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51. 发明授权

US07459571B2 Catalyst extrudates based on copper oxide and their use for hydrogenating carbonyl compounds 有权
标题翻译：基于氧化铜的催化剂挤出物及其用于氢化羰基化合物的用途
公开(公告)号：US07459571B2
公开(公告)日：2008-12-02
申请号：US11934266
申请日：2007-11-02
申请人： Stephan Schlitter , Olga Schubert , Michael Hesse , Sabine Borchers , Markus Roesch , Rolf Pinkos , Alexander Weck , Gunther Windecker
发明人： Stephan Schlitter , Olga Schubert , Michael Hesse , Sabine Borchers , Markus Roesch , Rolf Pinkos , Alexander Weck , Gunther Windecker
IPC分类号： C07D307/00 , C07D307/02
CPC分类号： B01J23/72 , B01J21/04 , B01J23/94 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/108 , B01J37/0009 , B01J37/18 , B01J38/10 , B01J38/12 , C07C29/149 , C07D315/00 , Y02P20/584
摘要： Catalyst in the form of an extrudate which comprises from 5 to 85% by weight of copper oxide and in which the same oxidic support material is present in the active composition and as binder, and the use of the catalyst for the hydrogenation of carbonyl compounds.
摘要翻译：挤出物形式的催化剂，其包含5至85重量％的氧化铜，其中相同的氧化性载体材料存在于活性组合物中并作为粘合剂，以及使用催化剂用于羰基化合物的氢化。

52. 发明授权

US07449609B2 Method for production of 1,6-hexanediol with a purity in excess of 99.5% 失效
标题翻译：制备纯度超过99.5％的1,6-己二醇的方法
公开(公告)号：US07449609B2
公开(公告)日：2008-11-11
申请号：US10569980
申请日：2005-07-07
申请人： Andrea Haunert , Rolf Pinkos , Thomas Krug , Tilman Sirch , Michael Koch , Gerd-Dieter Tebben
发明人： Andrea Haunert , Rolf Pinkos , Thomas Krug , Tilman Sirch , Michael Koch , Gerd-Dieter Tebben
IPC分类号： C07C29/149
CPC分类号： C07C29/145 , C07C29/149 , C07C2601/14 , C07C31/20 , C07C35/08
摘要： The present invention provides a process for preparing 1,6-hexanediol by hydrogenating dialkyl adipates, alkyl 6-hydroxycaproates, 1,4-cyclohexanedione and 4-hydroxycyclohexan-1-one as ester mixtures comprising impurities, by a) freeing resulting the esterification mixture of excess alcohol and low boilers in a first distillation stage (alcohol removal), b) carrying out a separation of the bottom product in a second distillation stage into an ester fraction substantially free of 1,4-cyclohexanediols and a fraction comprising at least the majority of the 1,4-cyclohexanediols, c) catalytically hydrogenating the ester fraction substantially free of 1,4-cyclohexanediols (ester hydrogenation) and d) in a purifying distillation stage, obtaining 1,6-hexanediol from the hydrogenation effluent in a manner known per se, which comprises selectively hydrogenating the ester mixture before stage a) and/or before stage b) (purifying hydrogenation).
摘要翻译：本发明提供了一种通过以下方式制备1,6-己二醇的方法：通过以下方法将氢化己二酸二烷基酯，6-羟基己酸烷基酯，1,4-环己二酮和4-羟基环己烷-1-酮作为包含杂质的酯混合物，在第一蒸馏阶段（醇去除）中的过量醇和低锅炉的b），b）在第二蒸馏阶段中将底部产物分离成基本上不含1,4-环己烷二醇的酯馏分和至少包含大部分1,4-环己烷二醇，c）催化氢化基本上不含1,4-环己二醇的酯馏分（酯氢化）和d）在纯化蒸馏阶段，以一种方式从氢化流出物中获得1,6-己二醇本身已知，其包括在阶段a）和/或阶段b）之前选择性地氢化酯混合物（纯化氢化）。

53. 发明申请

US20060264679A1 Method for the production of tetrahydrofuran copolymers 审中-公开
标题翻译：生产四氢呋喃共聚物的方法
公开(公告)号：US20060264679A1
公开(公告)日：2006-11-23
申请号：US10551142
申请日：2004-03-30
申请人： Martin Haubner , Rolf Pinkos , Stephan Sclitter
发明人： Martin Haubner , Rolf Pinkos , Stephan Sclitter
IPC分类号： C07C41/03
CPC分类号： C08G65/20 , C08G2650/08 , C08G2650/68
摘要： The present invention relates to a process for the single-stage preparation of polyoxyalkylene glycols by copolymerization of THF and neopentyl glycol in the presence of a heteropolyacid, wherein the total amount of all impurities of the formula (I) where R1 and R2 are each hydrogen when R3 is an oxyformyl or isopropionate radical, R1 is hydrogen and R2 is hydroxy when R3 is an isopropyl radical and R1 is hydrogen when R2 and R3 together form an —OCH2—C(CH3)—CH2— radical, in the neopentyl glycol is less than 1000 ppm.
摘要翻译：本发明涉及通过THF和新戊二醇在杂多酸的存在下共聚制备聚氧亚烷基二醇的方法，其中式（I）的所有杂质的总量，其中R 1， R 2和R 2各自为氢，当R 3为氧甲酰基或异丙酸基团时，R 1为氢，R 2为氢，当R 3是异丙基时，R 2是羟基，当R 2和R 3独立地是R 1时，R 1是氢，一起形成-OCH 2 -C（CH 3 CH 3）-CH 2 - 基，在新戊二醇中小于1000ppm 。

54. 发明申请

US20060258837A1 Method of producing tetrahydrofuran copolymers 失效
标题翻译：生产四氢呋喃共聚物的方法
公开(公告)号：US20060258837A1
公开(公告)日：2006-11-16
申请号：US10551137
申请日：2004-03-30
申请人： Martin Haubner , Rolf Pinkos
发明人： Martin Haubner , Rolf Pinkos
IPC分类号： C08G59/00
CPC分类号： C08G65/2666 , C08G65/20
摘要： The present invention relates to a process for the single-stage preparation of polyoxyalkylene glycols by copolymerization of THF and alpha, omega-diols in the presence of a heteropolyacid, wherein the content of organically bound nitrogen in the alpha, omega-diol is less than 15 ppm.
摘要翻译：本发明涉及通过THF和α，ω-二醇在杂多酸的存在下共聚制备聚氧亚烷基二醇的方法，其中α，ω-二醇中的有机结合的氮的含量小于 15 ppm。

55. 发明授权

US07084312B1 Catalyst and method for hydrogenating carbonyl compounds 有权
标题翻译：氢化羰基化合物的催化剂和方法
公开(公告)号：US07084312B1
公开(公告)日：2006-08-01
申请号：US10070275
申请日：2000-08-22
申请人： Sylvia Huber , Michael Jolyon Sprague , Boris Breitscheidel , Joachim Wulff-Döring , Michael Hesse , Rolf Pinkos , Shelue Liang , Otto Kumberger , Marc Walter
发明人： Sylvia Huber , Michael Jolyon Sprague , Boris Breitscheidel , Joachim Wulff-Döring , Michael Hesse , Rolf Pinkos , Shelue Liang , Otto Kumberger , Marc Walter
IPC分类号： C07C29/136 , C07C29/14 , C07C29/141 , C07C29/143 , C07C29/147
CPC分类号： B01J23/80 , C07C29/149 , C07C31/20
摘要： A process for the hydrogenation of an organic compound containing at least one carbonyl group comprises bringing the organic compound in the presence of hydrogen into contact with a shaped body which can be produced by a process in which (i) an oxidic material comprising copper oxide, zinc oxide and aluminum oxide is made available, (ii) pulverulent metallic copper or pulverulent cement or a mixture thereof is added to the oxidic material, and (iii) the mixture resulting from (ii) is shaped to form a shaped body.
摘要翻译：氢化含有至少一个羰基的有机化合物的方法包括使氢存在下的有机化合物与成形体接触，成形体可以通过以下工艺制备，其中（i）包含氧化铜的氧化物，提供氧化锌和氧化铝，（ii）将粉末状金属铜或粉状水泥或其混合物加入到氧化物中，和（iii）由（ii）得到的混合物成形为成形体。

56. 发明申请

US20060167321A1 METHOD FOR PRODUCING TETRAHYDROFURANE COPOLYMERS 失效
标题翻译：生产四氢呋喃共聚物的方法
公开(公告)号：US20060167321A1
公开(公告)日：2006-07-27
申请号：US10524555
申请日：2003-07-30
申请人： Martin Haubner , Rolf Pinkos , Alexander Weck
发明人： Martin Haubner , Rolf Pinkos , Alexander Weck
IPC分类号： C07C41/01
CPC分类号： C08G65/20
摘要： The present invention provides a process for one-stage preparation of polyoxyalkylene glycols by copolymerizing tetrahydrofuran and alpha,omega-diols in the presence of a heteropolyacid and of a hydrocarbon, which comprises distilling water in a mixture with this hydrocarbon out of the copolymerization.
摘要翻译：本发明提供了通过在杂多酸和烃的存在下共聚合四氢呋喃和α，ω-二醇来一步法制备聚氧亚烷基二醇的方法，该方法包括在共聚合中将与该烃的混合物中的水蒸馏出来。

57. 发明申请

US20060142543A1 Method for the polymerization of cyclic ethers 失效
公开(公告)号：US20060142543A1
公开(公告)日：2006-06-29
申请号：US10540510
申请日：2003-12-23
申请人： Stephan Schlitter , Martin Haubner , Peter Zehner , Michael Hesse , Alexander Weck , Rolf Pinkos , Thomas Grabler
发明人： Stephan Schlitter , Martin Haubner , Peter Zehner , Michael Hesse , Alexander Weck , Rolf Pinkos , Thomas Grabler
IPC分类号： C08G59/00 , C07C41/03
CPC分类号： C08G65/2654 , C08G65/2657
摘要： The present invention relates to a process for preparing polytetrahydrofuran, polytetrahydrofuran copolymer, diester or monoester by polymerizing tetrahydrofuran in the presence of at least one telogen and/or comonomer and of an acidic heterogeneous catalyst based on activated sheet silicates or mixed metal oxides in a fluidized bed.

58. 发明申请

US20060052550A1 Method for the production of tetrahydrofuran copolymers 失效
公开(公告)号：US20060052550A1
公开(公告)日：2006-03-09
申请号：US10537962
申请日：2003-12-16
申请人： Martin Haubner , Rolf Pinkos
发明人： Martin Haubner , Rolf Pinkos
IPC分类号： C08G59/14
CPC分类号： C08G65/20 , C08G65/2666
摘要： The present invention provides a process for preparing polyoxyalkylene glycols of a certain molecular weight in one stage by copolymerizing tetrahydrofuran and alpha,omega-diols as the comonomer in the presence of a heteropolyacid and of a hydrocarbon, by distilling off a mixture of water and this hydrocarbon from the copolymerization, which comprises terminating the polymerization when this molecular weight is attained by adding water, comonomer, butanediol or butanediol-water mixtures.

59. 发明申请

US20050176972A1 Catalytic hydrogenation over rhenium-containing catalysts supported on activated carbon 失效
标题翻译：通过负载在活性炭上的含铼催化剂进行催化氢化
公开(公告)号：US20050176972A1
公开(公告)日：2005-08-11
申请号：US11104408
申请日：2005-04-13
申请人： Rolf-Hartmuth Fischer , Rolf Pinkos , Stephan Schunk , Joachim Wulff-Doring , Frank Stein , Thomas Nobel , Sylvia Huber
发明人： Rolf-Hartmuth Fischer , Rolf Pinkos , Stephan Schunk , Joachim Wulff-Doring , Frank Stein , Thomas Nobel , Sylvia Huber
IPC分类号： B01J21/18 , B01J23/656 , B01J23/89 , C07C29/17 , C07D307/26 , C07C31/18
CPC分类号： C07C29/177 , B01J21/18 , B01J23/6567 , B01J23/8986 , C07C2601/20 , C07C31/207 , C07C31/20 , C07C31/133
摘要： In a process for preparing alcohols by catalytic hydrogenation of carbonyl compounds over a catalyst comprising rhenium on activated carbon, the catalyst used comprises rhenium (calculated as metal) in a weight ratio to the activated carbon of from 0.0001 to 0.5, platinum (calculated as metal) in a weight ratio to the activated carbon of from 0.0001 to 0.5 and, if appropriate, at least one further metal selected from among Zn, Cu, Ag, Au, Ni, Fe, Ru, Mn, Cr, Mo, W and V in a weight ratio to the activated carbon of from 0 to 0.25, and the activated carbon has been nonoxidatively pretreated. It is also possible to prepare ethers and lactones if the hydrogen pressure is not more than 25 bar. In this case, the activated carbon in the catalyst may also have been nonoxidatively pretreated.
摘要翻译：在通过羰基化合物催化氢化羰基化合物的方法中，所用的催化剂包括铼在活性炭上的催化剂，所用的催化剂包括铼（以金属计）与活性炭的重量比为0.0001至0.5，铂（以金属计算），活性炭的重量比为0.0001〜0.5，如果合适，选自Zn，Cu，Ag，Au，Ni，Fe，Ru，Mn，Cr，Mo，W和V中的至少一种以上的金属活性炭的重量比为0至0.25，并且活性炭已经被非氧化预处理。如果氢气压力不超过25巴，也可制备醚和内酯。在这种情况下，催化剂中的活性炭也可以被非氧化预处理。

60. 发明授权

US06673920B2 Method for the production of N-alkenyl-amides 失效
标题翻译：制备N-烯基酰胺的方法
公开(公告)号：US06673920B2
公开(公告)日：2004-01-06
申请号：US10168211
申请日：2002-06-19
申请人： Thomas Preiss , Arnd Böttcher , Rolf Pinkos , Rudolf Erich Lorenz
发明人： Thomas Preiss , Arnd Böttcher , Rolf Pinkos , Rudolf Erich Lorenz
IPC分类号： C07D22310
CPC分类号： C07D207/267 , C07C231/08 , C07D211/76 , C07D223/10
摘要： A process for preparing N-alkenyl-amides by reacting the corresponding NH-amides with acetylenes in the liquid phase in the presence of basic alkali metal compounds and of a cocatalyst comprises using as the cocatalyst diols of the general formula (I) where X is branched or unbranched alkylene selected from the group consisting of where R1 to R6 are independently hydrogen or C1- to C4-alkyl; or branched or unbranched cyclic alkylene of 3 to 14 carbon atoms including 3 to 12 ring carbon atoms, their monoalkenyl ethers, their dialkenyl ethers or mixtures thereof.
摘要翻译：在碱性碱金属化合物和助催化剂存在下，通过使液相中相应的NH-酰胺与乙炔反应来制备N-烯基酰胺的方法包括使用通式（I）的助催化剂二醇，其中X支化或非支链的亚烷基，其中R 1至R 6独立地为氢或C 1至C 4 - 烷基;包含3至12个环碳原子的3至14个碳原子的支链或非支链环状亚烷基，它们的单链烯基醚，它们的二链烯基醚或其混合物。

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