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51. 发明授权

US4500448A 1-Hydroxymethyl cyclopropanes organoleptic use of same 失效
标题翻译： 1-羟甲基环丙烷的感官使用相同
公开(公告)号：US4500448A
公开(公告)日：1985-02-19
申请号：US541275
申请日：1983-10-12
申请人： Richard M. Boden , Marie R. Hanna , Theodore J. Tyszkiewicz
发明人： Richard M. Boden , Marie R. Hanna , Theodore J. Tyszkiewicz
IPC分类号： A23G4/00 , A23G4/06 , A23L27/20 , C11D3/50 , A61K7/46
CPC分类号： A23G4/06 , A23L27/203 , C11D3/50
摘要： Described are 1-hydroxymethyl-2-acyl cyclopropane derivatives defined according to the structure: ##STR1## wherein Z represents hydrogen, acyl having the structure: ##STR2## and substituted oxyacyl having the structure: ##STR3## and cyclic condensation products thereof having the structure: ##STR4## wherein R.sub.1, R.sub.2 and R.sub.3 represent C.sub.1 -C.sub.10 alkyl; wherein R.sub.1 ' represents C.sub.1 -C.sub.10 alkylidene and wherein R.sub.4, R.sub.5, R.sub.6 and R.sub.7 represent hydrogen or C.sub.1 -C.sub.3 lower alkyl; processes for preparing same by means of a reaction of a halomethyloxirane or substituted halomethyloxirane with a substituted 1,3-propanedione derivative; and organoleptic uses of such 1-hydroxymethyl-2-acyl cyclopropane derivatives in augmenting or enhancing the aroma or taste of perfume compositions, perfumed articles (e.g. solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, perfumed polymers, hair preparations and shampoos), colognes, foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos.
摘要翻译：描述的是根据以下结构定义的1-羟甲基-2-酰基环丙烷衍生物：其中Z代表氢，具有以下结构的酰基：具有以下结构的取代的氧酰基：其具有下式的环状缩合产物：结构：其中R 1，R 2和R 3表示C 1 -C 10烷基; 其中R1'表示C1-C10亚烷基，其中R4，R5，R6和R7表示氢或C1-C3低级烷基; 通过卤代环氧丙烷或取代的卤代甲基环氧乙烷与取代的1,3-丙二酮衍生物的反应制备其的方法; 以及这种1-羟甲基-2-酰基环丙烷衍生物在增强或增强香料组合物，香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品）中的香味或味道的感官用途，加香聚合物，头发制剂和洗发剂），古龙水，食品，口香糖，牙膏，药用产品和咀嚼烟草。

52. 发明授权

US4448984A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4448984A
公开(公告)日：1984-05-15
申请号：US458890
申请日：1983-01-18
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C43/162 , C07C35/28 , C07C67/035 , C07C67/04
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++] is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

53. 发明授权

US4398038A Oxoalkyl esters 失效
标题翻译：氧代烷基酯
公开(公告)号：US4398038A
公开(公告)日：1983-08-09
申请号：US396290
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C07D319/08 , C11B9/00 , C07C69/76
CPC分类号： C07D319/08 , C11B9/0015 , C11B9/0061 , Y02P20/582
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or switterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后，如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（例如加香聚合物，或固体或液体阴离子，阳离子，非离子或转换洗涤剂，织物柔软剂组合物，干燥剂加入的织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

54. 发明授权

US4391284A Use in modifying smoking tobacco aroma and flavor or mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
标题翻译：用于改变吸烟烟草香气和风味或单氧甲基取代的多羟基甲基萘衍生物
公开(公告)号：US4391284A
公开(公告)日：1983-07-05
申请号：US354387
申请日：1982-03-02
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A24B3/12 , A24B15/30
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described is the use in modifying, augmenting or enhancing the aroma or taste of smoking tobacco products of mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl.
摘要翻译：描述了用于改变，增强或增强具有以下通用结构的单氧代甲基取代的多羟基甲基萘衍生物的烟草产品的香气或味道：其中虚线表示碳 - 碳单键或碳 - 碳双键; 其中R1，R1'，R1“，R1”，R1“，R3，R5，R5'，R5”，R5“，R5”和R6表示氢或甲基，条件：（i）R1，R1'，R1“，R1”和R1“”中的至少四个为氢; 和（ii）R5，R5'，R5“，R5”和R5“中的至少四个表示氢; （ⅰ）具有以下结构的甲醛：（ⅱ）具有以下结构的亚烷基二氧基或二烷氧基甲基：（ⅲ）具有以下结构的羟基甲基：（ⅳ）具有以下结构的乙酰氧基甲基：其中R7和R8分别代表C1-C4低级烷基或R7和R8一起代表C2-C4亚烷基; 其中由以下各项表示的线：[++++]是（i）当R 7和R 8一起为C 2 -C 4亚烷基时的碳 - 碳单键或（ii）当R7和R8分别表示C1 -C4低级烷基。

55. 发明授权

US4390448A Perfumed stable aqueous hypochlorite bleach compositions containing 2-methyl-2-octanol and thickened variation thereof 失效
标题翻译：含有2-甲基-2-辛醇的稀释稳定的含水次氯酸盐漂白剂组合物及其增稠变化
公开(公告)号：US4390448A
公开(公告)日：1983-06-28
申请号：US313685
申请日：1981-10-22
申请人： Richard M. Boden , Michael Licciardello , Joseph J. Maisano, Jr. , Marie R. Hanna
发明人： Richard M. Boden , Michael Licciardello , Joseph J. Maisano, Jr. , Marie R. Hanna
IPC分类号： A01N59/00 , C11D1/24 , C11D1/75 , C11D3/395 , C11D3/50 , C11D7/54
CPC分类号： C11D3/50 , A01N59/00 , C11D3/3956 , C11D1/24 , C11D1/75
摘要： Described is a process for producing a stable single phase aqueous alkali metal hypochlorite solution having good surface tension properties and optionally having a relatively high viscosity (5-25 centipoises at 20.degree.-40.degree. C.) and having a stable fragrance consisting, in sequential order, of the steps of (a) adjusting the pH of an aqueous alkali metal hypochlorite solution to the range of 11-14.0; (b) admixing a composition of matter selected from the group consisting of: (i) a chemical compound having the structure: ##STR1## wherein at least one of R.sub.1 and R.sub.2 is C.sub.10 -C.sub.12 straight chain or branched chain alkyl and M.sub..alpha. and M.sub..beta. are the same or different and each represents alkali metal selected from the group consisting of lithium, potassium and sodium; and (ii) a mixture of at least one compound having the structure: ##STR2## and a compound having the structure: ##STR3## wherein R.sub.3 "' is straight chain alkyl; wherein more than 55% of the R.sub.3 "' moieties consist of straight chain alkyl having from 11 up to 13 carbon atoms and wherein A and B are each separately methyl or taken together complete a morpholine ring, with a perfuming quantity of 2-methyl-2-octanol whereby a premix is formed; (c) optionally adding to said premix a gel-forming agent selected from the group consisting of sodium palmitate, lithium palmitate, potassium palmitate, sodium laurate, lithium laurate, potassium laurate, sodium stearate, potassium stearate and lithium stearate; and (d) adding said premix to the pH-adjusted hypochlorite solution.
摘要翻译：描述了一种制备稳定的单相碱金属碱金属次氯酸盐溶液的方法，该溶液具有良好的表面张力特性，并且任选具有较高的粘度（在20-40℃下为5-25厘泊），并具有稳定的香料，以下步骤：（a）将碱金属次氯酸盐水溶液的pH调节至11-14.0的范围; （b）混合选自以下的物质组合物：（i）具有以下结构的化合物：其中R 1和R 2中的至少一个为C 10 -C 12直链或支链烷基和Mα， Mβ相同或不同，各自表示选自锂，钾和钠的碱金属; 和（ii）具有以下结构的至少一种化合物的混合物：＆lt; IMAGE＆gt;和具有以下结构的化合物：其中R 3“是直链烷基; 其中超过55％的R3“部分由具有11至13个碳原子的直链烷基组成，并且其中A和B各自独立地是甲基或一起形成吗啉环，其中加香量为2-甲基 -2-辛醇，由此形成预混物; （c）任选地向所述预混物中加入选自棕榈酸钠，棕榈酸棕榈酸酯，棕榈酸钾，月桂酸钠，月桂酸锂，月桂酸钾，硬脂酸钠，硬脂酸钾和硬脂酸锂的凝胶形成剂; 和（d）将所述预混合物加入经pH调节的次氯酸盐溶液中。

56. 发明授权

US4390435A Oxoalkyl esters, organoleptic uses thereof and process for preparing same 失效
标题翻译：氧代烷基酯，感官用途及其制备方法
公开(公告)号：US4390435A
公开(公告)日：1983-06-28
申请号：US396252
申请日：1982-07-08
申请人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
发明人： Michael Licciardello , Richard M. Boden , Hugh Watkins , Marie R. Hanna
IPC分类号： C11B9/00 , D06M13/00 , D06M13/12
CPC分类号： D06M13/005 , C11B9/0015 , C11B9/0061
摘要： Described is a genus of compounds defined according to the structure: ##STR1## wherein Z represents carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and wherein R represents 3-heptanyl or phenyl produced by (i) reacting a carboxylic acid with 2,2-dimethyl-1,3-propanediol to form the compound wherein Z represents carbinol; (ii) and then, if, desired, subsequently reacting the resulting alcohol to form an aldehyde; and organoleptic uses of such compounds in the field of perfumery, colognes and perfumed articles (e.g. perfumed polymers, or solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, hair preparations, hair sprays, bath preparations and the like).
摘要翻译：描述了根据以下结构定义的化合物属：其中Z表示具有以下结构的甲醇：具有以下结构的羧甲基，其中R表示3-庚基或苯基，其通过以下步骤制备：（i）与2,2-二甲基-1,3-丙二醇的羧酸形成其中Z代表甲醇的化合物; （ii）然后如果需要，随后使所得醇反应形成醛; 以及这些化合物在香料，古龙水和香料制品领域（如加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加织物柔软剂制品，头发制剂，喷发剂）中的感官用途，浴液等）。

57. 发明授权

US6051548A Trimethylcyclohexenylcyclopropyl ketones perfume composition 有权
标题翻译：三甲基环己基环丙基酮香料组合物
公开(公告)号：US6051548A
公开(公告)日：2000-04-18
申请号：US186486
申请日：1998-11-05
申请人： Richard M. Boden , Marie R. Hanna
发明人： Richard M. Boden , Marie R. Hanna
IPC分类号： C07C45/45 , C07C49/553 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0034 , C07C45/455 , C07C49/553 , C11B9/0026
摘要： Described are trimethylcyclohexenylcyclopropyl ketones having the structure: ##STR1## wherein one of the dashed lines is a carbon--carbon double bond and the other of the dashed lines is a carbon--carbon single bond, uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles, and mixtures of same with 3-methyl-1-phenylpentanol-5 and/or butanoylcyclohexane derivatives and/or acetic or propionic acid esters of o-methylphenyl isopropanol.
摘要翻译：描述了具有以下结构的三甲基环己基环丙基酮：其中虚线中的一条是碳 - 碳双键，另一条虚线是碳 - 碳单键，其用途是增强或增强或赋予香料组合物中的香料，古龙水和香料制品，以及它们与3-甲基-1-苯基戊醇-5和/或丁酰基环己烷衍生物和/或邻甲基苯基异丙醇的乙酸或丙酸酯的混合物。

58. 发明授权

US6025527A Trimethylcyclohexenylcyclopropyl ketones, process for producing same, and uses thereof in perfumery 有权
标题翻译：三甲基环己基环丙基酮，其制备方法及其在香料中的应用
公开(公告)号：US6025527A
公开(公告)日：2000-02-15
申请号：US336053
申请日：1999-06-18
申请人： Richard M. Boden , Marie R. Hanna
发明人： Richard M. Boden , Marie R. Hanna
IPC分类号： C07C45/45 , C07C49/553 , C11B9/00 , C07C49/21
CPC分类号： C11B9/0034 , C07C45/455 , C07C49/553 , C11B9/0026
摘要： Described are trimethylcyclohexenylcyclopropyl ketones having the structure: ##STR1## wherein one of the dashed lines is a carbon--carbon double bond and the other of the dashed lines is a carbon--carbon single bond, uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles, and mixtures of same with 3-methyl-1-phenylpentanol-5 and/or butanoylcyclohexane derivatives and/or acetic or propionic acid esters of o-methylphenyl isopropanol.
摘要翻译：描述了具有以下结构的三甲基环己基环丙基酮：其中虚线中的一条是碳 - 碳双键，另一条虚线是碳 - 碳单键，其用途是增强或增强或赋予香料组合物中的香料，古龙水和香料制品，以及它们与3-甲基-1-苯基戊醇-5和/或丁酰基环己烷衍生物和/或邻甲基苯基异丙醇的乙酸或丙酸酯的混合物。

59. 发明授权

US5811592A Alkyl-substituted -C.sub.1 -C.sub.3 alkoxy-C.sub.6 -cycloaliphatic compounds, organoleptic uses thereof and processes for preparing same 失效
标题翻译：烷基取代的-C 1 -C 3烷氧基-C 6 - 脂环族化合物，其感官用途及其制备方法
公开(公告)号：US5811592A
公开(公告)日：1998-09-22
申请号：US754380
申请日：1996-11-21
申请人： Michael G. Monteleone , Richard A. Weiss , Marc D. Evans , Marie R. Hanna
发明人： Michael G. Monteleone , Richard A. Weiss , Marc D. Evans , Marie R. Hanna
IPC分类号： C07C43/184 , C11B9/00 , C07C41/20
CPC分类号： C11B9/0061 , C07C43/184 , C11B9/0034 , C07C2101/14
摘要： Described are compounds defined according to the structure: ##STR1## wherein Z represents meta or para cyclohexylene or meta or para phenylene and wherein R.sub.1 and R.sub.2 are the same or different methyl or hydrogen; and wherein R.sub.3 represents C.sub.1 -C.sub.3 alkyl; and wherein the moiety: ##STR2## is ortho with respect to R.sub.2 and para or meta with respect to the moiety: ##STR3## with the proviso that the sum of the number of carbon atoms in R.sub.1, R.sub.2 and R.sub.3 is 3 or 4; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles and hair preparations; as well as processes for preparing alkyl-substituted-C.sub.1 -C.sub.3 alkoxy-C.sub.6 -cycloaliphatic compounds.
摘要翻译：描述的是根据以下结构定义的化合物：其中Z表示间位或对亚环己基或间位或对亚苯基，其中R1和R2是相同或不同的甲基或氢; 并且其中R 3表示C 1 -C 3烷基; 并且其中所述部分：相对于所述部分相对于R 2和对位或间位的邻位：条件是R 1，R 2和R 3中的碳原子数之和为3或4; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品和毛发制品;以及其用于增强或增强香水组合物，古龙水和香料制品的香气。以及制备烷基取代的-C1-C3烷氧基-C6-环脂族化合物的方法。

60. 发明授权

US5683979A Malodor counteractant composition and process for using same 失效
标题翻译：恶臭抵消剂组合物及其使用方法
公开(公告)号：US5683979A
公开(公告)日：1997-11-04
申请号：US647243
申请日：1996-05-09
申请人： Lisa Schreck , Mary E. Gordon , Marie R. Hanna , Ruth M. Sutcliffe , William L. Hamilton
发明人： Lisa Schreck , Mary E. Gordon , Marie R. Hanna , Ruth M. Sutcliffe , William L. Hamilton
IPC分类号： A01K1/015 , A61L9/01 , A61K7/46
CPC分类号： A01K1/0152 , A61L9/01
摘要： Described is a process for counteracting malodors including but not limited to pet malodor, tobacco malodor and mildew malodor comprising using as an additive to a base perfume composition a mixture consisting essentially of from about 20 up to about 60% musk, from about 30% up to about 70% citrus, and from about 1% up to about 20% mint. Adding from about 0.5% up to about 20% of such a malodor coverage formulation will yield from about a 10% up to about a 75% improvement in malodor neutralization efficacy; and a composition useful in such process.
摘要翻译：描述了一种消除恶臭的方法，包括但不限于宠物恶臭，烟草恶臭和霉变恶臭，其包括使用基本上由约20％至约60％的麝香组成的混合物，约30％至约70％的柑橘，以及约1％至约20％的薄荷。从这种恶臭覆盖制剂的约0.5％至约20％添加将产生恶臭中和效力的约10％至约75％的改善; 和在该方法中有用的组合物。

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