217 , C04B2235/3286 , C04B2235/3289 , C04B2235/3418 , C04B2235/761 , H01F1/10
摘要： To provide a method for improving a coercive force of epsilon-type iron oxide particles, and an epsilon-type iron oxide. Specifically, to provide a method for improving the coercive force of an epsilon-type iron oxide comprising: substituting Fe-site of the epsilon-type iron oxide with other element, while not substituting Fe of D-site in the epsilon-type iron oxide with other element, and the epsilon type iron oxide.
摘要翻译：提供一种改善ε型氧化铁颗粒和ε型氧化铁的矫顽力的方法。具体地，提供一种改进ε型氧化铁的矫顽力的方法，包括：用其它元素代替ε型氧化铁的Fe部位，而不是在ε型氧化铁中代替D位的Fe 与其他元素，和epsilon型氧化铁。

60. 发明授权

US07563858B2 Method for stably producing an aromatic polycarbonate 有权
标题翻译：稳定生产芳族聚碳酸酯的方法
公开(公告)号：US07563858B2
公开(公告)日：2009-07-21
申请号：US10593035
申请日：2005-06-14
申请人： Ichiro Kakihara , Hiroshi Hachiya
发明人： Ichiro Kakihara , Hiroshi Hachiya
IPC分类号： C08G64/00 , C08G63/00
CPC分类号： C08G64/205 , C08G64/307
摘要： A method for stably producing an aromatic polycarbonate, which comprises continuously reacting an aromatic dihydroxy compound with a diaryl carbonate in a closed, reactor-pipeline system, the closed, reactor-pipeline system comprising: a plurality of reactors which are liquid-tightly connected through a pipeline toward an outlet for a final aromatic polycarbonate product, the pipeline comprising one or more pipes, wherein the plurality of reactors include at least two reactors connected in series, and at least one filter secured in the pipe or pipes of the reactor-pipeline system, wherein the or each filter is simultaneously or separately taken out to the outside of the reactor-pipeline system and subjected to washing in the outside of the reactor-pipeline system, followed by returning of the resultant washed filter into the inside of the pipe or pipes of the reactor-pipeline system, the washing being performed with the below-mentioned washing agents used in the following order: an aqueous solution of a basic compound, an aromatic monohydroxy compound, and a molten mixture of an aromatic dihydroxy compound and a diaryl carbonate, the molten mixture containing a basic compound.
摘要翻译：一种用于稳定制备芳族聚碳酸酯的方法，其包括使芳族二羟基化合物与碳酸二芳基酯在封闭的反应器 - 管道系统中连续反应，所述封闭的反应器 - 管道系统包括：多个反应器，其通过用于最终芳族聚碳酸酯产品的出口的管道，所述管道包括一个或多个管道，其中所述多个反应器包括串联连接的至少两个反应器，以及固定在所述反应器管道的管道中的至少一个过滤器系统，其中所述或每个过滤器同时或分别取出到反应器 - 管道系统的外部，并在反应器 - 管道系统的外部进行洗涤，然后将所得的洗涤过滤器返回到管道内部或反应器 - 管道系统的管道，用下列洗涤剂按以下顺序进行洗涤：水碱性化合物，芳族单羟基化合物和芳族二羟基化合物和碳酸二芳基酯的熔融混合物的有效溶液，所述熔融混合物含有碱性化合物。

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